1,3,6-Octatriene, 3,7-dimethyl-, (Z)-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxHP-InnowaxBP-20DB-WaxDB-Wax
Column length (m) 60.60. 15.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.220.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.40.80.
Tend (C) 230.220.200.260.240.
Heat rate (K/min) 2.5.5.4.3.
Initial hold (min)  1.   
Final hold (min) 5.5. 5.2.
I 1215.1241.1230.1235.1236.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Feng, Cui, et al., 2011Mishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxRTX-WaxCP-Wax 52CBTC-FFAPCarbowax 20M
Column length (m) 30.60.30. 30.
Carrier gas HydrogenHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 30.60.40.60.60.
Tend (C) 230.230.220.220.230.
Heat rate (K/min) 8.2.3.3.3.
Initial hold (min) 5. 1.  
Final hold (min) 10.30.2.30. 
I 1246.1215.1241.1246.1195.
ReferenceKarlsson, Birgersson, et al., 2009Museli, Pau, et al., 2009Hymete, Rohloff, et al., 2007Kurose, Okamura, et al., 2007Limberger, Scopel, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10CarbowaxSupelcowax-10Innowax
Column length (m) 60.30.60.30.30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 70.70.40.40.50.
Tend (C) 220.220.180.250.280.
Heat rate (K/min) 4.3.5.2.9.
Initial hold (min)     3.
Final hold (min)  15. 33.3.
I 1232.1235.1236.1251.1230.
ReferencePala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007Singh, Kumar, et al., 2007Sylvestre, Pichette, et al., 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxBP-20DB-WaxSupelcowax 10BP-20
Column length (m) 30.50.60.30.50.
Carrier gas N2 HeHeliumHe
Substrate      
Column diameter (mm) 0.250.220.250.200.22
Phase thickness (μm) 0.250.250.50.200.25
Tstart (C) 50.60.50.70.60.
Tend (C) 280.220.230.220.220.
Heat rate (K/min) 9.2.3.3.2.
Initial hold (min) 3. 2.  
Final hold (min) 3.20.20.15.20.
I 1232.1233.1243.1235.1230.
ReferenceAbdelwahed, Hayder, et al., 2006Boti, Yao, et al., 2006Cai, Lin, et al., 2006Cavaleiro, Pinto, et al., 2006Fanciullino, Tomi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBFFAPDB-WaxSupelcowaxNB-20M
Column length (m) 30.20.60.30.30.
Carrier gas HeHe N2He
Substrate      
Column diameter (mm) 0.320.250.250.320.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.90.70.50.50.
Tend (C) 220.250.230.200.250.
Heat rate (K/min) 3.36.2.5.2.
Initial hold (min) 7. 2.  
Final hold (min) 3. 20.  
I 1233.1265.1236.1241.1220.
ReferenceHymete, Rohloff, et al., 2006Kitchlu, Bakshi, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Martin, Joseph, et al., 2006Orav, Raal, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Supelcowax-10Carbowax 20MHP-20M
Column length (m) 60.30.30.60.50.
Carrier gas  HeHeN2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.250.250.250.20
Tstart (C) 70.50.50.40.70.
Tend (C) 230.220.250.190.250.
Heat rate (K/min) 2.4.4.10.4.
Initial hold (min) 2.1.1.2.4.
Final hold (min) 20.10.10.15.10.
I 1236.1233.1245.1238.1218.
ReferenceSawamura, Onishi, et al., 2006Wong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Babu and Kaul, 2005Bezic, Skocibusic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxSupelcowaxStabilwaxStabilwaxHP-20M
Column length (m) 30.60.30.30.50.
Carrier gas HeHeH2 Helium
Substrate      
Column diameter (mm) 0.250.20.320.320.20
Phase thickness (μm) 0.170.20.50.50.20
Tstart (C) 60.60.40.40.70.
Tend (C) 210.230.280.280.180.
Heat rate (K/min) 4.4.6.6.4.
Initial hold (min) 3.30.5.5.4.
Final hold (min) 15. 5.5.10.
I 1240.1211.1224.1225.1218.
ReferenceFerretti, Maggi, et al., 2005Gauvin and Smadja, 2005Jirovetz, Buchbauer, et al., 2005Jirovetz, Buchbauer, et al., 2005, 2Kulisic, Radonic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxSupelcowax-10DB-WaxDB-Wax
Column length (m) 60.60.30.30.60.
