1,1'-Biphenyl, 2,2',3,3',4,6'-hexachloro-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryApiezon L180.2255.Ballschmiter and Zell, 1980H2; Column length: 40. m; Column diameter: 0.30 mm
CapillaryApiezon L205.2299.Sissons and Welti, 1971He; Column length: 15. m; Column diameter: 0.20 mm

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySPB-12227.Nakano, Tsuji, et al., 198730. m/0.25 mm/0.25 μm, 4. K/min; Tstart: 130. C; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryApolane2264.Bush, Murphy, et al., 1985He; Column length: 50. m; Column diameter: 0.25 mm; Program: 70 0C (2 min) 10 0C/min (6 min) 2 0C/min -> 250 0C
CapillaryApiezon L2254.Ballschmiter and Zell, 1980H2; Column length: 40. m; Column diameter: 0.30 mm; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ballschmiter and Zell, 1980
Ballschmiter, K.; Zell, M., Analysis of polychlorinated biphenyls (PCB) by glass capillary gas chromatography, Fresenius Z. Anal. Chem., 1980, 302, 1, 20-31, https://doi.org/10.1007/BF00469758 . [all data]

Sissons and Welti, 1971
Sissons, D.; Welti, D., Structural Identification of Polychlorinated Biphenyls in Commercial Mixtures by Gas-Liquid Chromatography, Nuclear Magnetic Resonance and Mass Spectrometry, J. Chromatogr., 1971, 60, 15-32, https://doi.org/10.1016/S0021-9673(00)95526-2 . [all data]

Nakano, Tsuji, et al., 1987
Nakano, T.; Tsuji, M.; Okuno, T., Analytical methods for PCB using GC/ECD and GC/MS with capillary column, Report of the Environmental Science Institute of Hyoho Prefecture, 1987, 19, 57-62. [all data]

Bush, Murphy, et al., 1985
Bush, B.; Murphy, M.J.; Connor, S.; Snow, J.; Barnard, E., Improvements in Glass Capillary Gas Chromatographic Polychlorobiphenyl Analysis, J. Chromatogr. Sci., 1985, 23, 11, 509-515, https://doi.org/10.1093/chromsci/23.11.509 . [all data]


Notes

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