1-Eicosene

Data at NIST subscription sites:

NIST subscription sites provide data under the NIST Standard Reference Data Program, but require an annual fee to access. The purpose of the fee is to recover costs associated with the development of data collections included in such sites. Your institution may already be a subscriber. Follow the links above to find out more about the data in these sites and their terms of usage.


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-ALLOY-5Ultra-ALLOY-5HP-5 MSHP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas   HeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.70.70.50.
Tend (C) 320.320.290.290.280.
Heat rate (K/min) 20.20.5.5.5.
Initial hold (min) 2.2.  1.
Final hold (min) 13.13.10.10.1.
I 1993.1993.1994.1994.1986.
ReferenceTsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011Radulovic, Blagojevic, et al., 2010Radulovic, Blagojevic, et al., 2009Bousaada, Ammar, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSPetrocol DHHP-5BPX-5HP-1
Column length (m) 30.150.30. 60.
Carrier gas He Helium He
Substrate      
Column diameter (mm) 0.250.250.32 0.25
Phase thickness (μm) 0.251.00.25 0.25
Tstart (C) 60.40.40.40.50.
Tend (C) 280.300.300.260.280.
Heat rate (K/min) 3.1.4.5.4.
Initial hold (min)     5.
Final hold (min)   5.  
I 1996.1992.1994.1987.1994.
ReferenceBozin, Mimicá-Dukic, et al., 2006Sojak, Kubinec, et al., 2006Utsunomia, Kawata, et al., 2005Diaz and Kite, 2002Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1Cross-Linked MethylsiliconeDB-1DB-1Ultra-1
Column length (m) 25.25.30.30.25.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.310.320.250.250.32
Phase thickness (μm) 0.15 0.250.250.25
Tstart (C) 70.35.50.50.80.
Tend (C) 220.225.240.240.260.
Heat rate (K/min) 3.4.5.5.3.
Initial hold (min)  3.3.3. 
Final hold (min)      
I 1988.2000.1991.2000.1988.
ReferenceRamaroson-Raonizafinimanana, Gaydou, et al., 1997Bravo and Hotchkiss, 1993Shiota, 1993Shiota, 1993Okumura, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SE-54CP Sil 8 CB
Column length (m) 25.25.
Carrier gas  H2
Substrate   
Column diameter (mm) 0.320.20
Phase thickness (μm)  0.13
Tstart (C) 100.60.
Tend (C) 280.300.
Heat rate (K/min) 2.6.
Initial hold (min)   
Final hold (min)   
I 1995.1988.
ReferenceScribe, Ngoumbi-Nzouzi, et al., 1990Yruela, Barbe, et al., 1990
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tsuge, Ohtan, et al., 2011
Tsuge, S.; Ohtan, H.; Watanabe, C., Pyrolysis - GC/MS Data Book of Synthetic Polymers, Elsevier, 2011, 420. [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Radulovic, Blagojevic, et al., 2009
Radulovic, N.S.; Blagojevic, P.D.; Palic, R.M.; Zlatkovic, B.K.; Stevanovic, B.M., Volatiles from vegetative organs of the paleoendemic resurrection plants Ramonda serbica Panc. and Ramonda nathaliae Panc. at Petrov, J. Serb. Chem. Soc., 2009, 74, 1, 35-44, https://doi.org/10.2298/JSC0901035R . [all data]

Bousaada, Ammar, et al., 2008
Bousaada, O.; Ammar, S.; Saidana, D.; Chriaa, J.; Chraif, I.; Daami, M.; Helal, A.N.; Mighri, Z., Chemical composition and antimicrobial activity of volatile components from capitula and aerial parts of Rhaponticum acaule DC growing wild in Tunisia, Microbiol. Res., 2008, 163, 1, 87-95, https://doi.org/10.1016/j.micres.2007.02.010 . [all data]

Bozin, Mimicá-Dukic, et al., 2006
Bozin, B.; Mimicá-Dukic, N.; Simin, N.; Anackov, G., Characterization of the volatile composition of essential oils of some lamiaceae spices and the antimicrobial and antioxidant activities of the entire oils, J. Agric. Food Chem., 2006, 54, 5, 1822-1828, https://doi.org/10.1021/jf051922u . [all data]

Sojak, Kubinec, et al., 2006
Sojak, L.; Kubinec, R.; Jurdakova, H.; Hajekova, E.; Bajus, M., GC-MS of polyethylene and polypropylene thermal cracking produxts, Petroleum Coal, 2006, 48, 1, 1-14. [all data]

Utsunomia, Kawata, et al., 2005
Utsunomia, H.; Kawata, J.; Chanoki, W.; Shirakawa, N.; Miyazawa, M., Components of Essential Oil from Woods of Prunus mume Sieb. at Zucc., J. Oleo Sci., 2005, 54, 11, 609-612, https://doi.org/10.5650/jos.54.609 . [all data]

Diaz and Kite, 2002
Diaz, A.; Kite, G.C., A comparison of the pollination ecology of Arum maculatum and A. italicum in England, Watsonia, 2002, 24, 171-181. [all data]

Stashenko, Cervantes, et al., 1998
Stashenko, E.E.; Cervantes, M.; Combariza, Y.; Martínez, J.R., HRGC-FID-MSD Analysis of the Secondary Metabolites Obtained by Different Extraction Methods from Lepechinia schiedeana, and Evaluation of its Antioxidant Activity in vitro in 20th International Symposium on Capillary Chromatography, 1998, 1-11. [all data]

Ramaroson-Raonizafinimanana, Gaydou, et al., 1997
Ramaroson-Raonizafinimanana, B.; Gaydou, E.M.; Bombarda, I., Hydrocarbons from three vanilla bean species: V. fragrans, V. madagascariensis, and V. tahitensis, J. Agric. Food Chem., 1997, 45, 7, 2542-2545, https://doi.org/10.1021/jf960927b . [all data]

Bravo and Hotchkiss, 1993
Bravo, A.; Hotchkiss, J.H., Identification of volatile compounds resulting from the thermal oxidation of polyethylene, J. Appl. Polym. Sci., 1993, 47, 10, 1741-1748, https://doi.org/10.1002/app.1993.070471004 . [all data]

Shiota, 1993
Shiota, H., New esteric components in the volatiles of banana fruit (Musa sapientum L.), J. Agric. Food Chem., 1993, 41, 11, 2056-2062, https://doi.org/10.1021/jf00035a046 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Scribe, Ngoumbi-Nzouzi, et al., 1990
Scribe, P.; Ngoumbi-Nzouzi, J.-S.; Fuché, C.; Pèpe, C.; Saliot, A., Biogeochemistry of organic matter in Lake Geneva: I. Particulate hydrocarbons as biogenic and anthropogenic molecular markers, Hydrobiologia, 1990, 207, 1, 319-331, https://doi.org/10.1007/BF00041471 . [all data]

Yruela, Barbe, et al., 1990
Yruela, I.; Barbe, A.; Grimalt, J.O., Determination of Double Bond Position and Geometry in Linear and High Branched Hydrocarbons and Fatty Acids from Gas Chromatography-Mass Spectrometry of Epoxides and Diols Generated by Stereospecific Resin Hydration, J. Chromatogr. Sci., 1990, 28, 8, 421-427, https://doi.org/10.1093/chromsci/28.8.421 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References