1,6,10-Dodecatrien-3-ol, 3,7,11-trimethyl-, (E)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSPolydimethyl siloxane with 5 % PhDB-1SPB-5DB-5
Column length (m) 30.30.30.60.50.
Carrier gas HeliumHeliumHeliumNitrogenNitrogen
Substrate      
Column diameter (mm) 0.25 0.250.350.20
Phase thickness (μm) 0.25 0.250.250.32
Tstart (C) 60.80.50.60.60.
Tend (C) 230.200.220.230.220.
Heat rate (K/min) 3.5.4.4.5.
Initial hold (min)   2. 3.
Final hold (min)  25.2.40. 
I 1571.1564.1560.1568.1564.
ReferencePripdeevech and Saansoomchai, 2013Priya, Prathapan, et al., 2012Xu, Tang, et al., 2010Gauvin-Bialecki and Marodon, 2009Kazemi and Akhavani, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1RTX-1DB-5HP-5
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.320.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.40.50.
Tend (C) 280.230.230.250.280.
Heat rate (K/min) 5.2.2.3.9.
Initial hold (min) 2.  1.3.
Final hold (min) 5.30.30.10.3.
I 1564.1533.1546.1555.1565.
ReferenceLago, Favero, et al., 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Rahimi-Nasrabadi, Gholivand, et al., 2009Aicha, Ines, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5SLB-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.100.50.50.
Tend (C) 220.230.240.250.280.
Heat rate (K/min) 3.4.5.3.5.
Initial hold (min)  4.2.2.1.
Final hold (min)  10.5.10.1.
I 1563.1564.1564.1560.1572.
ReferenceBastos, Ishimoto, et al., 2008Forero, Quijano, et al., 2008Lago, Romoff, et al., 2008Lo Presti, Sciarrone, et al., 2008Saidana, Mahjoub, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 5 CBDB-5RTX-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeHelium
Substrate      
Column diameter (mm) 0.250.320.260.250.26
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.300.240.200.290.
Heat rate (K/min) 3.4.3.2.3.
Initial hold (min)    2. 
Final hold (min)    10. 
I 1583.1544.1558.1562.1558.
ReferenceArgyropoulou, Daferera, et al., 2007Baran, von Reuss, et al., 2007Bos, Woerdenbag, et al., 2007Edris, Chizzola, et al., 2007Elfami, Bos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSCol-Elite 5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.260.250.250.250.25
Tstart (C) 60.60.30.60.60.
Tend (C) 240.250.246.300.240.
Heat rate (K/min) 4.2.3.3.2.
Initial hold (min) 2.8.   
Final hold (min) 20.15.   
I 1568.1562.1574.1555.1559.
ReferenceFarsam, Amanlou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Gudaityte and Venskutonis R.P., 2007Limberger, Scopel, et al., 2007Miyazawa and Tamura, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5DB-5DB-1DB-5HP-5
Column length (m) 30.30.50.30.30.
Carrier gas  HeliumHeHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.95.50.40.
Tend (C) 220.300.240.250.260.
Heat rate (K/min) 4.3.4.4.4.
Initial hold (min) 5.    
Final hold (min) 20.    
I 1560.1538.1567.1559.1559.
ReferenceMohottalage, Tabacchi, et al., 2007Moreno, Lima, et al., 2007Pala-Paul, Brophy, et al., 2007Pontes, de Olivera, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DB-5DB-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas Hydrogen  HeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.40.40.60.60.
Tend (C) 260.210.250.200.300.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min)      
Final hold (min) 20.33.33.20. 
I 1566.1565.1565.1534.1557.
ReferenceRojas, Velasco, et al., 2007Sylvestre, Longtin, et al., 2007Sylvestre, Pichette, et al., 2007Tiwary, Nail, et al., 2007Apel, Sobral, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5BP-1DB-5HP-5
Column length (m) 30.60.50.30.30.
Carrier gas  He N2He
Substrate      
Column diameter (mm) 0.250.250.220.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.60.
Tend (C) 300.250.220.230.246.
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min)    2. 
Final hold (min)   20.20. 
I 1550.1568.1548.1539.1564.
ReferenceApel, Sobral, et al., 2006, 2Bertrand, Comte, et al., 2006Boti, Yao, et al., 2006Choi, 2006Coronel, Cerda-Garcia-Rojas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-1HP-5BPX-5
Column length (m) 30.30.50.30.25.
Carrier gas  HeliumHeHeHelium
Substrate      
Column diameter (mm) 0.250.260.20.250.20
Phase thickness (μm) 0.250.250.330.250.13
Tstart (C) 60.60.60.50.50.
Tend (C) 280.290.250.300.230.
Heat rate (K/min) 4.3.2.5.3.
Initial hold (min)    5.2.
Final hold (min)   60.5. 
I 1562.1558.1550.1561.1556.
ReferenceEbrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Fernandez, Pintaric, et al., 2006Figuérédo, Cabassu, et al., 2006Fons, Rapior, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBRTX-1BP-1CP Sil 5 CB
Column length (m) 30.30.30.50.30.
Carrier gas   HeHeN2
Substrate      
Column diameter (mm) 0.250.250.320.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.50.
Tend (C) 210.220.300.220.200.
