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2-Buten-1-one, 1-(2,6,6-trimethyl-1-cyclohexen-1-yl)-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase StabilwaxInnowaxHP-InnowaxDB-WaxDB-Wax
Column length (m) 30.60.60.30.60.
Carrier gas  HeHe  
Substrate      
Column diameter (mm) 0.320.250.250.530.25
Phase thickness (mum) 0.50.250.251.0.25
Tstart (C) 40.60.60.40.40.
Tend (C) 280.220.220.210.210.
Heat rate (K/min) 6.  5.5.
Initial hold (min) 5.10.10.  
Final hold (min) 5.    
I 1836.1830.1830.1824.1822.
ReferenceJirovetz, Buchbauer, et al., 2005Kaya, Baser, et al., 1999Kaya, Baser, et al., 1999, 2Kumazawa and Masuda, 1999Kumazawa and Masuda, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase HP-Innowax FSCCarbowax 20M
Column length (m) 60.40.
Carrier gas He 
Substrate   
Column diameter (mm) 0.250.4
Phase thickness (mum) 0.25 
Tstart (C) 60.50.
Tend (C) 220.170.
Heat rate (K/min) 4.4.
Initial hold (min) 10.10.
Final hold (min) 10. 
I 1830.1815.
ReferenceTümen, Baser, et al., 1998Kanasawud and Crouzet, 1990
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jirovetz, Buchbauer, et al., 2005
Jirovetz, L.; Buchbauer, G.; Stoyanova, A.; Balinova, A.; Guangjiun, Z.; Xihan, M., Solid phase microextraction/gas chromatographic and olfactory analysis of the scent and fixative properties of the essential oil of Rosa damascena L. from China, Flavour Fragr. J., 2005, 20, 1, 7-12, https://doi.org/10.1002/ffj.1375 . [all data]

Kaya, Baser, et al., 1999
Kaya, A.; Baser, K.H.C.; Demirci, B.; Koca, F., The essential oil of Acinos alpinus (L.) Moench growing in Turkey, Flavour Fragr. J., 1999, 14, 1, 55-59, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<55::AID-FFJ784>3.0.CO;2-Q . [all data]

Kaya, Baser, et al., 1999, 2
Kaya, A.; Baser, K.H.C.; Tümen, G.; Koca, F., The essential oil of Acinos suaveolens (Sm.) G. Don fil. Acinos arvensis (Lam.) Dandy and Acinos rotundifolius Pers. growing wild in Turkey, Flavour Fragr. J., 1999, 14, 1, 60-64, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<60::AID-FFJ785>3.0.CO;2-0 . [all data]

Kumazawa and Masuda, 1999
Kumazawa, K.; Masuda, H., Identification of potent odorants in Japanese green tea (Sen-cha), J. Agric. Food Chem., 1999, 47, 12, 5169-5172, https://doi.org/10.1021/jf9906782 . [all data]

Tümen, Baser, et al., 1998
Tümen, G.; Baser, K.H.C.; Demirci, B.; Ermin, N., The essential oils of Satureja coerulea Janka and Thymus aznavourii Velen., Flavour Fragr. J., 1998, 13, 1, 65-67, https://doi.org/10.1002/(SICI)1099-1026(199801/02)13:1<65::AID-FFJ695>3.0.CO;2-Q . [all data]

Kanasawud and Crouzet, 1990
Kanasawud, P.; Crouzet, J.C., Mechanism of formation of volatile compounds by thermal degradation of carotenoids in aqueous medium. 1. «beta»-Carotene degradation, J. Agric. Food Chem., 1990, 38, 1, 237-243, https://doi.org/10.1021/jf00091a052 . [all data]


Notes

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