5,9-Undecadien-2-one, 6,10-dimethyl-, (E)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5 MSHP-5 MSHP-5OV-1
Column length (m) 60.30.25.30.50.
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.220.250.200.250.32
Phase thickness (μm) 0.250.250.300.250.50
Tstart (C) 60.50.40.50.40.
Tend (C) 230.250.260.300.270.
Heat rate (K/min) 2.5.10.50.2.
Initial hold (min)  0.52.5. 
Final hold (min) 5.0.520.5.10.
I 1429.1453.1455.1447.1430.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Fanaro, Duarte, et al., 2012Sandoval-Montemayor, Garcia, et al., 2012Bi Kouame, Bedi, et al., 2010Da Costa, Yang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1HP-5HP-5 MSHP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.70.60.60.
Tend (C) 250.240.290.220.220.
Heat rate (K/min) 5.3.5.5.5.
Initial hold (min) 3.2. 10.10.
Final hold (min) 2.    
I 1429.1455.1455.1455.1457.
ReferenceHu, Liang, et al., 2010Kahriman, Tosun, et al., 2010Lazarevic, Radulovic, et al., 2010Ogunwande, Flamini, et al., 2010Ogunwande, Flamini, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1-MSVF-5MSVF-5Mega 5 MS
Column length (m) 30.60.30.30.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.30.40.60.40.
Tend (C) 290.200.220.300.240.
Heat rate (K/min) 5.2.2.10.3.
Initial hold (min)  4.1.2.2.
Final hold (min) 10.35.30.10. 
I 1456.1431.1461.1453.1454.
ReferenceRadulovic, Blagojevic, et al., 2010Takeoka, Hobbs, et al., 2010Fernandes, de Pinho, et al., 2009Li and Zhao, 2009Romeo, Verzera, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSDB-5HP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 40.50.60.50.70.
Tend (C) 230.280.220.240.240.
Heat rate (K/min) 2.4.3.3.5.
Initial hold (min)      
Final hold (min)      
I 1455.1454.1452.1485.1455.
ReferenceScrivanti, Anton, et al., 2009Zhao, Zeng, et al., 2009Bastos, Ishimoto, et al., 2008Sarikurkcu, Tepe, et al., 2008Asekun, Olusegun, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5DB-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.251.00.250.25
Tstart (C) 60.60.35.40.60.
Tend (C) 280.250.240.240.240.
Heat rate (K/min) 3.2.15.3.2.
Initial hold (min)  8.7.  
Final hold (min)  15.10.  
I 1435.1446.1448.1447.1447.
ReferenceBasta, Tzakou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Gogus, Ozel, et al., 2007Machado, Bastos, et al., 2007Miyazawa and Tamura, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5CP Sil 5 CBRTX-1HP-5
Column length (m) 30.30.25.30.30.
Carrier gas Helium HeHeHelium
Substrate      
Column diameter (mm) 0.250.25 0.320.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.40.80.60.40.
Tend (C) 280.240.270.300.240.
Heat rate (K/min) 3.5.10.4.4.
Initial hold (min)  3.   
Final hold (min)  10.  5.
I 1455.1460.1430.1430.1444.
ReferenceVagionas, Graikou, et al., 2007Wenguang, Wenlai, et al., 2007Ayoub, Al-Azizi, et al., 2006Kula, Izydorczyk, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5PE-5SPB-5DB-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeliumHydrogenHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.100.60.70.40.
Tend (C) 250.280.250.280.260.
Heat rate (K/min) 4.3.4.4.2.
Initial hold (min)  1.2.4.5.
Final hold (min)   20. 20.
I 1461.1460.1455.1451.1452.
ReferenceNajafpour Navaei, Mirza, et al., 2006Pandey-Rai S., Mallavarapu G.R., et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Senatore, Landolfi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5HP-1Methyl Silicone
Column length (m) 30.30.30.50.60.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.3
Phase thickness (μm) 0.250.250.250.5 
Tstart (C) 60.60.60.60.50.
Tend (C) 250.280.250.250.240.
Heat rate (K/min) 2.3.10.2.3.
Initial hold (min) 8. 2.  
Final hold (min) 15. 10.60. 
I 1446.1424.1460.1428.1445.
ReferenceTigrine-Kordiani, Meklati, et al., 2006Tzakou, Said, et al., 2006Wang, Yang, et al., 2006Bendimerad and Bendiab, 2005Chalchat and Özcan, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX5Polymethylsiloxane, (PMS-20000)HP-5HP-5CP Sil 5 CB
Column length (m) 25.25.25.60.30.
Carrier gas HeliumHeH2HeHe
Substrate      
Column diameter (mm) 0.220.200.320.320.25
Phase thickness (μm) 0.25 0.520.250.25
Tstart (C) 50.50.40.30.40.
Tend (C) 320.250.240.260.220.
Heat rate (K/min) 5.3.4.2.4.
Initial hold (min) 5.3. 2.1.
Final hold (min)    28. 
I 1457.1422.1439.1457.51455.