Heat rate (K/min) 2.3.4.2.5.
Initial hold (min) 2.    
Final hold (min) 33.3. 20. 
I 1566.1563.1542.1551.1545.
ReferenceGarneau F.X., Collin G., et al., 2006Hymete, Rohloff, et al., 2006Kula, Izydorczyk, et al., 2006Lesueur, Ban, et al., 2006Martin, Joseph, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5NB-30DB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHe HeN2
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.50.95.
Tend (C) 220.250.265.250.240.
Heat rate (K/min) 4.3.2.52.4.
Initial hold (min) 5.5.0.5  
Final hold (min)      
I 1564.1570.1552.1552.1587.
ReferenceMorteza-Semnani K., Saeedi M., et al., 2006Navaei and Mirza, 2006Nickavar B., Kamalinejad M., et al., 2006Orav, Raal, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-5DB-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHydrogenHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.70.60.60.
Tend (C) 260.250.280.280.200.
Heat rate (K/min) 4.4.4.3.2.
Initial hold (min)  2.4.  
Final hold (min)  20.  60.
I 1569.1564.1564.1530.1568.
ReferencePetrovic, Ristic, et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Rout, Naik, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSFSOT-RSL-200DB-5HP-5MSSPB-5
Column length (m) 30.30.30.30. 
Carrier gas HeHydrogenHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.25 
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.40.40.60.50.
Tend (C) 243.280.260.280.250.
Heat rate (K/min) 3.6.2.3.5.
Initial hold (min)  5.5.5.3.
Final hold (min)  5.20. 15.
I 1564.1561.1564.1566.1564.
ReferenceSabulal, Dan, et al., 2006Schmidt, Jirovetz, et al., 2006Senatore, Landolfi, et al., 2006Setzer, Noletto, et al., 2006Stojanovic, Palic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSBPX-5SPB-1BPX5
Column length (m) 30.30.50.50.25.
Carrier gas  He HeHe
Substrate      
Column diameter (mm) 0.320.250.220.20.20
Phase thickness (μm) 0.250.251.0.330.13
Tstart (C) 60.60.70.50.50.
Tend (C) 230.280.280.220.230.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min) 3.  1.2.
Final hold (min) 10. 4.10. 
I 1550.1536.1581.1547.1560.
ReferenceTohar, Mohd, et al., 2006Tzakou, Said, et al., 2006Wohlmuth, Smith, et al., 2006Wong, Lim, et al., 2006Boustie, Rapior, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5ZB-5HP-5
Column length (m) 50.30.30.60.25.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.30.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.60.60.40.60.
Tend (C) 240.240.240.250.240.
Heat rate (K/min) 2.3.3.6.3.
Initial hold (min)    7. 
Final hold (min)    1.7.
I 1565.1569.1568.1569.1563.
ReferenceChagonda and Chalchat, 2005Chaverri and Cicció, 2005Chaverri and Cicció, 2005Dötterl, Wolfe, et al., 2005Duarte, Figueira, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RSL-200DB-5DB-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.35.60.60.
Tend (C) 30.280.280.230.280.
Heat rate (K/min) 4.6.4.3.3.
Initial hold (min) 3.2.2. 30.
Final hold (min) 15.10.   
I 1563.1561.1568.1558.1536.
ReferenceFerretti, Maggi, et al., 2005Jirovetz, Buchbauer, et al., 2005Kowalski and Wolski, 2005Limberger, Sobral, et al., 2005Marongiu, Piras, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5HP-5DB-5
Column length (m) 25.25.30.30.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.150.25 0.25
Tstart (C) 50.50.70.60.40.
Tend (C) 230.230.240.240.260.
Heat rate (K/min) 3.3.5.5.2.
Initial hold (min)     5.
Final hold (min)     20.
I 1553.1553.1568.1564.1564.
ReferenceOgunwande, Olawore, et al., 2005Olawore, Ogunwande, et al., 2005Oyedeji, Yani, et al., 2005Saeidnia, Gohari, et al., 2005Senatore, Apostolides Arnold, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSBP-1DB-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.220.280.240.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min) 5.    
Final hold (min)   15.  
I 1566.1565.1561.1545.1562.
ReferenceSetzer, Noletto, et al., 2005Slavkovska, Couladis, et al., 2005Srivastava, Srivastava, et al., 2005Tzakou and Constantinidis, 2005Urdampilleta, Amat, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1DB-5DB-5BP-1
Column length (m) 50.50.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.20.20.320.250.22
Phase thickness (μm) 0.330.330.250.250.25
Tstart (C) 50.50.40.90.60.
Tend (C) 220.220.250.220.220.
Heat rate (K/min) 4.4.5.7.2.
Initial hold (min) 3.3.2.2. 
Final hold (min) 30.30.10.5.20.
I 1549.1536.1549.1550.1544.
ReferenceWong, Lee, et al., 2005Wong and Tan, 2005Wu, Krings, et al., 2005Agnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-1DB-5DB-5MSDB-5
Column length (m) 60.30.30.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 230.300.300.240.300.
Heat rate (K/min) 2.4.3.3.3.
Initial hold (min) 2.    
Final hold (min) 20.    
I 1555.1550.1541.1565.1553.
