trans-β-Ocimene

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-5-10(4)8-6-7-9(2)3/h5,7-8H,1,6H2,2-4H3/b10-8+
IUPAC Standard InChIKey: IHPKGUQCSIINRJ-CSKARUKUSA-N
CAS Registry Number: 3779-61-1
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: 1,3,6-Octatriene, 3,7-dimethyl-, (E)-; β-trans-Ocimene; trans-3,7-Dimethyl-1,3,6-Octatriene; Ocimene, trans-β-; (E)-Ocimene; trans-Ocimene; (3E)-3,7-Dimethyl-1,3,6-octatriene; β-(E)-Ocimene; β-Ocimene, (E)-; (E)- β-Ocimene; (E)-3,7-Dimethyl-1,3,6-octatriene; Ocimene, trans; t-β-Ocimene; Ocimene trans-beta-form; (E)-3,7-Dimethylocta-1,3,6-triene; t-Ocimene; β-Ocymene, (E)-; ocimene-x; (E)- β-Ocimene (trans-ocimene); (E)-β-3,7-dimethyl-1,3,6-octatriene ((E)-β-ocimene); (E)- β-Ocymene
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	RTX-1	Mega-5	HP-5 MS	HP-5 MS
Column length (m)	60.	60.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	40.	50.
T_end (C)	250.	230.	220.	250.	180.
Heat rate (K/min)	3.	2.	3.	3.	2.
Initial hold (min)	1.		1.	1.
Final hold (min)	20.	5.	5.	3.
I	1048.	1041.	1050.	1050.	1050.
Reference	Sardashti, Valizadeh, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Dell'Agli, Sanna, et al., 2012	Jian-Yu, Zhu, et al., 2012	Phungpanya, Thongpoon, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5 MS	HP-5
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	Hydrogen	Hydrogen	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.52	0.52	0.52	0.25	0.25
T_start (C)	40.	40.	40.	50.	60.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	4.	4.	7.	3.
Initial hold (min)				1.
Final hold (min)	10.	10.	10.	5.
I	1036.	1045.	1045.	1049.	1050.
Reference	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP-Sil 5 CB	HP-5	SE-30 MS	HP-5 MS
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	Helium	Hydrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	40.	50.	60.	50.	40.
T_end (C)	250.	230.	240.	250.	260.
Heat rate (K/min)	3.	3.	3.	5.	4.
Initial hold (min)	5.		2.	5.
Final hold (min)	20.			10.	5.
I	1049.	1045.	1051.	1047.	1050.
Reference	Cao, Li, et al., 2011	Esseien, Aboaba, et al., 2011	Kahriman, Tosun, et al., 2011	Menichini, Tundis, et al., 2011	Miyazawa, Marumoto, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	ZB-5	ZB-5	DB-5 MS	DB-5 MS
Column length (m)	60.	30.	30.	25.	25.
Carrier gas	Helium	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.30	0.30
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	40.	40.	50.	50.
T_end (C)	220.	200.	200.	240.	240.
Heat rate (K/min)	10.	5.	5.	3.	3.
Initial hold (min)	1.	5.	5.
Final hold (min)	15.		5.
I	1048.	1059.	1058.	1046.	1046.
Reference	Piyachaiseth, Jirapakkul, et al., 2011	Vazques, Aimar, et al., 2011	Vazquez, Demmel, et al., 2011	Chalchat, Figueredo, et al., 2010	Chalchat, Figueredo, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTx-1	RTX-1	DB-5	OV-1	DB-5 MS
Column length (m)	60.	60.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	40.
T_end (C)	230.	230.	250.	250.	250.
Heat rate (K/min)	2.	2.	2.	5.	5.
Initial hold (min)				3.	15.
Final hold (min)	35.	30.		2.	15.
I	1041.	1041.	1050.	1028.	1048.
Reference	Dib, Bendahou, et al., 2010	Dib, Djabou, et al., 2010	Ho, Wang, et al., 2010	Hu, Liang, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5	HP-5 MS	HP-5 MS	HP-5
Column length (m)		30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Hydrogen
Substrate
Column diameter (mm)		0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	100.	70.
T_end (C)	220.	260.	220.	220.	290.
Heat rate (K/min)	5.	4.	5.	2.	5.
Initial hold (min)	10.		10.
Final hold (min)	30.	5.
I	1041.	1049.	1052.	1044.	1048.
Reference	Mishra, Chaudhary, et al., 2010	Miyazawa, Kawauchi, et al., 2010	Ogunwande, Flamini, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	SLB-5 MS	DB-1-MS	CP Sil 5 CB	DB-5
Column length (m)	10.	10.	60.	25.	30.
Carrier gas	Helium	Helium	Helium		Helium
Substrate
Column diameter (mm)	0.10	0.10	0.25	0.25	0.25
Phase thickness (μm)	0.10	0.10	0.25	0.15	0.25
T_start (C)	50.	50.	30.	50.	80.
T_end (C)	250.	250.	200.	230.	240.
Heat rate (K/min)	10.	10.	2.	3.	3.
Initial hold (min)			4.
Final hold (min)			35.		2.
I	1045.	1053.	1041.	1045.	1046.
Reference	Scandinaro, Tranchida, et al., 2010	Scandinaro, Tranchida, et al., 2010	Takeoka, Hobbs, et al., 2010	Usman, Zubair, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	SE-54	ZB-5	SPB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.53
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.50
T_start (C)	60.	70.	60.	50.	50.
T_end (C)	240.	220.	260.	240.	210.
Heat rate (K/min)	3.	2.	2.	3.	3.
Initial hold (min)			5.		5.
Final hold (min)			999.	1.	45.
I	1036.	1037.	1050.	1016.	1061.
Reference	Alim, Goze, et al., 2009	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009	Gardini, Beletti, et al., 2009	Gilani, Shah, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5MS	HP-5
Column length (m)	30.	50.	30.	60.	25.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.33
T_start (C)	50.	60.	50.	70.	60.
T_end (C)	250.	220.	250.	250.	240.
Heat rate (K/min)	5.	5.	5.	3.	3.
Initial hold (min)	2.	3.
Final hold (min)					7.
I	1050.	1050.	1069.	1048.	1035.
Reference	Ho, Wang, et al., 2009	Kazemi and Akhavani, 2009	Koba, Catherine, et al., 2009	Males, Plazibat, et al., 2009	Maridass, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	DB-5	5 % Phenyl methyl siloxane	DB-5
Column length (m)	60.	60.	30.	60.	50.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.32
T_start (C)	60.	60.	45.	90.	60.
T_end (C)	230.	230.	250.	225.	220.
Heat rate (K/min)	2.	2.	3.	3.	5.
Initial hold (min)			3.		3.
Final hold (min)	30.	30.	5.	3.	5.
