Dimethyl trisulfide


Van Den Dool and Kratz RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPFFAPFFAPFFAPDB-Wax
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.50.250.250.250.5
Tstart (C) 35.35.35.35.40.
Tend (C) 225.225.225.225.240.
Heat rate (K/min) 4.10.10.10.7.
Initial hold (min) 5.5.5.5. 
Final hold (min) 30.25.25.25.5.
I 1381.1373.1376.1387.1383.
ReferenceJarunrattanasri, Theerakulkait, et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Miracle E.R., et al., 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.50.50.50.250.5
Tstart (C) 40.40.40.50.40.
Tend (C) 250.250.240.230.240.
Heat rate (K/min) 4.4.7.10.5.
Initial hold (min) 5.5. 5. 
Final hold (min) 15.15.5.25.10.
I 1370.1377.1385.1378.1390.
ReferencePozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Ruiz Perez-Cacho, Mahattanatawee, et al., 2007Fernandez-Segovia, Escriche, et al., 2006Lopez-Galilea I., Fournier N., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBCP-Wax 52CBCP-Wax 52CBCP-Wax 52CBDB-Wax
Column length (m) 50.50.50.60.30.
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm)    0.250.25
Tstart (C) 60.60.60.35.40.
Tend (C) 220.220.220.203.200.
Heat rate (K/min) 4.4.4.3.10.
Initial hold (min) 5.5.5.4.3.
Final hold (min) 30.30.30. 20.
I 1373.1375.1361.1375.1362.
ReferenceMahadevan and Farmer, 2006Mahadevan and Farmer, 2006Mahadevan and Farmer, 2006Alasalvar, Taylor, et al., 2005Carunchia Whetstine, Croissant, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase StabilwaxCarbowax 20MDB-WaxDB-FFAPDB-Wax
Column length (m) 30.60.30.15.30.
Carrier gas N2He He 
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 40.45.40.35.40.
Tend (C) 230.250.200.225.200.
Heat rate (K/min) 4.2.10.10.10.
Initial hold (min) 2.0.173.5.5.
Final hold (min) 10. 20.15.15.
I 1404.1357.1362.1386.1365.
ReferenceFang and Qian, 2005Verzera, Campisi, et al., 2005Whetstine, Cadwallader, et al., 2005Avsar, Karagul-Yuceer, et al., 2004Avsar, Karagul-Yuceer, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPFFAPDB-WaxDB-WaxDB-Wax
Column length (m) 15.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 35.40.40.45.45.
Tend (C) 225.220.230.240.240.
Heat rate (K/min) 10.5.5.6.3.
Initial hold (min) 5.3.2.10.10.
Final hold (min) 15. 10.30.30.
I 1371.1369.1367.1376.1356.
ReferenceAvsar, Karagul-Yuceer, et al., 2004Calvo-Gómez, Morales-López, et al., 2004Mahajan, Goddik, et al., 2004Nielsen, Larsen, et al., 2004Nielsen and Poll, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPDB-WaxDB-WaxCarbowaxDB-Wax
Column length (m) 30.30.30.60.30.
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 35.40.35.50.35.
Tend (C) 200.240.240.200.200.
Heat rate (K/min) 10.6.6.2.10.
Initial hold (min) 5.10.2. 5.
Final hold (min) 30.30.6. 30.
I 1367.1376.1380.1380.1360.
ReferenceKaragül-Yüceer, Vlahovich, et al., 2003Nielsen, Larsen, et al., 2003Peterson and Reineccius, 2003Edris and Fadel, 2002Karagül-Yüceer, Cadwallader, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPDB-WaxDB-FFAPDB-FFAPEC-WAX
Column length (m) 30.30.15.15.30.
Carrier gas  He  He
Substrate      
Column diameter (mm) 0.250.530.320.320.32
Phase thickness (μm) 0.251.0.250.250.5
Tstart (C) 35.40.30.30.40.
Tend (C) 200.200.225.225.250.
Heat rate (K/min) 10.10.10.10.5.
Initial hold (min) 5.5.2.2.2.
Final hold (min) 30.30.20.20.10.
I 1352.1380.1359.1359.1390.
ReferenceKaragül-Yüceer, Cadwallader, et al., 2002Wu and Cadwallader, 2002Zhou, Wintersteen, et al., 2002Zhou, Wintersteen, et al., 2002le Guen, Prost, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxCP-Wax 52CBCP-Wax 52CB
Column length (m) 60.60.60.50.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 40.40.40.50.45.
Tend (C) 200.200.200.200.250.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 5.   0.17
Final hold (min) 30.    
I 1368.1381.1381.1370.1357.
ReferenceKim, 2001Lee, Suriyaphan, et al., 2001Lee, Suriyaphan, et al., 2001Liu, Yang, et al., 2001Verzera, Campisi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBDB-WaxDB-WaxDB-WaxCP-Wax 52CB
Column length (m) 50.60.60.60.50.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm)  0.50.50.5 
Tstart (C) 60.40.40.40.60.
Tend (C) 220.250.250.250.220.
Heat rate (K/min) 4.3.4.4.4.