ReferenceChoi, 2004Kalemba and Thiem, 2004Lago, de Ávila, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5MSDB-5NB-30
Column length (m) 30.30.30.30.50.
Carrier gas N2 He He
Substrate      
Column diameter (mm) 0.320.250.250.250.2
Phase thickness (μm) 0.250.250.250.150.25
Tstart (C) 60.40.60.60.50.
Tend (C) 300.210.280.220.250.
Heat rate (K/min) 4.2.3.3.2.
Initial hold (min)  2. 3. 
Final hold (min)  33.30.  
I 1557.1565.1528.1555.1552.
ReferenceLis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004Marongiu, Piras, et al., 2004Mevy, Bessiere, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-1NB-30DB-5DB-5
Column length (m) 50.50.50.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.200.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.95.50.35.60.
Tend (C) 250.240.250.220.300.
Heat rate (K/min) 2.4.2.2.53.
Initial hold (min)      
Final hold (min)    6. 
I 1550.1554.1554.1563.1563.
ReferenceOrav, Stulova, et al., 2004Palá-Paúl, Velasco-Negueruela, et al., 2004Raal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Tirillini, Pellegrino, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5HP-5MSHP-1DB-1
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.320.2490.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.70.50.
Tend (C) 200.300.280.200.200.
Heat rate (K/min) 5.3.3.10.5.
Initial hold (min) 5.    
Final hold (min)      
I 1565.1560.1562.1549.1537.
ReferenceWang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004Couladis, Özcan, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1RSL-200DB-5DB-5DB-1
Column length (m) 50.30.50.30.30.
Carrier gas HeH2HeHeN2
Substrate      
Column diameter (mm) 0.20.320.20.250.25
Phase thickness (μm) 0.50.250.250.250.25
Tstart (C) 60.40.50.60.80.
Tend (C) 220.280.220.250.250.
Heat rate (K/min) 2.6.3.3.4.
Initial hold (min)  5.2.  
Final hold (min) 45.5.10.  
I 1550.1543.1563.1558.1552.
ReferenceFernandez, Lizzani-Cuvelier, et al., 2003Jirovetz, Buchbauer, et al., 2003Juteau, Jerkovic, et al., 2003Limberger, Simões-Pires, et al., 2003Mahalwal and Ali, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-5HP-5DB-1
Column length (m) 30.30.50.30.50.
Carrier gas HeHeHeHeliumN2
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.60.50.70.95.
Tend (C) 240.280.220.210.240.
Heat rate (K/min) 3.3.3.2.4.
Initial hold (min)   2.  
Final hold (min)  30. 60. 
I 1566.1552.1559.1564.1570.
ReferenceMaia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003Masotti, Juteau, et al., 2003Mookdasanit, Tamura, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas H2H2HeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 280.280.280.230.280.
Heat rate (K/min) 4.4.3.2.4.
Initial hold (min) 10.10.   
Final hold (min) 40.40.   
I 1564.1564.1544.1564.1561.
ReferencePino, Marbot, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Rotman, Ahumada, et al., 2003Sajjadi and Mehregan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-1DB-1
Column length (m) 30.60.60.60.60.
Carrier gas He  N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.70.70.
Tend (C) 240.250.250.230.230.
Heat rate (K/min) 3.5.5.2.2.
Initial hold (min)  15.15.2.2.
Final hold (min)    20.20.
I 1567.1564.1537.1557.1565.
Referenceda Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003Stashenko, Jaramillo, et al., 2003Tu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101HP-15 % Phenyl methyl siloxaneBP-1
Column length (m) 30.25.30.30.25.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.50
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.70.75.60.
Tend (C) 240.200.220.200.220.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min)    4. 
Final hold (min)   15.8.10.
I 1562.1536.1545.1564.1550.
ReferenceZoghbi, Andrade, et al., 2003Boyom, Keumedjio, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002Das, Ram, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5DB-5DB-1SE-30RSL-200
Column length (m)  30.30.50.30.
Carrier gas  N2H2HeH2
Substrate      
Column diameter (mm)  0.250.320.250.32
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.50.40.70.40.
Tend (C) 260.250.245.240.280.
Heat rate (K/min) 5.4.3.4.6.
Initial hold (min)   20. 5.
Final hold (min)     5.
I 1575.1564.1544.1556.1550.
ReferenceDiaz and Kite, 2002Farah, Fechtal, et al., 2002Gancel, Ollé, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.35.35.60.60.
Tend (C) 220.280.280.250.240.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min) 2.2.2.  
Final hold (min)  15.15.  
I 1561.1569.1570.1558.1564.
ReferenceJuteau, Masotti, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002, 2Limberger, Simões-Pires, et al., 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSPB-5HP-1DB-5DB-1
Column length (m) 30.30.50.30.60.
Carrier gas HeHeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.90.60.40.