I	1040.	1041.	1051.	1049.	1050.
Reference	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Porto, Decorti, et al., 2009	Retta, Gattuso, et al., 2009	Shafaghat and Sadeghi, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	DB-5 MS	HP-5MS	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	50.	50.	50.
T_end (C)	220.	250.	240.	280.	280.
Heat rate (K/min)	3.	4.	5.	4.	9.
Initial hold (min)	2.	2.			3.
Final hold (min)	70.	2.			3.
I	1044.	1049.	1050.	1047.	1050.
Reference	Shimizu, Imayoshi, et al., 2009	Su, Wang, et al., 2009	Wannes, Mhamdi, et al., 2009	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5 MS	SLB-5 MS	ZB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		N2	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	45.
T_end (C)	280.	220.	230.	250.	230.
Heat rate (K/min)	3.	5.	4.	3.	3.
Initial hold (min)		10.	4.	2.
Final hold (min)			10.	10.
I	1040.	1052.	1050.	1045.	1033.
Reference	Baziou, Couladis, et al., 2008	Flamini, Tebano, et al., 2008	Forero, Quijano, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5 MS	BPX-5	RTX-5	HP-5
Column length (m)	30.	30.	7.5	20.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.10	0.18	0.25
Phase thickness (μm)	0.25	0.25	10.	0.20	0.32
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	300.	250.	240.	280.	250.
Heat rate (K/min)	5.	2.	3.	4.	5.
Initial hold (min)	5.	8.		1.	30.
Final hold (min)	5.	15.
I	1044.	1045.	1050.	1052.	1051.
Reference	Noudogbessi, Yedomonhan, et al., 2008	Sahraoui, Vian, et al., 2008	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008	Yassa and Akhani, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SE-54	DB-5	HP-5MS	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	230.	260.	220.	280.	240.
Heat rate (K/min)	3.	2.	5.	3.	3.
Initial hold (min)	10.	5.	3.
Final hold (min)	10.	20.	5.
I	1050.	1051.	1045.	1043.	1036.
Reference	Adams, Beauchamp, et al., 2007	Alma, Ertas, et al., 2007	Amiri, 2007	Basta, Pavlovic, et al., 2007	Bos, Woerdenbag, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5MS	DB-5	HP-5	ZP-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	N2	He	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.26	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	240.	240.	290.	240.	260.
Heat rate (K/min)	5.	3.	3.	4.	6.
Initial hold (min)	1.			2.	7.
Final hold (min)	4.			20.	1.
I	1050.	1050.	1036.	1049.	1058.
Reference	Cheraif, Ben Jannet, et al., 2007	Da Silva J.K.R., Sousa P.J.C., et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Füssel, Dötterl, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	Col-Elite 5MS	BP-1	DB-5	DB-5
Column length (m)	60.	30.		30.	30.
Carrier gas	Nitrogen	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	30.	60.	60.	40.
T_end (C)	250.	246.	220.	300.	240.
Heat rate (K/min)	4.	3.	5.	3.	3.
Initial hold (min)	1.
Final hold (min)	10.		6.
I	1040.	1057.	1040.	1031.	1003.
Reference	Ghasempour, Shirinpour, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Kiran, Devi, et al., 2007	Limberger, Scopel, et al., 2007	Machado, Bastos, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5Sil MS	ZB-5	DB-1	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He		Helium	Helium	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	260.	220.	260.	300.	240.
Heat rate (K/min)	5.	4.	2.5	3.	3.
Initial hold (min)	2.	5.	1.
Final hold (min)	10.	20.	20.
I	1050.	1054.	1037.	1033.	1051.
Reference	Matasyoh, Matasyoh, et al., 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007	Moreno, Lima, et al., 2007	Oliveira, Leitão, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BPX-5	DB-1	HP-5 MS	DB-5
Column length (m)	50.	50.	60.	60.	30.
Carrier gas	He	He	Nitrogen	Hydrogen	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	95.	50.	60.	60.	50.
T_end (C)	240.	300.	250.	260.	240.
Heat rate (K/min)	4.	4.	4.	4.	4.
Initial hold (min)		1.	1.
Final hold (min)		10.	10.	20.
I	1041.	1056.	1040.	1039.	1047.
Reference	Pala-Paul, Brophy, et al., 2007	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Rojas, Velasco, et al., 2007	Sefidkon, Abbasi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	Elite-5MS	HP-5 MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas			He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	210.	250.	280.	280.	280.
Heat rate (K/min)	2.	2.	4.	3.	3.
Initial hold (min)			5.
Final hold (min)	33.	33.	10.
I	1057.	1057.	1046.	1053.	1015.
Reference	Sylvestre, Longtin, et al., 2007	Sylvestre, Pichette, et al., 2007	Tava, Pecetti, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	60.	40.	60.	50.	50.
T_end (C)	280.	250.	250.	280.	280.
Heat rate (K/min)	3.	3.	5.	9.	9.
Initial hold (min)		5.	30.	3.	3.
Final hold (min)		10.		3.	3.
I	1050.	1046.	1051.	1047.	1048.
Reference	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Yassa and Akhani, 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5	HP-1	BP-1	HP-1
Column length (m)	25.	60.	50.	50.	50.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)		0.25	0.2	0.22	0.2
Phase thickness (μm)		0.25	0.33	0.25	0.33
T_start (C)	80.	60.	60.	60.	60.
T_end (C)	270.	250.	250.	220.	250.
Heat rate (K/min)	10.	3.	2.	2.	2.
Initial hold (min)					4.
Final hold (min)			20.	20.	30.
I	1041.	1047.	1036.	1037.	1032.
Reference	Ayoub, Al-Azizi, et al., 2006	Bertrand, Comte, et al., 2006	Berlioz, Cordella, et al., 2006	Boti, Yao, et al., 2006	Castel, Fernandez, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	Ultra-2	HP-5	HP-5MS	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	Helium	H2	He		Helium
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.25	0.26
Phase thickness (μm)	0.20	0.33	0.25	0.25	0.25
T_start (C)	70.	40.	60.	60.	60.
