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2-Buten-1-one, 1-(2,6,6-trimethyl-1-cyclohexen-1-yl)-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-PetroDB-PetroHP-5ZB-5HP-5
Column length (m) 50.50.30.0.30.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.20.20.250.320.25
Phase thickness (mum) 0.50.50.250.50.25
Tstart (C) 50.50.50.40.60.
Tend (C) 270.270.250.265.280.
Heat rate (K/min) 2.2.4.7.4.
Initial hold (min)   5. 5.
Final hold (min)   15.5. 
I 1391.61393.1409.1403.1383.
ReferencePang T., Zhu S., et al., 2007Pang T., Zhu S., et al., 2007Mahattanatawee, Goodner, et al., 2005Gocmen, Gurbuz, et al., 2004Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-1
Column length (m) 37.30.30.
Carrier gas He  
Substrate    
Column diameter (mm) 0.320.250.25
Phase thickness (mum) 0.25  
Tstart (C) 100.50.50.
Tend (C) 250.300.300.
Heat rate (K/min) 8.2.2.
Initial hold (min)    
Final hold (min)    
I 1401.1366.61366.8
ReferenceMisharina, Samusenko, et al., 2002Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pang T., Zhu S., et al., 2007
Pang T.; Zhu S.; Lu X.; Xu G., Identification of unknown compounds on the basis of retention index data in comprehensive two-dimensional gas chromatography, J. Sep. Sci., 2007, 30, 6, 868-874, https://doi.org/10.1002/jssc.200600471 . [all data]

Mahattanatawee, Goodner, et al., 2005
Mahattanatawee, K.; Goodner, K.L.; Baldwin, E.A., Volatile constituents and character impact compounds of selected Florida's tropical fruit, Proc. Fla. State Hort. Soc., 2005, 118, 414-418. [all data]

Gocmen, Gurbuz, et al., 2004
Gocmen, D.; Gurbuz, O.; Rouseff, R.L.; Smoot, J.M.; Dagdelen, A.F., Gas chromatographic-olfactometric characterization of aroma active compounds in sun-dried and vacuum-dried tarhana, Eur. Food Res. Technol., 2004, 218, 6, 573-578, https://doi.org/10.1007/s00217-004-0913-6 . [all data]

Skaltsa, Demetzos, et al., 2003
Skaltsa, H.D.; Demetzos, C.; Lazari, D.; Sokovic, M., Essential oil analysis and antimicrobial activity of eight Stachys species from Greece, Phytochemistry, 2003, 64, 3, 743-752, https://doi.org/10.1016/S0031-9422(03)00386-8 . [all data]

Misharina, Samusenko, et al., 2002
Misharina, T.A.; Samusenko, A.L.; Belyaeva, N.V., Gas chromatographic and IR spectroscopic characteristics of tri- and tetramethylcyclohexenyl butenyl ketones, Russ. Chem. Bull. (Engl. Transl.), 2002, 51, 9, 1684-1688, https://doi.org/10.1023/A:1021347404479 . [all data]

Chang, Sheng, et al., 1989
Chang, L.P.; Sheng, L.S.; Yang, M.Z.; An, D.K., Retention index of essential oil in temperature-programmed capillary column gas chromatography, Acta Pharm. Sin., 1989, 24, 11, 847-852. [all data]


Notes

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