Tend (C) 240.250.220.300.280.
Heat rate (K/min) 3.4.3.2.4.
Initial hold (min)  2.  5.
Final hold (min)  20.   
I 1567.1564.1561.1560.1544.
ReferenceMaia, Zoghbi, et al., 2002Pino, Marbot, et al., 2002Priestap, van Baren, et al., 2002Ruberto, Biondi, et al., 2002Sefidkon, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5SPB-5HP-5BP-1
Column length (m) 50.30.60.30.30.
Carrier gas N2N2HeN2N2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 240.220.220.220.220.
Heat rate (K/min) 3.5.3.5.5.
Initial hold (min)  10.5.10. 
Final hold (min)   15.  
I 1528.1564.1566.1565.1550.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2002Campeol, Flamini, et al., 2001Cornu, Carnat, et al., 2001Gallori, Flamini, et al., 2001Gupta, Mallavarapu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CBP-1OV-101DB-1PTE-5
Column length (m) 30.25.50.30.60.
Carrier gas N2NitrogenHeHeH2
Substrate      
Column diameter (mm) 0.250.250.20.20.32
Phase thickness (μm) 0.250.250.5 0.3
Tstart (C) 60.50.50.60.60.
Tend (C) 300.210.250.240.285.
Heat rate (K/min) 4.3.2.3.4.3
Initial hold (min)  2.   
Final hold (min)      
I 1551.1561.1546.1573.51564.
ReferenceKalemba, Marschall, et al., 2001Ly, Yamauchi, et al., 2001Orav, Kailas, et al., 2001Santos, Moreira, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1RTX-1HP-1
Column length (m) 60.30.25.30.25.
Carrier gas N2HeNitrogenN2H2
Substrate      
Column diameter (mm) 0.250.250.500.250.32
Phase thickness (μm) 0.250.250.250.250.17
Tstart (C) 60.60.60.60.40.
Tend (C) 220.240.220.300.260.
Heat rate (K/min) 3.3.5.4.3.
Initial hold (min) 5.   5.
Final hold (min) 22.    
I 1555.1563.1548.1552.1549.
ReferenceBailac, Dellacasa, et al., 2000Maia, Zoghbi, et al., 2000Mallavarapu, Rao, et al., 2000Kalemba, 1999Lopes, Koketsu, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 5 CBBP-1DB-5CP Sil 5 CB
Column length (m) 25.25.25.30.25.
Carrier gas N2HeN2HeN2
Substrate      
Column diameter (mm) 0.500.250.50.25 
Phase thickness (μm) 0.25  0.250.39
Tstart (C) 60.50.60.60.60.
Tend (C) 220.230.220.240.220.
Heat rate (K/min) 5.3.5.3.5.
Initial hold (min)      
Final hold (min) 10. 10.  
I 1548.1545.1548.1563.1551.
ReferenceMallavarapu, Kulkarni, et al., 1999Oyedeji, Olawore, et al., 1999Rao, Bhattacharya, et al., 1999Tellez, Canel, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5HP-5DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 60.60.60.70.60.
Tend (C) 240.240.240.290.240.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)    8. 
Final hold (min)    20. 
I 1563.1568.1570.1571.1566.
ReferenceZoghbi, Andrade, et al., 1999Zoghbi, Andrade, et al., 1999, 2Maia, Zohhbi, et al., 1998Poiana, Sicari, et al., 1998Santos, Andrade, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1CP Sil 5 CBDB-5DB-1DB-5
Column length (m) 60.25.30.60.30.
Carrier gas HeN2HeHe 
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (μm) 0.250.25 0.50 
Tstart (C) 50.50.60.50.40.
Tend (C) 280.290.240.250.210.
Heat rate (K/min) 4.4.4.8.2.
Initial hold (min) 5.  1.2.
Final hold (min)    6.33.
I 1547.1542.1562.1552.1565.
ReferenceStashenko, Cervantes, et al., 1998Bos, Woerdenbag, et al., 1997Zunino, Novillo-Newton, et al., 1997Sagrero-Nieves and Bartley, 1996Sohounhloue, Dangou, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1OV-1HP-101Methyl Silicone
Column length (m) 25.60.50.50.50.
Carrier gas HeliumHeN2H2N2
Substrate      
Column diameter (mm) 0.320.250.270.320.25
Phase thickness (μm) 0.250.250.20.30.17
Tstart (C) 60.50.80.65.80.
Tend (C) 220.250.240.300.200.
Heat rate (K/min) 4.3.53.2.2.
Initial hold (min) 2.5. 5. 
Final hold (min) 20.    
I 1547.1553.1550.1547.1553.
ReferenceThanh, Dung, et al., 1996Stashenko, Torres, et al., 1995Ramanoelina, Viano, et al., 1994Demarne and van der Walt, 1993Gopalakrishnan, Menon, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase Methyl SiliconeCP Sil 5 CBSE-54
Column length (m) 50.25.30.
Carrier gas N2 Hydrogen
Substrate    
Column diameter (mm) 0.250.250.25
Phase thickness (μm) 0.17 0.25
Tstart (C) 80.60.60.
Tend (C) 200.280.250.
Heat rate (K/min) 3.5.2.
Initial hold (min)   5.
Final hold (min)   2.
I 1551.1552.1564.
ReferenceGopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pripdeevech and Saansoomchai, 2013
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Elfami, Bos, et al., 2007
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Pontes, de Olivera, et al., 2007
Pontes, W.J.T.; de Olivera, J.C.G.; da Camara, C.A.G.; Lopes, A.C.H.R.; Gondim Jr.; de Olivera, J.V.; Barros, R.; Schwartz, M.O.E., Chemical composition and acaridical activity of the leaf and fruit essential oils of Protium heptaphyllum (Aubl.) Marchand (Burseraceae), Acta Amazonica, 2007, 37, 1, 103-110, https://doi.org/10.1590/S0044-59672007000100012 . [all data]