T_end (C)	220.	280.	246.	280.	290.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)		2.
Final hold (min)	15.	10.
I	1035.	1056.	1050.	1053.	1036.
Reference	Cavaleiro, Pinto, et al., 2006	Ceva-Antunes, Bizzo, et al., 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	HP-1	HP-5	DB-5
Column length (m)	50.	50.	50.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.22	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	220.	250.	300.	250.
Heat rate (K/min)	2.	2.	2.	5.	3.
Initial hold (min)				5.
Final hold (min)	20.	20.	60.	5.	10.
I	1034.	1034.	1033.	1048.	1041.
Reference	Fanciullino, Tomi, et al., 2006	Fanciullino, Tomi, et al., 2006	Fernandez, Pintaric, et al., 2006	Figuérédo, Cabassu, et al., 2006	Havlik, Kokoska, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	CP Sil 5 CB	BP-1
Column length (m)	30.	30.	30.	25.
Carrier gas	He	He	Helium		Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	260.	260.	230.	220.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)
Final hold (min)					6.
I	1050.	1050.	1047.	1038.	1040.
Reference	Ibañez and Usubillaga, 2006	Ibanez and Usubillaga, 2006	Javidnia, Miri, et al., 2006	Kasali, Ekundayo, et al., 2006	Kiran, Bhavani, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	CP Sil 5 CB	CP Sil 5 CB	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He	N2	N2	Helium	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	90.	50.	50.	50.	60.
T_end (C)	220.	300.	200.	250.	220.
Heat rate (K/min)	7.	4.	5.	3.	4.
Initial hold (min)	2.			5.	5.
Final hold (min)
I	1044.	1043.	1038.	1048.	1052.
Reference	Kitchlu, Bakshi, et al., 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006	Mirza, Navaei, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	SE-52	DB-1
Column length (m)	30.	30.	25.	50.	50.
Carrier gas	He		N2	Helium	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15		0.25
T_start (C)	50.	50.	50.	50.	95.
T_end (C)	250.	265.	200.	240.	240.
Heat rate (K/min)	4.	2.5	4.	3.	4.
Initial hold (min)		0.5	3.
Final hold (min)
I	1052.	1047.	1045.	1050.	1048.
Reference	Najafpour Navaei, Mirza, et al., 2006	Nickavar B., Kamalinejad M., et al., 2006	Ouamba, Ouabonzi, et al., 2006	Ozcan, Chalchat, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	DB-5	HP-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Hydrogen	Hydrogen	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	70.	50.	60.
T_end (C)	250.	280.	280.	280.	280.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)	2.	4.	4.	2.
Final hold (min)	20.			10.
I	1051.	1050.	1050.	1050.	1017.
Reference	Pino, Marquez, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Sauri-Duch, et al., 2006	Pitarokili, Tzakou, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	H2		He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	240.	250.	200.	200.	260.
Heat rate (K/min)	3.	10.	2.	2.	5.
Initial hold (min)		5.
Final hold (min)			60.	60.
I	1052.	1049.	1050.	1051.	1049.
Reference	Potzernheim, Bizzo, et al., 2006	Robinson, 2006	Rout, Naik, et al., 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	FSOT-RSL-200	DB-5	DB-5	DB-1	HP-5
Column length (m)	30.	30.	30.	60.	25.
Carrier gas	Hydrogen	He	He	He	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25		0.33
T_start (C)	40.	50.	40.	40.	30.
T_end (C)	280.	240.	240.	250.	280.
Heat rate (K/min)	6.	4.	4.	4.	3.
Initial hold (min)	5.
Final hold (min)	5.
I	1049.	1053.	1050.	1042.	1049.
Reference	Schmidt, Jirovetz, et al., 2006	Sefidkon, Abbasi, et al., 2006	Sefidkon and Jamzad, 2006	Sefidkon, Jamzad, et al., 2006	Shafi, Jose, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP Sil 5 CB	Methyl Silicone	SPB-5
Column length (m)	30.	25.	25.	25.	60.
Carrier gas	H2	H2		N2	He
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.3	0.32
Phase thickness (μm)	0.18			0.15	1.
T_start (C)	60.	50.	50.	50.	40.
T_end (C)	240.	230.	230.	210.	230.
Heat rate (K/min)	3.	3.	3.	2.	3.
Initial hold (min)				5.	5.
Final hold (min)					2.
I	1049.	1044.	1043.	1055.	1052.
Reference	Silva, Oliveira, et al., 2006	Tesso, König, et al., 2006	Tesso, Kubeczka, et al., 2006	Tonzibo, Coffy, et al., 2006	Tornambe, Cornu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	SPB-1	SPB-1	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	60.	60.	50.	50.	40.
T_end (C)	240.	250.	220.	250.	250.
Heat rate (K/min)	4.	10.	4.	4.	4.
Initial hold (min)		2.	1.	1.
Final hold (min)		10.	10.	10.
I	1049.	1042.	1037.	1037.	1038.
Reference	Trilles, Bombarda, et al., 2006	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	He	He	He
Substrate
Column diameter (mm)		0.25	0.25	0.3	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.15
T_start (C)	90.	60.	60.	60.	40.
T_end (C)	220.	210.	280.	240.	220.
Heat rate (K/min)	7.	3.	3.	2.	3.
Initial hold (min)	2.	5.			5.
Final hold (min)
I	1041.	1048.	1041.	1051.	1045.
Reference	Ahuja, Bakshi, et al., 2005	Askari and Sefidkon, 2005	Basta, Tzakou, et al., 2005	Chagonda and Chalchat, 2005	Chagonda and Chalchat, 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	ZB-5	ZB-5	HP-5	DB-5
Column length (m)	60.	60.	60.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.2	0.25
Phase thickness (μm)	1.	0.25	0.25	0.33	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	230.	250.	250.	240.	300.
Heat rate (K/min)	3.	6.	6.	3.	3.
Initial hold (min)	5.	7.	7.		3.
Final hold (min)		1.	1.	7.
I	1050.	1058.	1058.	1044.	1043.
Reference	Cornu, Kondjoyan, et al., 2005	Dötterl and Jürgens, 2005	Dötterl, Wolfe, et al., 2005	Duarte, Figueira, et al., 2005	Ferraz, Limberger, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5MS	HP-5MS	CP Sil 5 CB
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	50.	60.	50.	60.
