Dimethyl trisulfide


Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TR-5 MSHP-5 MSPolydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsHP-5 MS
Column length (m) 15.30.  30.
Carrier gas HeliumHelium  Helium
Substrate      
Column diameter (mm) 0.250.25  0.32
Phase thickness (μm) 0.250.25  0.25
Program 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)not specifiednot specifiednot specifiednot specified
I 957.976.976.982.970.
ReferenceKurashov, Mitrukova, et al., 2014Kotowska, Zalikowski, et al., 2012Robinson, Adams, et al., 2012Robinson, Adams, et al., 2012Pino, Marquez, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54HP-5HP-1SE-54Nonpolar
Column length (m) 30.60.50.  
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.320.250.20  
Phase thickness (μm) 0.250.250.33  
Program 35 0C (2 min) 10 0C/min -> 50 0C (2 min) 6 0C/min -> 250 0C30 0C (2 min) 2 0Cmin -> 60 0C 10 0C/min -> 100 0C 20 0C/min -> 140 0C 10 0C/min -> 200 0C (10 min)not specifiednot specifiednot specified
I 969.974.938.961.974.
ReferenceChristlbauer and Schieberle, 2009Rotsatschakul, Visesanguan, et al., 2009Breme, Langle, et al., 2008Frauendorfer and Schieberle, 2008Staples and Zeiger, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSSPB-1HP-5CP-Sil5 CB MSDB-1
Column length (m) 60.30. 50.20.
Carrier gas HeliumHeliumHeN2 
Substrate      
Column diameter (mm) 0.320.32 0.320.18
Phase thickness (μm) 1.00.25 1.20.18
Program 40 0C (2 min) 6 0C/min -> 100 0C 4 0C/min -> 180 0C 8 0C/min -> 250 0C (12 min)not specified50C => 3C/min => 200C(10min) => 10C/min => 290C(10min)36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)not specified
I 970.949.953.957.943.
ReferenceLiu, Xu, et al., 2007Rao, Nagender, et al., 2007Splivallo, Bossi, et al., 2007Callemien, Dasnoy, et al., 2006Chantreau, Rochat, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSCP-Sil 5 CBCP-Sil 5 CBHP-5
Column length (m) 20.30.50.50.60.
Carrier gas   NitrogenNitrogen 
Substrate      
Column diameter (mm) 0.180.250.320.320.32
Phase thickness (μm) 0.180.251.21.201.
Program not specified40 0C (3 min) 2 0C/min -> 150 0C 20 0C/min -> 220 0C (5 min)36 0C 20 0C/min -> 85 0C 1 iC/min -> 145 0C 3 0C/min -> 250 0C36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0Cnot specified
I 943.955.957.957.973.
ReferenceChantreau, Rochat, et al., 2006Pyun and Shin, 2006Callamien, Dasnoy, et al., 2005Callemien, Dasnoy, et al., 2005Thierry, Maillard, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5BPX-5SPB-5RTX-5 MS
Column length (m) 50.50.60.60.60.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 1.21.051.1.0.5
Program 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)40C(10min) => 5C/min => 200C => 20C/min => 250C(5min)40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min)not specified35C (3min) => 10C/min => 50C => 4C/min => 200C => 50C/min => 250C (10min)
I 949.982.984.978.977.
ReferenceCounet, Ouwerx, et al., 2004Garcia-Estaban, Ansorena, et al., 2004Machiels, Istasse, et al., 2004Begnaud, Pérès, et al., 2003Machiels and Istasse, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5DB-5CP Sil 5 CBCP-Sil 5 CB
Column length (m) 60.60.30.50.50.
Carrier gas HeHe  Helium
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 1.1.1.1.21.20
Program 40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min)40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min)35C(4min) => 2C/min => 130C => 4C/min => 250C36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min)36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0C (30 min)
I 977.977.950.969.959.
ReferenceMachiels, van Ruth, et al., 2003Machiels, van Ruth, et al., 2003Qian and Reineccius, 2003Counet, Callemien, et al., 2002Gijs, Chevanese, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBCP Sil 5 CBCP Sil 5 CBDB-5 MS
Column length (m) 60.60.50.50.30.
Carrier gas He   Helium
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (μm) 0.250.251.21.21.0
Program 40C(2min) => 40C/min => 60C(2min) => 6C/min => 250C(15min)not specified36C => 20C/min => 120C(20min) => 2C/min => 250C(30min)36C => 20C/min => 120C(20min) => 2C/min => 250C(30min)not specified
I 986.987.961.959.988.
ReferenceLandy, Boucon, et al., 2002Duckham, Dodson, et al., 2001Lermusieau, Bulens, et al., 2001Lermusieau, Bulens, et al., 2001Luo and Agnew, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54CP Sil 5 CBCP-Sil5 CB MSRTX-5RTX-5
Column length (m)  50.50.  
Carrier gas  He   
Substrate      
Column diameter (mm)  0.320.32  
Phase thickness (μm)  1.20.4  
Program 35C (2min) => 40C/min => 50C (2min) => 6C/min => 180C => 10C/min => 240C33C (16.5min) => 2C/min => 160C => 20C/min => 200C (9min)0C (3min) => 3C/min => 50C => 5C/min => 220C (30min)not specifiednot specified
I 969.952.949.967.967.
ReferenceSchieberle and Steinhaus, 2001Gijs, Piraprez, et al., 2000Tirillini, Verdelli, et al., 2000Masanetz, Guth, et al., 1998Masanetz, Guth, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54SE-54SE-54SE-54
Column length (m) 30.25.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Program 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230C35C(2min) => 50C/min => 60C(2min) => 4C/min => 230C35C (1min) => 40C/min => 60C (1min) => 6C/min => 250C (10min)35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
I 963.968.970.969.969.
ReferenceMatsui, Guth, et al., 1998Zehentbauer and Grosch, 1998Guth, 1997Schermann and Schieberle, 1997Schermann and Schieberle, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5DB-5Methyl SiliconeSE-54
Column length (m) 30.50.50.  
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.320.32  
Phase thickness (μm) 0.250.250.25  
Program 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C40C (10min) => 3C/min => 95C => 10C/min => 270C (10min)40C (10min) => 3C/min => 95C => 10C/min => 270C (10min)not specified0C (2min) => 6C/min => 50C (2min) => 6C/min => 230 C (10min)
I 969.985.981.949.970.
ReferenceSchermann and Schieberle, 1997Mateo and Zumalacárregui, 1996Mateo and Zumalacárregui, 1996Misharina, 1995Guth and Grosch, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-54methyl silicone oil with 5% Igepalmethyl silicone oil with 5% IgepalOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.
Column length (m) 60.30.150.150.50.
Carrier gas  He  Hydrogen
Substrate      
Column diameter (mm) 0.320.320.750.750.32
Phase thickness (μm)  0.3   
Program not specified35C(2min) => 40C/min => 50C(2min) => 6C/min => 230C(10min)not specifiednot specifiednot specified
I 941.974.940.949.948.
ReferenceButtery, Teranishi, et al., 1990Blank, Fischer, et al., 1989Schultz, Flath, et al., 1988Schultz, Flath, et al., 1988Waggott and Davies, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kurashov, Mitrukova, et al., 2014
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Pino, Marquez, et al., 2010
Pino, J.A.; Marquez, E.; Quijano, C.E.; Castro, D., Volatile compounds in noni (Morinda citrifolia L.) at two ripening stages, Ciencia e Technologia de Alimentos, 2010, 30, 1, 183-187, https://doi.org/10.1590/S0101-20612010000100028 . [all data]