Initial hold (min) 5.5.2.2.5.
Final hold (min) 30.10.10.10.30.
I 1356.1391.1394.1390.1359.
ReferenceChevance, Farmer, et al., 2000le Guen, Prost, et al., 2000Le Guen, Prost, et al., 2000Le Guen, Prost, et al., 2000Chevance and Farmer, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBCP-Wax 52CBCP-Wax 52CBSupelcowax-10DB-Wax
Column length (m) 50.50.50.60.30.
Carrier gas    He 
Substrate      
Column diameter (mm) 0.320.320.320.250.32
Phase thickness (μm)    0.250.25
Tstart (C) 60.40.40.35.40.
Tend (C) 220.220.220.195.200.
Heat rate (K/min) 4.4.4.2.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 30.30.30.90.30.
I 1376.1357.1373.1386.1366.
ReferenceChevance and Farmer, 1999Chevance and Farmer, 1999, 2Chevance and Farmer, 1999, 2Chung, 1999Cha and Cadwallader, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxFFAPDB-WaxDB-Wax
Column length (m) 60.30.30.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.530.53
Phase thickness (μm) 0.250.250.251.1.
Tstart (C) 40.40.20.20.20.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 3.6.4.4.4.
Initial hold (min) 5.5.1.5.5.
Final hold (min) 60.30.1.10.10.
I 1379.1365.1405.1403.1406.
ReferenceCha, Kim, et al., 1998Cha, Kim, et al., 1998Ott, Fay, et al., 1997Ott, Fay, et al., 1997Ott, Fay, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCP-Wax 52CBCP-Wax 52CBSupelcowax-10
Column length (m) 60.60.50.50.60.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.530.250.250.250.25
Phase thickness (μm) 1.0.25  0.25
Tstart (C) 20.50.60.60.40.
Tend (C) 200.230.200.200.195.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min) 5. 4.4.5.
Final hold (min) 10. 30.30.40.
I 1406.1387.1380.1380.1382.
ReferenceOtt, Fay, et al., 1997Shimoda, Peralta, et al., 1996Kim, Wu, et al., 1995Kim, Wu, et al., 1995Chung and Cadwallader, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBSupelcowax-10Supelcowax-10CP-Wax 52CBSupelcowax-10
Column length (m) 50.60.60.50.60.
Carrier gas H2  N2 
Substrate      
Column diameter (mm) 0.320.250.250.220.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 40.40.40.50.40.
Tend (C) 200.175.175.200.175.
Heat rate (K/min) 1.52.2.2.2.
Initial hold (min) 10.5.5. 5.
Final hold (min) 60.20.20. 20.
I 1329.1387.1388.1380.1389.
ReferenceYu, Wu, et al., 1993Tanchotikul and Hsieh, 1989Tanchotikul and Hsieh, 1989Yu, Wu, et al., 1989Vejaphan, Hsieh, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jarunrattanasri, Theerakulkait, et al., 2007
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Avsar, Karagul-Yuceer, et al., 2004
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le Guen, Prost, et al., 2001
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Lee, Suriyaphan, et al., 2001
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Verzera, Campisi, et al., 2001
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le Guen, Prost, et al., 2000
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Le Guen, Prost, et al., 2000
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Chevance and Farmer, 1999
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Chevance and Farmer, 1999, 2
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Chung, 1999
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Cha and Cadwallader, 1998
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Cha, Kim, et al., 1998
Cha, Y.J.; Kim, H.; Cadwallader, K.R., Aroma-active compounds in Kimchi during fermentation, J. Agric. Food Chem., 1998, 46, 5, 1944-1953, https://doi.org/10.1021/jf9706991 . [all data]

Ott, Fay, et al., 1997
Ott, A.; Fay, L.B.; Chaintreau, A., Determination and origin of the aroma impact compounds of yogurt flavor, J. Agric. Food Chem., 1997, 45, 3, 850-858, https://doi.org/10.1021/jf960508e . [all data]

Shimoda, Peralta, et al., 1996
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Kim, Wu, et al., 1995
Kim, S.M.; Wu, C.M.; Kubota, K.; Kobayashi, A., Effect of soybean oil on garlic volatile compounds isoalted by distillation, J. Agric. Food Chem., 1995, 43, 2, 449-452, https://doi.org/10.1021/jf00050a036 . [all data]

Chung and Cadwallader, 1993
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Notes

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