T_end (C)	30.	300.	200.	250.	250.
Heat rate (K/min)	4.	5.	4.	3.	5.
Initial hold (min)	3.	5.	30.	3.
Final hold (min)	15.	5.		10.	10.
I	1050.	1048.	1042.	1052.	1041.
Reference	Ferretti, Maggi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Gauvin and Smadja, 2005	Ghasemi Y., Faridi P., et al., 2005	Jassbi, Mehrdad, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-1	RTX-5 MS	SPB-5
Column length (m)	30.	60.	50.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	50.	95.	50.	60.
T_end (C)	240.	250.	240.	280.	250.
Heat rate (K/min)	3.	4.	4.	8.	4.
Initial hold (min)		5.		2.	2.
Final hold (min)				2.	20.
I	1053.	1049.	1041.	1052.	1050.
Reference	Khayyat and Karimi, 2005	Khajeh, Yamini, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Pellati, Benvenuti, et al., 2005	Pino, Marbot, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	HP-5MS	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	220.	220.	220.	280.	275.
Heat rate (K/min)	4.	4.	6.	4.	4.
Initial hold (min)	1.	1.	3.
Final hold (min)
I	1050.	1050.	1056.	1049.	1046.
Reference	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Safaei-Ghomi, Bamoniri, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	280.	240.	280.	300.	300.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)			5.
Final hold (min)
I	1045.	1050.	1046.	1039.	1039.
Reference	Sajjadi, 2005	Sefidkon and Jamzad, 2005	Setzer, Noletto, et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	BP-1	DB-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.50
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	230.	280.	220.	210.	260.
Heat rate (K/min)	3.	3.	5.	2.	3.
Initial hold (min)				2.
Final hold (min)	20.		15.	33.	20.
I	1050.	1044.	1035.	1058.	1048.
Reference	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Srivastava, Srivastava, et al., 2005	Stevanovic, Garneau, et al., 2005	Topçu, Barla, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-5 MS	DB-1	HP-5MS
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	280.	280.	240.	240.	220.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)					5.
Final hold (min)					10.
I	1017.	1019.	1050.	1030.	1046.
Reference	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005	Urdampilleta, Amat, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Vichi, Riu-Aumatell, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	DB-5	BP-1	SE-52
Column length (m)	50.	30.	30.	50.	25.
Carrier gas	He	H2	He		N2
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.22	0.32
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.15
T_start (C)	50.	50.	90.	60.	45.
T_end (C)	220.	290.	220.	220.	200.
Heat rate (K/min)	4.	4.	7.	2.	3.
Initial hold (min)	3.		2.		5.
Final hold (min)	30.		5.	20.	30.
I	1037.	1044.	1037.	1035.	1063.
Reference	Wong, Lee, et al., 2005	Abreu, Reis, et al., 2004	Agnihotri, Thappa, et al., 2004	Blanc, Muselli, et al., 2004	Cakir, Kordali, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-5	DB-5	DB-5	ZB-5
Column length (m)	30.	60.	30.	25.	60.
Carrier gas	He	He	N2	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	40.
T_end (C)	240.	200.	230.	240.	260.
Heat rate (K/min)	2.	4.	2.	3.	6.
Initial hold (min)					4.6
Final hold (min)		30.			1.
I	1050.	1058.	1050.	1050.	1054.
Reference	Cicció, 2004	Gauvin, Ravaomanarivo, et al., 2004	González, Guerra, et al., 2004	JAvidnia, Mojab, et al., 2004	Jürgens and Dötterl, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	SE-54	RTX-1	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.053	0.32	0.25
Phase thickness (μm)	0.25	0.25	1.5	0.25	0.25
T_start (C)	40.	60.	100.	60.	40.
T_end (C)	280.	300.	250.	300.	210.
Heat rate (K/min)	4.	4.	5.	4.	2.
Initial hold (min)	4.				2.
Final hold (min)					33.
I	1046.	1041.	1055.	1040.	1058.
Reference	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-1	DB-1	DB-1	NB-30
Column length (m)	30.	60.	50.	50.	50.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	70.	95.	50.
T_end (C)	280.	270.	220.	240.	250.
Heat rate (K/min)	3.	4.	4.	4.	2.
Initial hold (min)
Final hold (min)	30.
I	1016.	1045.	1034.	1032.	1039.
Reference	Marongiu, Piras, et al., 2004	Nik, Mirza, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Arak, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5MS	HP-5MS	DB-5	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	He		He
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	90.	60.	50.	60.
T_end (C)	250.	200.	280.	250.	300.
Heat rate (K/min)	2.	30.	4.	3.	3.
Initial hold (min)				5.
Final hold (min)		10.
I	1039.	1064.	1045.	1050.	1039.
Reference	Raal, Paaver, et al., 2004	Robledo and Arzuffi, 2004	Sadeghpour, Asghari, et al., 2004	Sefidkon, Jamzad, et al., 2004	Suyenaga, Apel, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 8 CB	CP Sil 8 CB	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	300.	200.	200.	240.	280.
Heat rate (K/min)	3.	10.	5.	4.	3.
Initial hold (min)		3.	5.
Final hold (min)		2.
I	1050.	1050.	1049.	1040.	1048.
Reference	Tirillini, Pellegrino, et al., 2004	Wang and Guo-Y. -L., 2004	Wang, Guo, et al., 2004	Cabanillas, Lopez, et al., 2003	Couladis, Özcan, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	RTX-5Sil	DB-5	DB-5
Column length (m)	60.	60.	30.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)			0.25
T_start (C)	50.	50.	70.	50.	50.
T_end (C)	250.	250.	200.	200.	220.
Heat rate (K/min)	4.	4.	4.	3.	3.
Initial hold (min)
Final hold (min)			10.
I	1037.	1037.	1046.	1045.	1061.
Reference	Dabiri and Sefidkon, 2003	Dabiri and Sefidkon, 2003, 2	Dudai, Larkov, et al., 2003	Edris, Shalaby, et al., 2003	Edris, Shalaby, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-1	DB-1	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	50.	60.	60.
