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3,5-Octadien-2-one


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5MDN-5SPB-1HP-5OV-101
Column length (m) 60.30.30.50.50.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (mum) 1.000.250.250.520.5
Tstart (C) 40.40.40.35.50.
Tend (C) 230.280.200.250.250.
Heat rate (K/min) 3.20.3.2.4.
Initial hold (min) 5.1.10.15. 
Final hold (min) 10.1. 45. 
I 1074.1098.1043.1096.1056.
ReferenceSivadier, Ratel, et al., 2009Mildner-Szkudlarz, Jelen, et al., 2003Vichi, Castellote, et al., 2003Boylston and Viniyard, 1998Misharina, Golovnya, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1OV-101
Column length (m) 50.50.50.50.50.
Carrier gas     He
Substrate      
Column diameter (mm) 0.320.320.320.320.31
Phase thickness (mum)      
Tstart (C) 0.50.0.50.0.
Tend (C) 250.250.250.250.225.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)     1.
Final hold (min)      
I 1040.1040.1065.1063.1048.
ReferenceHabu, Flath, et al., 1985Habu, Flath, et al., 1985Habu, Flath, et al., 1985Habu, Flath, et al., 1985del Rosario, de Lumen, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-101
Column length (m) 50.
Carrier gas He
Substrate  
Column diameter (mm) 0.31
Phase thickness (mum)  
Tstart (C) 0.
Tend (C) 225.
Heat rate (K/min) 3.
Initial hold (min) 1.
Final hold (min)  
I 1072.
Referencedel Rosario, de Lumen, et al., 1984
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sivadier, Ratel, et al., 2009
Sivadier, G.; Ratel, J.; Engel, E., Latency and persistence of diet volatile biomarkers in lamb fats, J. Agric. Food Chem., 2009, 57, 2, 645-652, https://doi.org/10.1021/jf802467q . [all data]

Mildner-Szkudlarz, Jelen, et al., 2003
Mildner-Szkudlarz, S.; Jelen, H.H.; Zawirska-Wojtasiak, R.; Wasowicz, E., Application of headspace - solid phase microextraction and multivariate analysis for plant oils differentiation, Food Chem., 2003, 83, 4, 515-522, https://doi.org/10.1016/S0308-8146(03)00147-X . [all data]

Vichi, Castellote, et al., 2003
Vichi, S.; Castellote, A.I.; Pizzale, L.; Conte, L.S.; Buxaderas, S.; López-Tamames, E., Analysis of virgin olive oil volatile compounds by headspace solid-phase microextraction coupled to gas chromatography with mass spectrometric and flame ionization detection, J. Chromatogr. A, 2003, 983, 1-2, 19-33, https://doi.org/10.1016/S0021-9673(02)01691-6 . [all data]

Boylston and Viniyard, 1998
Boylston, T.D.; Viniyard, B.T., Isolation of volatile flavor compounds from peanut butter using purge-and-trap technique in Instrumental Methods in Food and Beverage Analysis, D. Wetzel and G. Charalambous, ed(s)., 1998, 225-243. [all data]

Misharina, Golovnya, et al., 1991
Misharina, T.A.; Golovnya, R.V.; Charnomskii, V.V., Volatile components of boiled shrimp funchalia woodwardi and crab geryon maritae, Zh. Anal. Khim., 1991, 46, 1421-1429. [all data]

Habu, Flath, et al., 1985
Habu, T.; Flath, R.A.; Mon, T.R.; Morton, J.F., Volatile components of Rooibos tea (Aspalathus linearis), J. Agric. Food Chem., 1985, 33, 2, 249-254, https://doi.org/10.1021/jf00062a024 . [all data]

del Rosario, de Lumen, et al., 1984
del Rosario, R.; de Lumen, B.O.; Habu, T.; Flath, R.A.; Mon, T.R.; Teranishi, R., Comparison of headspace volatiles from winged beans and soybeans, J. Agric. Food Chem., 1984, 32, 5, 1011-1015, https://doi.org/10.1021/jf00125a015 . [all data]


Notes

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