Ristic, Krivokuca-Dokic, et al., 2007
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Rojas, Velasco, et al., 2007
Rojas, J.; Velasco, J.; Rojas, L.B.; Carmona, J.; Morales, A., Chemical composition and antimicrobial activity of the essential oil of Baacharis latifolia Pers. and B. prunifolia H.B.K. (Asteraceae), Natural Product Communications, 2007, 2, 12, 1245-1248. [all data]

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Sylvestre, Pichette, et al., 2007
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Tiwary, Nail, et al., 2007
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Apel, Sobral, et al., 2006
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of four Plinia species (Myrtaceae), Flavour Fragr. J., 2006, 21, 3, 565-567, https://doi.org/10.1002/ffj.1638 . [all data]

Apel, Sobral, et al., 2006, 2
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of Calycorectes australis and Calycorectes psidiiflorus (Myrtaceae), Flavour Fragr. J., 2006, 21, 4, 656-658, https://doi.org/10.1002/ffj.1640 . [all data]

Bertrand, Comte, et al., 2006
Bertrand, C.; Comte, G.; Piola, F., Solid-phase microextraction of volatile compounds from flowers of two Brunfelsia species, Biochem. Syst. Ecol., 2006, 34, 5, 371-375, https://doi.org/10.1016/j.bse.2005.12.005 . [all data]