T_end (C)	220.	200.	200.	275.	275.
Heat rate (K/min)	5.	10.	5.	4.	4.
Initial hold (min)	20.
Final hold (min)	20.
I	1054.	1039.	1038.	1048.	1049.
Reference	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003	Ghannadi and Zolfaghari, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RSL-200	RSL-200	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	H2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	35.	60.
T_end (C)	275.	280.	280.	280.	280.
Heat rate (K/min)	4.	6.	6.	5.	5.
Initial hold (min)		5.	5.	2.5
Final hold (min)		5.	5.
I	1049.	1042.	1039.	1030.	1035.
Reference	Hajhashemi, Ghannadi, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Kanjilal, Kotoky, et al., 2003	Lago, de Ávila, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	ZB-1	DB-1	HP-5
Column length (m)	30.	50.	30.	60.	30.
Carrier gas	He	He	N2	He	Helium
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	45.	50.	70.
T_end (C)	240.	220.	230.	270.	210.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)		2.
Final hold (min)					60.
I	1047.	1048.	1033.	1046.	1048.
Reference	Maia, Taveira, et al., 2003	Masotti, Juteau, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	HP-5	DB-1	DB-5
Column length (m)	50.	30.	30.	60.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	75.
T_end (C)	250.	280.	280.	250.	220.
Heat rate (K/min)	2.	4.	3.	4.	3.
Initial hold (min)		10.			4.
Final hold (min)		40.
I	1038.	1051.	1032.	1025.	1051.
Reference	Orav, Kailas, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Priestap, van Baren, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	HP-5MS	HP-5	DB-1	DB-5
Column length (m)	50.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	250.	275.	280.	280.	240.
Heat rate (K/min)	2.	4.	4.	4.	3.
Initial hold (min)
Final hold (min)
I	1040.	1051.	1048.	1046.	1047.
Reference	Raal, Arak, et al., 2003	Sadraei, Ghannadi, et al., 2003	Sajjadi and Mehregan, 2003	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	DB-1	HP-5
Column length (m)	60.	60.	60.	50.	25.
Carrier gas				N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.53
T_start (C)	40.	40.	40.	90.	40.
T_end (C)	250.	250.	250.	240.	280.
Heat rate (K/min)	5.	5.	5.	4.	4.
Initial hold (min)	15.	15.	15.
Final hold (min)
I	1043.	1043.	1043.	1038.	1050.
Reference	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Randjelovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	HP-5
Column length (m)	25.	25.	25.	25.	30.
Carrier gas	H2	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.53	0.32
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	280.	280.	280.	280.	250.
Heat rate (K/min)	4.	4.	4.	4.	5.
Initial hold (min)					30.
Final hold (min)
I	1050.	1044.	1045.	1050.	1060.
Reference	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	OV-101	OV-101	HP-1
Column length (m)	30.	60.	10.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	60.	60.	35.	50.	70.
T_end (C)	240.	220.	225.	200.	220.
Heat rate (K/min)	3.	4.	6.	5.	3.
Initial hold (min)			5.
Final hold (min)					15.
I	1048.	1037.	1049.	1039.	1035.
Reference	Zoghbi, Andrade, et al., 2003	Baher, Mirza, et al., 2002	Bloss, Acree, et al., 2002	Boyom, Keumedjio, et al., 2002	Cavaleiro, Salgueiro, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	BP-1	DB-5	DB-1	SE-30
Column length (m)	30.	25.	30.	30.	50.
Carrier gas	He	N2	He	H2	He
Substrate
Column diameter (mm)	0.25	0.50	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	75.	60.	60.	40.	70.
T_end (C)	200.	220.	240.	245.	240.
Heat rate (K/min)	3.	5.	3.	3.	4.
Initial hold (min)	4.			20.
Final hold (min)	8.	10.
I	1050.	1040.	1051.	1032.	1037.
Reference	Cicció and Gómez-Laurito, 2002	Das, Ram, et al., 2002	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002	Iñigo, Palá-Paúl, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RSL-200	RSL-200	CP Sil 8 CB	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		H2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	40.	50.	50.	35.
T_end (C)	200.	280.	280.	220.	280.
Heat rate (K/min)	3.	6.	6.	3.	4.
Initial hold (min)		5.	5.	2.	2.
Final hold (min)		5.	5.		15.
I	1049.	1038.	1037.	1047.	1051.
Reference	Isidorov and Jdanova, 2002	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	DB-5	DB-5MS	DB-1
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	200.	290.	240.	240.	250.
Heat rate (K/min)	5.	7.	3.	3.	4.
Initial hold (min)					10.
Final hold (min)
I	1039.	1049.	1049.	1046.	1047.
Reference	Kuiate, Bessière, et al., 2002	Lin, Rouseff, et al., 2002	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	HP-1	DB-5	DB-1	DB-1
Column length (m)	50.	50.	25.	60.	50.
Carrier gas	He	N2	He	He	N2
Substrate
Column diameter (mm)	0.2	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.5	0.25		0.25	0.25
T_start (C)	50.	90.	60.	40.	60.
T_end (C)	250.	220.	220.	280.	240.
Heat rate (K/min)	2.	3.	3.	4.	3.
Initial hold (min)				5.
Final hold (min)
I	1037.	1046.	1045.	1037.	1017.
Reference	Orav, Kailas, et al., 2002	Priestap, van Baren, et al., 2002	Schwob, Bessière, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	SPB-5	DB-5MS	DB-5MS
Column length (m)	30.	30.	60.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	40.	35.	35.
T_end (C)	270.	240.	220.	250.	250.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			5.	5.	5.
Final hold (min)			15.
I	1046.	1051.	1051.	1050.	1051.
Reference	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Cornu, Carnat, et al., 2001	Fernando and Grün, 2001	Fernando and Grün, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	BP-1	RSL-200	BP-1
