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5,6,7,8-Tetrahydroquinoxaline


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-11173.Du, Clery, et al., 200850. m/0.20 mm/0.33 «mu»m, Helium, 2. K/min, 280. C @ 20. min; Tstart: 50. C
CapillaryHP-51212.Du, Clery, et al., 200850. m/0.20 mm/0.33 «mu»m, Helium, 10. K/min, 280. C @ 8.5 min; Tstart: 50. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51223.Hartmann, 200330. m/0.25 mm/0.25 «mu»m, He; Program: 50 C(1min) => 20C/min => 80C => 25C/min => 250C (3 min)
CapillaryHP-51226.Hartmann, 200330. m/0.25 mm/0.25 «mu»m, He; Program: 50 C(1min) => 20C/min => 80C => 25C/min => 250C (3 min)

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax1717.Wong and Bernhard, 1988He, 70. C @ 8. min, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 160. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Du, Clery, et al., 2008
Du, Z.; Clery, R.; Hammond, C.J., Volatile organic nitrogen-containing constituents in ambrette seed Abelmoschus moschatus Medik (Malvaceae), J. Agric. Food Chem., 2008, 56, 16, 7388-7392, https://doi.org/10.1021/jf800958d . [all data]

Hartmann, 2003
Hartmann, P.J., The effect of wine matrix ingredients on 3-alkyl-2-methoxypyrazines measurements by headspace solid-phase microextraction (HS-SPME), Master's Thesis, Virginia Tech., Blacksburg, Va., 2003, 30. [all data]

Wong and Bernhard, 1988
Wong, J.M.; Bernhard, R.A., Effect of nitrogen source on pyrazine formation, J. Agric. Food Chem., 1988, 36, 1, 123-129, https://doi.org/10.1021/jf00079a032 . [all data]


Notes

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