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3-Mercapto-3-methylbutanol


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBCP Sil 5 CBDB-5CP Sil 5 CB
Column length (m) 50.50. 50.
Carrier gas Nitrogen  He
Substrate     
Column diameter (mm) 0.320.32 0.32
Phase thickness (mum) 1.201.2 1.2
Program 36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0C (30 min)40C(4min) => 2C/min => 132C => 10C/min => 250C (15min)not specified40C(4min) => 2C/min => 132C => 10C/min => 250C(45min)
I 938.944.972.944.
ReferenceGros, Nizet, et al., 2011Vermeulen, Lejeune, et al., 2006Acree and Arn, 2004Vermeulen, Guyot-Declerck, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gros, Nizet, et al., 2011
Gros, J.; Nizet, S.; Collin, S., Occurence of odorant polyfunctional thiols in the Super Alpha Tomahawk Hop cultivar. Comparison with the thiol-rich Nelson Sauvin bitter variety, J. Agric. Food Chem., 2011, 59, 16, 8853-8865, https://doi.org/10.1021/jf201294e . [all data]

Vermeulen, Lejeune, et al., 2006
Vermeulen, C.; Lejeune, I.; Tran, T.T.H.; Collin, S., Occurrence of polyfunctional thiols in fresh lager beers, J. Agric. Food Chem., 2006, 54, 14, 5061-5068, https://doi.org/10.1021/jf060669a . [all data]

Acree and Arn, 2004
Acree, T.; Arn, H., Flavornet, 2004, retrieved from http://www.flavornet.org/. [all data]

Vermeulen, Guyot-Declerck, et al., 2003
Vermeulen, C.; Guyot-Declerck, C.; Collin, S., Combinatorial synthesis and sensorial properties of mercapto primary alcohols and analogues, J. Agric. Food Chem., 2003, 51, 12, 3623-3628, https://doi.org/10.1021/jf0212340 . [all data]


Notes

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