ReferenceDickschat, Bode, et al., 2005Dohou, Yamni, et al., 2005Jovanovic, Kitic, et al., 2005Leffingwell and Alford, 2005Rohloff and Bones, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-5HP-5SPB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.320.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 40.40.40.40.50.
Tend (C) 220.220.260.300.220.
Heat rate (K/min) 4.4.2.4.4.
Initial hold (min) 1.1.5. 3.
Final hold (min)   20.5.30.
I 1455.1455.1452.1446.1428.
ReferenceRohloff and Bones, 2005Rohloff and Bones, 2005Senatore, Apostolides Arnold, et al., 2005Utsunomia, Kawata, et al., 2005Wong and Tan, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1ZB-5RTX-1HP-5MSDB-5
Column length (m) 50.60.30.30.30.
Carrier gas  HeN2HeHelium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.40.60.60.60.
Tend (C) 220.260.300.280.240.
Heat rate (K/min) 2.6.4.3.2.
Initial hold (min)  4.6   
Final hold (min) 20.1.  999.
I 1426.1461.1428.1452.1446.
ReferenceBlanc, Muselli, et al., 2004Jürgens and Dötterl, 2004Kalemba and Thiem, 2004Malencic, Couladis, et al., 2004Miyazawa, Fuhita, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5HP-5OV-101
Column length (m) 50.30.60.30.25.
Carrier gas Helium HeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm)  0.250.25  
Tstart (C) 60.90.35.70.50.
Tend (C) 240.200.280.210.200.
Heat rate (K/min) 2.30.5.2.5.
Initial hold (min)   2.  
Final hold (min) 999.10.4.60. 
I 1446.1444.1445.1454.1452.
ReferenceMiyazawa, Fujita, et al., 2004Robledo and Arzuffi, 2004Dhanda, Pegg, et al., 2003Mookdasanit, Tamura, et al., 2003Boyom, Keumedjio, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5Optima-1RSL-200PTE-5
Column length (m) 30.30.25.30.60.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.200.320.32
Phase thickness (μm) 0.250.250.250.250.3
Tstart (C) 60.60.50.40.60.
Tend (C) 280.240.250.280.285.
Heat rate (K/min) 3.3.3.6.4.3
Initial hold (min)   3.5. 
Final hold (min) 30.  5. 
I 1444.1453.1431.1428.1453.
ReferenceCaredda, Marongiu, et al., 2002Tellez, Khan, et al., 2002Brun, Bessière, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1HP-5DB-5OV-101CP Sil 5 CB
Column length (m) 25.30.30.50.25.
Carrier gas HeH2HeNitrogenN2
Substrate      
Column diameter (mm) 0.200.250.250.25 
Phase thickness (μm) 0.250.250.25 0.39
Tstart (C) 50.40.60.40.60.
Tend (C) 250.280.240.200.220.
Heat rate (K/min) 3.3.3.2.5.
Initial hold (min) 3.10. 10. 
Final hold (min)  10.   
I 1433.1452.1453.1432.1430.
Referencede Beck, Bessière, et al., 2000Bicalho, Pereira, et al., 2000Maia, Zoghbi, et al., 2000Tamura, Boonbumrung, et al., 2000Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-1DB-1OV-101OV-101
Column length (m) 30.60.60.50.50.
Carrier gas He HeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Tstart (C) 60.30.30.80.80.
Tend (C) 240.200.200.200.200.
Heat rate (K/min) 4.4.4.2.2.
Initial hold (min)  25.25.  
Final hold (min)  20.20.  
I 1429.1429.1429.1427.1431.
ReferenceLamarque, Maestri, et al., 1998Buttery, Ling, et al., 1997Buttery and Ling, 1995Tamura, Nakamoto, et al., 1995Tamura, Nakamoto, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSOV-101OV-101DB-5DB-1
Column length (m) 30.50.50.60.60.
Carrier gas Helium  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm)    1.0 
Tstart (C) 50.80.80.40.30.
Tend (C) 250.200.200.240.200.
Heat rate (K/min) 4.2.2.3.4.
Initial hold (min)     25.
Final hold (min)     5.
I 1449.1422.1425.1452.1428.
ReferenceGomez and Ledbetter, 1994Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Berdague, Denoyer, et al., 1991Buttery, Teranishi, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 50.50.50.50.50.
Carrier gas NitrogenNitrogenN2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Tstart (C) 70.80.80.80.80.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1434.1432.1430.1431.1431.
ReferenceSugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Sugisawa, Yamamoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-1DB-1DB-1
Column length (m) 50.50.50.50.60.
Carrier gas N2N2   
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm)      
Tstart (C) 80.80.0.50.50.
Tend (C) 200.200.250.250.250.
Heat rate (K/min) 2.2.3.3.4.
Initial hold (min)     0.1
Final hold (min)     5.
I 1429.1431.1429.1429.1427.
ReferenceSugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Habu, Flath, et al., 1985Habu, Flath, et al., 1985Flath, Mon, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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