Carrier gas N2N2HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.50.90.70.
Tend (C) 230.230.220.220.230.
Heat rate (K/min) 2.2.4.7.2.
Initial hold (min) 2.2.3.2.2.
Final hold (min) 20.20.30.5.20.
I 1256.1256.1227.1264.1246.
ReferenceNjoroge, Koaze, et al., 2005Njoroge, Koaze, et al., 2005, 2Wong, Lee, et al., 2005Agnihotri, Thappa, et al., 2004Choi, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxSupelcowax-10Innowax FSCDB-Wax
Column length (m) 60.60.30.60.60.
Carrier gas HeHe HeliumHe
Substrate      
Column diameter (mm) 0.20.250.250.250.32
Phase thickness (μm) 0.2 0.25 0.25
Tstart (C) 60.60.40.60.35.
Tend (C) 200.220.210.220.220.
Heat rate (K/min) 4.2.2.4.3.
Initial hold (min)  4.2.10. 
Final hold (min) 40. 33.  
I 1210.1244.1200.1246.1234.
ReferenceGauvin, Ravaomanarivo, et al., 2004Jiang and Kubota, 2004Lopez Arze, Collin, et al., 2004Lourens, Reddy, et al., 2004Palá-Paúl, Brophy, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxSW-10DB-WaxDB-WaxHP-20M
Column length (m) 50.50.60.60.50.
Carrier gas HeHe NitrogenHe
Substrate      
Column diameter (mm) 0.20.200.250.250.2
Phase thickness (μm) 0.20.250.250.250.2
Tstart (C) 70.50.70.70.70.
Tend (C) 220.230.230.230.180.
Heat rate (K/min) 4.2.2.2.4.
Initial hold (min)   2.2.4.
Final hold (min)   20. 10.
I 1244.1221.1250.1250.1218.
ReferencePalá-Paúl, García-Jiménez, et al., 2004Raal, Paaver, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Juteau, Jerkovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-20MDB-WaxSupelcowax-10Carbowax 20MSW-10
Column length (m) 50.60.50.50.50.
Carrier gas HeHeliumHeN2He
Substrate      
Column diameter (mm) 0.20.250.20.250.20
Phase thickness (μm) 0.2 0.250.250.25
Tstart (C) 70.70.70.90.50.
Tend (C) 180.210.230.220.250.
Heat rate (K/min) 4.2.2.3.2.
Initial hold (min) 4.    
Final hold (min) 10.60.   
I 1230.1238.1232.1234.1232.
ReferenceMastelic and Jerkovic, 2003Mookdasanit, Tamura, et al., 2003Orav, Kailas, et al., 2003Priestap, van Baren, et al., 2003Raal, Arak, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxDB-WaxDB-WaxHP-InnowaxDB-Wax
Column length (m) 60.60.60.50.60.
Carrier gas HeN2N2HeH2
Substrate      
Column diameter (mm) 0.250.250.250.20.32
Phase thickness (μm)  0.250.250.20.25
Tstart (C) 60.70.70.70.40.
Tend (C) 220.230.230.190.245.
Heat rate (K/min) 4.2.2.5.1.5
Initial hold (min) 10.2.2.  
Final hold (min) 10.20.20. 20.
I 1246.1222.1226.1234.1228.
ReferenceSuleimenov, Atazharova, et al., 2003Tu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2Velasco-Negueruela, Pérez-Alonso, et al., 2003Gancel, Ollé, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10HP-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.50.60.60.60.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.50.250.250.250.25
Tstart (C) 70.75.70.70.40.
Tend (C) 220.220.230.230.200.
Heat rate (K/min) 2.3.2.2.2.
Initial hold (min)  4.2. 2.
Final hold (min)   20.  
I 1232.1234.1230.1234.1225.
ReferenceOrav, Kailas, et al., 2002Priestap, van Baren, et al., 2002Tu, Onishi, et al., 2002Tu, Thanh, et al., 2002Umano, Hagi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxStabilwaxCarbowax 20MBP-20
Column length (m) 60.60.30.30.50.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.22
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 45.40.60.50.60.
Tend (C) 240.220.280.215.230.
Heat rate (K/min) 3.2.10.4.2.
Initial hold (min)   5.  
Final hold (min)   5. 35.
I 1238.1234.1234.1228.1228.