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	N2	N2	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	220.	220.	220.	280.	230.
Heat rate (K/min)	5.	5.	5.	6.	2.
Initial hold (min)	10.	10.		5.
Final hold (min)				5.	35.
I	1051.	1052.	1042.	1040.	1035.
Reference	Flamini, Cioni, et al., 2001	Gallori, Flamini, et al., 2001	Gupta, Mallavarapu, et al., 2001	Jirovetz L., Buchbauer G., et al., 2001	Lota, de Rocca Serra, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-1	OV-101	OV-101	DB-1
Column length (m)	30.	60.	50.	50.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.5		0.25
T_start (C)	60.	50.	50.	50.	80.
T_end (C)	240.	270.	250.	250.	225.
Heat rate (K/min)	3.	4.	2.	2.	4.
Initial hold (min)
Final hold (min)	30.
I	1058.	1036.	1038.	1039.	1027.
Reference	Marongiu, Porcedda, et al., 2001	Mirza, Ahmadi, et al., 2001	Orav, Kailas, et al., 2001	Orav and Kann, 2001	Palá-Paúl, Pérez-Alonso, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	DB-5	SPB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		H2	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.25	0.32
Phase thickness (μm)	0.5	0.25		0.25	0.25
T_start (C)	35.	60.	60.	60.	50.
T_end (C)	275.	285.	240.	240.	250.
Heat rate (K/min)	6.	3.	3.	3.	2.
Initial hold (min)
Final hold (min)
I	1050.	1044.	1050.5	1050.	1045.
Reference	Rouseff, Jella, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Santos, Moreira, et al., 2001	Tellez M., Estell R., et al., 2001	Vijayanand, Rao, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	RSL-200	DB-5	DB-1	DB-5
Column length (m)	30.	60.	30.	25.	30.
Carrier gas	He	H2	He	Nitrogen	N2
Substrate
Column diameter (mm)	0.2	0.32	0.25	0.50	0.22
Phase thickness (μm)	0.2	0.25	0.25	0.25	0.25
T_start (C)	80.	40.	60.	60.	70.
T_end (C)	300.	250.	240.	220.	230.
Heat rate (K/min)	5.	6.	3.	5.	4.
Initial hold (min)	3.				2.
Final hold (min)					20.
I	1052.	1040.	1048.	1040.	1047.
Reference	Fraternale, Giamperi, et al., 2000	Jirovetz, Puschmann, et al., 2000	Maia, Zoghbi, et al., 2000	Mallavarapu, Rao, et al., 2000	Mitiku, Sawamura, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5	DB-1	OV-101	SE-30
Column length (m)	25.	30.	30.	50.	25.
Carrier gas	N2	He	He	Nitrogen	He
Substrate
Column diameter (mm)	0.33	0.25	0.25	0.25	0.2
Phase thickness (μm)	1.0	0.25	0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	275.	275.	260.	200.	230.
Heat rate (K/min)	4.	4.	2.	2.	3.
Initial hold (min)			5.	10.
Final hold (min)			2.
I	1048.	1048.	1034.	1038.	1052.
Reference	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2	Senatore, Napolitano, et al., 2000	Tamura, Boonbumrung, et al., 2000	Ali N.A.M. and Jantan, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	OV-1	OV-1	OV-101	RTX-1
Column length (m)	25.	25.	25.	52.	30.
Carrier gas	Hydrogen	Hydrogen	Hydrogen	Helium	N2
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.26	0.25
Phase thickness (μm)	0.30	0.30	0.30	0.13	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	200.	200.	200.	220.	300.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)	1.	1.	1.	0.
Final hold (min)	10.	10.	10.	0.
I	1034.	1034.	1034.	1026.	1042.
Reference	Bicchi, Binello, et al., 1999	Bicchi, Binello, et al., 1999	Bicchi, Binello, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CBP-1	HP-1	SE-30	OV-1
Column length (m)	25.	25.	25.	25.	25.
Carrier gas		He	H2	He	H2
Substrate
Column diameter (mm)	0.32	0.3	0.32	0.2	0.25
Phase thickness (μm)			0.17		0.25
T_start (C)	50.	60.	40.	60.	40.
T_end (C)	200.	240.	260.	230.	220.
Heat rate (K/min)	5.	4.	3.	3.	3.
Initial hold (min)			5.	10.	5.
Final hold (min)					5.
I	1039.	1040.	1038.	1052.	1039.
Reference	Kuiate, Zollo, et al., 1999	Labuckas, Zygadlo, et al., 1999	Lopes, Koketsu, et al., 1999	Mohd and Jantan, 1999	Oberhofer, Nikiforov, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	DB-1	OV-101	DB-5	SE-30
Column length (m)	25.	50.	50.	30.	30.
Carrier gas	H2	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.20
T_start (C)	40.	70.	70.	40.	60.
T_end (C)	220.	240.	220.	250.	200.
Heat rate (K/min)	3.	4.	2.	2.	3.
Initial hold (min)	5.		5.	5.	4.
Final hold (min)	5.			60.
I	1044.	1027.	1035.	1046.	1047.
Reference	Oberhofer, Nikiforov, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Pateira, Nogueira, et al., 1999	Porta, Porcedda, et al., 1999	Prikhod'ko, Klyuev, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	Ultra-2	BP-1	DB-1	DB-5
Column length (m)	30.	25.	25.	60.	30.
Carrier gas	Helium		N2	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.5	0.25	0.25
Phase thickness (μm)	0.20			0.25	0.25
T_start (C)	60.	40.	60.	40.	40.
T_end (C)	200.	300.	220.	280.	220.
Heat rate (K/min)	3.	5.	5.	4.	4.
Initial hold (min)	4.	4.		5.	5.
Final hold (min)			10.
I	1092.	1046.	1044.	1038.	1047.
Reference	Prikhod'ko, Klyuev, et al., 1999	Quiroz, Fuentes-Contreras, et al., 1999	Rao, Bhattacharya, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	OV-101	DB-5	DB-5MS
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	He	He	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	220.	240.	220.	240.	240.
Heat rate (K/min)	4.	3.	4.	3.	3.
Initial hold (min)			0.
Final hold (min)			0.
I	1047.	1051.	1025.	1047.	1048.
Reference	Sefidkon and Mirza, 1999	Tellez, Canel, et al., 1999	Tropnikova, Zenkevich, et al., 1999	Zoghbi, Andrade, et al., 1999	Zoghbi, Andrade, et al., 1999, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	OV-1	DB-5	HP-5	HP-1
Column length (m)	50.	50.	30.	25.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	50.	60.	70.	50.
T_end (C)	240.	250.	240.	290.	280.
Heat rate (K/min)	3.	10.	3.	3.	4.
Initial hold (min)		5.		8.	5.
Final hold (min)	20.	20.		20.
I	1043.	1041.	1048.	1050.	1046.