Christlbauer and Schieberle, 2009
Christlbauer, M.; Schieberle, P., Characterization of the key aroma compounds in beef and pork vegetable gravies a la chef by application of the aroma extract dilution analysis, J. Agric. Food Chem., 2009, 57, 19, 9114-9112, https://doi.org/10.1021/jf9023189 . [all data]

Rotsatschakul, Visesanguan, et al., 2009
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Breme, Langle, et al., 2008
Breme, K.; Langle, S.; Fernandez, X.; Meierhenrich, U.J.; Brevard, H.; Joulain, D., Character impact odorants from Brassicaceae by aroma extracts dilution analysis (AEDA): Brassica cretica and Brassica insularis, Flavour Fragr. J., 2008, 24, 2, 88-93, https://doi.org/10.1002/ffj.1912 . [all data]

Frauendorfer and Schieberle, 2008
Frauendorfer, F.; Schieberle, P., Changes in key aroma compounds of criollo cocoa beans during roasting, J. Agric. Food Chem., 2008, 56, 21, 10244-10251, https://doi.org/10.1021/jf802098f . [all data]

Staples and Zeiger, 2008
Staples, E.; Zeiger, K., On-Site Measurements of VOCs and Odors from Metal Casting Operations Using an Ultra-Fast Gas Chromatograph, 2008, retrieved from http://www.estcal.com/TechPapers/Industrial/FoundryOdors.doc. [all data]

Liu, Xu, et al., 2007
Liu, Y.; Xu, X.-L.; Zhou, G.-H., Comparative study of volatile compounds in traditional Chinese Nanjing marinated duck by different extraction techniques, Int. J. Food Sci. Technol., 2007, 42, 5, 543-550, https://doi.org/10.1111/j.1365-2621.2006.01264.x . [all data]

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Chantreau, Rochat, et al., 2006
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Pyun and Shin, 2006
Pyun, M.-S.; Shin, S., Antifungal effects of the volatile oils from Allium plants against Trichophyton species and synergism of the oils with ketoconazole, Phytomedicine, 2006, 13, 6, 394-400, https://doi.org/10.1016/j.phymed.2005.03.011 . [all data]