Boti, Yao, et al., 2006
Boti, J.B.; Yao, P.A.; Koukoua, G.; N'Guessan, T.Y.; Casanova, J., Components and chemical variability of Isolona campanulata Engler Diels leaf oil, Flavour Fragr. J., 2006, 21, 1, 166-170, https://doi.org/10.1002/ffj.1555 . [all data]

Choi, 2006
Choi, H.-S., Headspace analyses of fresh leaves and stems of Angelica gigas Nakai, a Korean medicinal herb, Flavour Fragr. J., 2006, 21, 4, 604-608, https://doi.org/10.1002/ffj.1602 . [all data]

Coronel, Cerda-Garcia-Rojas, et al., 2006
Coronel, A. del.C.; Cerda-Garcia-Rojas, C.M.; Joseph-Nathan, P.; Catalán, C.A.N., Chemical composition, seasonal variation and a new sesquiterpene alcohol from the essential oil of Lippia integrifolia, Flavour Fragr. J., 2006, 21, 5, 839-847, https://doi.org/10.1002/ffj.1736 . [all data]

Ebrahim Sajjadi and Mehregan, 2006
Ebrahim Sajjadi, S.; Mehregan, I., Volatile constituents of flowers and leaves of Anthemis hyalina, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 531-533, https://doi.org/10.1007/s10600-006-0207-2 . [all data]

Elfami, Komar, et al., 2006
Elfami, R.B.; Komar, R.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential oil constituents of Piper cubeba from Indonesia, 2006, retrieved from http://dissertations.ub.rug.nl/FILES/facultiew/science/2006/elfahmi/05c5.pdf. [all data]

Fernandez, Pintaric, et al., 2006
Fernandez, X.; Pintaric, C.; Lizzani-Cuvelier, L.; Loiseau, A.-M.; Morello, A.; Pellerin, P., Chemical composition of absolute and supercritical carbon dioxide extract of Aframomum melegueta, Flavour Fragr. J., 2006, 21, 1, 162-165, https://doi.org/10.1002/ffj.1554 . [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Fons, Rapior, et al., 2006
Fons, F.; Rapior, S.; Fruchier, A., Volatile composition of Clitocybe amoenolens, Tricholoma caligatum and Hebeloma radicosum, Cryptogamie, Mycologie, 2006, 27, 1, 45-55. [all data]

Garneau F.X., Collin G., et al., 2006
Garneau F.X.; Collin G.; Gagnon H.; Jean F.I.; Strobl H.; Pichette A., The essential oil composition of Devil's Club, Oplopanax horridus J. E. Smith Miq., Flavour Fragr. J., 2006, 21, 5, 792-794, https://doi.org/10.1002/ffj.1716 . [all data]

Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

Kula, Izydorczyk, et al., 2006
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Lesueur, Ban, et al., 2006
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Notes

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