Reference	Doneanu and Anitescu, 1998	Kökdil, Kurucu, et al., 1998	Maia, Zohhbi, et al., 1998	Poiana, Sicari, et al., 1998	Stashenko, Cervantes, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-1	SPB-Sulfur	SPB-Sulfur	DB-1
Column length (m)	25.	30.	30.	30.
Carrier gas		He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32
Phase thickness (μm)		0.25	4.	4.
T_start (C)	50.	40.	45.	45.	80.
T_end (C)	200.	270.	240.	240.	220.
Heat rate (K/min)	5.	2.	5.	5.	6.
Initial hold (min)		4.	13.	13.
Final hold (min)			5.	5.
I	1042.	1056.	1040.	1042.	1027.
Reference	Zollo, Biyiti, et al., 1998	Kökdil, Kurucu, et al., 1997	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-1	OV-101	DB-5
Column length (m)	30.	30.	23.	50.	30.
Carrier gas	Helium	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25		0.17	0.17	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	240.	250.	220.	300.
Heat rate (K/min)	3.	4.	5.	5.	4.
Initial hold (min)			3.		2.
Final hold (min)			30.		5.
I	1050.	1050.	1038.	1041.	1045.0
Reference	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996	Gawdzik, Mardarowicz, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	BP-1	BP-1	BP-1	DB-1
Column length (m)	50.	25.	25.	25.	60.
Carrier gas	He	N2	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.50	0.50	0.50	0.32
Phase thickness (μm)					0.50
T_start (C)	50.	60.	60.	60.	50.
T_end (C)	250.	220.	220.	220.	250.
Heat rate (K/min)	2.	5.	5.	5.	8.
Initial hold (min)					1.
Final hold (min)					6.
I	1037.	1042.	1044.	1046.	1042.
Reference	Orav, Kailas, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Sagrero-Nieves and Bartley, 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-1	OV-101	DB-1	DB-1
Column length (m)	60.	50.	52.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.33		0.25	0.25
T_start (C)	50.	40.	50.	50.	70.
T_end (C)	250.	200.	220.	250.	270.
Heat rate (K/min)	2.5	3.	3.	3.5	2.5
Initial hold (min)	5.	3.		5.	5.
Final hold (min)		30.
I	1047.	1040.	1039.	1037.	1035.
Reference	Stashenko, Puertas, et al., 1996	Wong and Lai, 1996	Dzumayev, Tsibulskaya, et al., 1995	Stashenko, Torres, et al., 1995	Tirado, Stashenko, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-101	Methyl Silicone	Methyl Silicone	Methyl Silicone
Column length (m)	60.	50.	50.	50.	25.
Carrier gas	He	H2	N2	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.50
Phase thickness (μm)	0.25	0.3	0.17	0.17
T_start (C)	70.	65.	80.	80.	60.
T_end (C)	270.	300.	200.	200.	220.
Heat rate (K/min)	2.5	2.	2.	3.	5.
Initial hold (min)	5.	5.
Final hold (min)
I	1035.	1035.	1038.	1045.	1042.
Reference	Tirado, Stashenko, et al., 1995	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Mallavarapu, Ramesh, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	BP-1	DB-1	BP-1	SE-30
Column length (m)	30.	25.	60.	50.	40.
Carrier gas	Hydrogen			H2	He
Substrate
Column diameter (mm)	0.25	0.33	0.32	0.30	0.50
Phase thickness (μm)	0.25				0.75
T_start (C)	60.	45.	50.	40.	30.
T_end (C)	250.	180.	250.	250.	220.
Heat rate (K/min)	2.	3.	4.	10.	3.
Initial hold (min)	5.	3.	0.1	1.
Final hold (min)	2.		5.
I	1050.	1039.	1037.	1040.	1037.
Reference	Kollmannsberger, Nitz, et al., 1992	Wyllie, Brophy, et al., 1990	Binder and Flath, 1989	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	OV-1	OV-1	OV-3
Column length (m)	60.	60.	50.	60.	150.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.20	0.50	0.66
Phase thickness (μm)			0.20	1.2
T_start (C)	30.	30.	30.	40.	30.
T_end (C)	210.	210.	220.	220.	170.
Heat rate (K/min)	2.	2.	2.	2.	1.
Initial hold (min)	4.	4.
Final hold (min)
I	1037.	1041.	1037.	1037.	1050.
Reference	Takeoka and Butter, 1989	Takeoka and Butter, 1989	de Pooter, Nicolai, et al., 1988	Wahab, Aboutabl, et al., 1987	Buttery, Flath, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	OV-1	OV-101
Column length (m)	50.	50.	50.	40.	30.
Carrier gas				He	He
Substrate
Column diameter (mm)	0.30	0.30	0.30	0.5	0.5
Phase thickness (μm)				0.75	0.8
T_start (C)	40.	40.	40.	30.	40.
T_end (C)	230.	230.	230.	220.	220.
Heat rate (K/min)	3.5	3.5	3.5	3.	2.
Initial hold (min)	5.	5.	5.
Final hold (min)
I	1040.	1041.	1051.	1037.	1038.
Reference	Nykanen, 1986	Nykanen, 1986	Nykanen, 1986	de Pooter, de Buyck, et al., 1986	De Pooter and Schamp, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-3	DB-1
Column length (m)	30.	30.	150.	60.
Carrier gas	He	He
Substrate
Column diameter (mm)	0.5	0.5	0.66	0.32
Phase thickness (μm)	0.8	0.8
T_start (C)	40.	40.	20.	50.
T_end (C)	220.	220.	170.	250.
Heat rate (K/min)	2.	2.	1.	4.
Initial hold (min)				0.1
Final hold (min)				5.
I	1037.	1038.	1050.	1036.
Reference	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	Buttery, Xu, et al., 1985	Flath, Mon, et al., 1983
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Gilani, Shah, et al., 2009
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Ho, Wang, et al., 2009
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Maia, Zoghbi, et al., 2000
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Ali N.A.M. and Jantan, 1999
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Kalemba, 1999
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Mohd and Jantan, 1999
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Sefidkon and Khajavi, 1999
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Ayedoun, Adeoti, et al., 1996
Ayedoun, A.M.; Adeoti, B.S.; Sossou, P.V.; Leclerq, P.A., Influence of fruit conservation methods on the essential oil composition of xylopia aethiopica (Dunal) A. Richard from Benin, Flavour Fragr. J., 1996, 11, 4, 245-250, https://doi.org/10.1002/(SICI)1099-1026(199607)11:4<245::AID-FFJ583>3.0.CO;2-K . [all data]