Callamien, Dasnoy, et al., 2005
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Callemien, Dasnoy, et al., 2005
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Thierry, Maillard, et al., 2005
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Counet, Ouwerx, et al., 2004
Counet, C.; Ouwerx, C.; Rosoux, D.; Collin, S., Relationship between procyanidin and flavor contents of cocoa liquors from different origins, J. Agric. Food Chem., 2004, 52, 20, 6243-6249, https://doi.org/10.1021/jf040105b . [all data]

Garcia-Estaban, Ansorena, et al., 2004
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Machiels, Istasse, et al., 2004
Machiels, D.; Istasse, L.; van Ruth, S.M., Gas chromatography-olfactometry analysis of beef meat originating from differently fed Belgian Blue, Limousin and Aberdeen Angus bulls, Food Chem., 2004, 86, 3, 377-383, https://doi.org/10.1016/j.foodchem.2003.09.011 . [all data]

Begnaud, Pérès, et al., 2003
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Machiels and Istasse, 2003
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Machiels, van Ruth, et al., 2003
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Counet, Callemien, et al., 2002
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Gijs, Chevanese, et al., 2002
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Landy, Boucon, et al., 2002
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Duckham, Dodson, et al., 2001
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Lermusieau, Bulens, et al., 2001
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Schieberle and Steinhaus, 2001
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Gijs, Piraprez, et al., 2000
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Tirillini, Verdelli, et al., 2000
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Masanetz, Guth, et al., 1998
Masanetz, C.; Guth, H.; Grosch, W., Fishy and hay-like off-flavours of dry spinach, Z. Lebensm. Unters. Forsch. A, 1998, 206, 2, 108-113, https://doi.org/10.1007/s002170050224 . [all data]

Matsui, Guth, et al., 1998
Matsui, T.; Guth, H.; Grosch, W., A comparative study of potent odorants in peanut, hazelnut, and pumpkin seed oils on the basis of aroma extract dilution analysis (AEDA) and gas chromatography-olfactometry of headspace samples (GCOH), Lipid - Fett, 1998, 100, 2, 51-56, https://doi.org/10.1002/(SICI)1521-4133(199802)100:2<51::AID-LIPI51>3.0.CO;2-W . [all data]

Zehentbauer and Grosch, 1998
Zehentbauer, G.; Grosch, W., Crust aroma of baguettes. I. Key odorants of baguettes prepared in two different ways, J. Cereal Science, 1998, 28, 1, 81-92, https://doi.org/10.1006/jcrs.1998.0184 . [all data]

Guth, 1997
Guth, H., Identification of character impact odorants of different white wine varieties, J. Agric. Food Chem., 1997, 45, 8, 3022-3026, https://doi.org/10.1021/jf9608433 . [all data]

Schermann and Schieberle, 1997
Schermann, P.; Schieberle, P., Evaluation of key odorants in milk chocolate and cocoa mass by aroma extract dilution analyses, J. Agric. Food Chem., 1997, 45, 3, 867-872, https://doi.org/10.1021/jf960670h . [all data]

Mateo and Zumalacárregui, 1996
Mateo, J.; Zumalacárregui, J.M., Volatile compounds in chorizo and their changes during ripening, Meat Sci., 1996, 44, 4, 255-273, https://doi.org/10.1016/S0309-1740(96)00028-9 . [all data]

Misharina, 1995
Misharina, T.A., Sorption regularities of sulfur- and oxygen-containing compounds in chromatography and their application in identification of volatile organic compounds, Diss. degree of Dr. Sci. (Chemistry), 1995, 52. [all data]

Guth and Grosch, 1994
Guth, H.; Grosch, W., Identification of the character impact odorants of stewed beef juice by instrumental analyses and sensory studies, J. Agric. Food Chem., 1994, 42, 12, 2862-2866, https://doi.org/10.1021/jf00048a039 . [all data]

Buttery, Teranishi, et al., 1990
Buttery, R.G.; Teranishi, R.; Flath, R.A.; Ling, L.C., Identification of additional tomato paste volatiles, J. Agric. Food Chem., 1990, 38, 3, 792-795, https://doi.org/10.1021/jf00093a042 . [all data]

Blank, Fischer, et al., 1989
Blank, I.; Fischer, K.-H.; Grosch, W., Intensive neutral odourants of linden honey, Z. Lebensm. Unters. Forsch., 1989, 189, 5, 426-433, https://doi.org/10.1007/BF01028316 . [all data]

Schultz, Flath, et al., 1988
Schultz, T.H.; Flath, R.A.; Stern, D.J.; Mon, T.R.; Teranishi, R.; McKenna Kruse, S.; Butlder, B.; Howard, W.E., Coyote estrous urine volatiles, J. Chem. Ecol., 1988, 14, 2, 701-712, https://doi.org/10.1007/BF01013917 . [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References