Chacko, Jayalekshmy, et al., 1996
Chacko, S.; Jayalekshmy, A.; Gopalakrishnan, M.; Narayanan, C.S., Roasting studies on black pepper (Piper nigrum L.), Flavour Fragr. J., 1996, 11, 5, 305-310, https://doi.org/10.1002/(SICI)1099-1026(199609)11:5<305::AID-FFJ588>3.0.CO;2-1 . [all data]

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Rajeswara, Kaul, et al., 1996
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Sagrero-Nieves and Bartley, 1996
Sagrero-Nieves, L.; Bartley, J.P., Volatile components from the leaves of heterotheca inuloides Cass., Flavour Fragr. J., 1996, 11, 1, 49-51, https://doi.org/10.1002/(SICI)1099-1026(199601)11:1<49::AID-FFJ538>3.0.CO;2-J . [all data]

Stashenko, Puertas, et al., 1996
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Wong and Lai, 1996
Wong, K.C.; Lai, F.Y., Volatile constituents from the fruits of four Syzygium species grown in Malaysia, Flavour Fragr. J., 1996, 11, 1, 61-66, https://doi.org/10.1002/(SICI)1099-1026(199601)11:1<61::AID-FFJ539>3.0.CO;2-1 . [all data]

Dzumayev, Tsibulskaya, et al., 1995
Dzumayev, Kh.K.; Tsibulskaya, I.A.; Zenkevich, I.G.; Tkachenko, K.G.; Satzyperova, I.F., Essential Oils od Salvia Sclarea L. Produced from Plants Grown in Southern Uzbekistan, J. Essent. Oil Res., 1995, 7, 6, 597-604, https://doi.org/10.1080/10412905.1995.9700513 . [all data]

Stashenko, Torres, et al., 1995
Stashenko, E.E.; Torres, W.; Morales, J.R.M., A study of the compositional variation of the essential oil of ylang-ylang (Cananga odorata Hook Fil. et Thomson, forma genuina) during flower development, J. Hi. Res. Chromatogr., 1995, 18, 2, 101-104, https://doi.org/10.1002/jhrc.1240180206 . [all data]

Tirado, Stashenko, et al., 1995
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Demarne and van der Walt, 1993
Demarne, F.-E.; van der Walt, J.J.A., Composition of the Essential Oil of Pelargonium citronellum (Geraniaceae), J. Essent. Oil Res., 1993, 5, 3, 233-238, https://doi.org/10.1080/10412905.1993.9698214 . [all data]

Gopalakrishnan, Menon, et al., 1993
Gopalakrishnan, M.; Menon, N.; Padmakumari, K.P.; Jayalekshmy, A.; Narayanan, C.S., GC Analysis and Odor Profiles of Four New Indian Genotypes of Piper nigrum L., J. Essent. Oil Res., 1993, 5, 3, 247-253, https://doi.org/10.1080/10412905.1993.9698217 . [all data]

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Binder and Flath, 1989
Binder, R.G.; Flath, R.A., Volatile components of pineapple guava, J. Agric. Food Chem., 1989, 37, 3, 734-736, https://doi.org/10.1021/jf00087a034 . [all data]

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Takeoka and Butter, 1989
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de Pooter, Nicolai, et al., 1988
de Pooter, H.L.; Nicolai, B.; De Laet, J.; De Buyck, L.F.; Schamp, N.M.; Goetghebeur, P., The Essential Oils of Five Nepeta Species. A Preliminary Evaluation of their Use in Chemotaxonomy by Cluster Analysis, Flavour Fragr. J., 1988, 3, 4, 155-159, https://doi.org/10.1002/ffj.2730030404 . [all data]

Wahab, Aboutabl, et al., 1987
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Buttery, Flath, et al., 1986
Buttery, R.G.; Flath, R.A.; Mon, T.R.; Ling, L.C., Identification of germacrene D in walnut and fig leaf volatiles, J. Agric. Food Chem., 1986, 34, 5, 820-822, https://doi.org/10.1021/jf00071a013 . [all data]

Nykanen, 1986
Nykanen, I., High Resolution Gas Chromatographic - Mass Spectrometric determination of the Flavour Composition of Wild Majoram (Origanum vulgare L.) Cultivated in Finland, Z. Lebensm Unters Forsch, 1986, 183, 4, 267-272, https://doi.org/10.1007/BF01087742 . [all data]

de Pooter, de Buyck, et al., 1986
de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Aboutabl, E.; De Bruyn, A.; Husain, S.Z., The Volatile Fraction of Senecio glaucus subsp. coronopifolius, Flavour Fragr. J., 1986, 1, 4-5, 159-163, https://doi.org/10.1002/ffj.2730010406 . [all data]

De Pooter and Schamp, 1986
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Buttery, Xu, et al., 1985
Buttery, R.G.; Xu, C.; Ling, L.C., Volatile components of wheat leaves (and stems): Possible insect attractants, J. Agric. Food Chem., 1985, 33, 1, 115-117, https://doi.org/10.1021/jf00061a033 . [all data]

Flath, Mon, et al., 1983
Flath, R.A.; Mon, T.R.; Lorenz, G.; Whitten, C.J.; Mackley, J.W., Volatile components of Acacia sp. blossoms, J. Agric. Food Chem., 1983, 31, 6, 1167-1170, https://doi.org/10.1021/jf00120a008 . [all data]

Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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