ReferenceChristoph, 2001Jiang and Kubota, 2001Jirovetz L., Buchbauer G., et al., 2001Kasali, Oyedeji, et al., 2001Lota, de Rocca Serra, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MCP-Wax 52CBCP-Wax 52CBDB-WaxDB-Wax
Column length (m) 50.50.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.300.300.20.2
Phase thickness (μm)  0.250.25  
Tstart (C) 70.40.40.50.50.
Tend (C) 220.220.220.180.180.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min)  5.5.8.8.
Final hold (min)      
I 1232.1240.1240.1236.1236.
ReferenceOrav and Kann, 2001Chagonda, Makanda, et al., 2000Chagonda, Makanda, et al., 2000Franco and Shibamoto, 2000Franco and Shibamoto, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20DB-WaxDB-WaxDB-WaxInnowax
Column length (m) 25.60.60.60.60.
Carrier gas NitrogenHeliumNitrogenHeHe
Substrate      
Column diameter (mm) 0.500.320.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.50.40.40.60.
Tend (C) 200.230.200.200.220.
Heat rate (K/min) 5.5.2.2. 
Initial hold (min)  2.10.2.10.
Final hold (min)      
I 1220.1235.1241.1230.1246.
ReferenceMallavarapu, Rao, et al., 2000Paniandy, Chane-Ming, et al., 2000Tamura, Boonbumrung, et al., 2000Umano, Hagi, et al., 2000Kaya, Baser, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxDB-WaxBP-20BP-20CP-Wax 52CB
Column length (m) 60.60.25.25.25.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.250.250.50.330.32
Phase thickness (μm) 0.250.25 0.50.2
Tstart (C) 60.60.60.80.60.
Tend (C) 220.240.200.220.240.
Heat rate (K/min)  4.5.5.6.
Initial hold (min) 10.   2.
Final hold (min)     10.
I 1246.1232.1257.1248.1227.
ReferenceKaya, Baser, et al., 1999, 2Ngassoum, Yonkeu, et al., 1999Rao, Bhattacharya, et al., 1999Bignell, Dunlop, et al., 1998Chisowa, Hall, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-Innowax FSCPEG-20MHP-Innowax FSCBP-20
Column length (m) 30.60.60.60.25.
Carrier gas N2He HeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.33
Phase thickness (μm) 0.250.25  0.5
Tstart (C) 45.60.70.60.80.
Tend (C) 220.220.220.240.220.
Heat rate (K/min) 3.4.3.4.5.
Initial hold (min)  10. 10. 
Final hold (min)  10. 10. 
I 1236.1246.1237.1246.1248.
ReferenceMölleken, Sinnwell, et al., 1998Tümen, Baser, et al., 1998Awano, Ichikawa, et al., 1997Baser, Kirimer, et al., 1997Bignell, Dunlop, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20SP-1000DB-Wax
Column length (m) 25.25.25.85.60.
Carrier gas H2 H2HeHe
Substrate      
Column diameter (mm) 0.330.330.330.500.32
Phase thickness (μm) 0.50.50.5 0.50
Tstart (C) 80.80.80.65.50.
Tend (C) 220.220.220.225.250.
Heat rate (K/min) 5.5.5.3.8.
Initial hold (min)     1.
Final hold (min)     6.
I 1248.1248.1248.1237.1226.
ReferenceBignell, Dunlop, et al., 1997, 2Bignell, Dunlop, et al., 1997, 3Bignell, Dunlop, et al., 1997, 4Brophy, Goldsack, et al., 1996Sagrero-Nieves and Bartley, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MDB-WaxDB-WaxCarbowax 20M
Column length (m) 60.45.30.60.25.
Carrier gas HeHydrogen He 
Substrate      
Column diameter (mm) 0.250.320.320.3220.30
Phase thickness (μm) 0.251.0 0.25 
Tstart (C) 50.60.70.50.40.
Tend (C) 150.200.200.230.220.
Heat rate (K/min) 2.2.4.4.2.
Initial hold (min) 10.5.2. 5.
Final hold (min) 20.    
I 1235.1242.1248.1232.1239.
ReferenceTirado, Stashenko, et al., 1995Kollmannsberger, Nitz, et al., 1992Wyllie, Brophy, et al., 1990Engel, Flath, et al., 1988Nykanen, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 30.150.150.50.50.
Carrier gas H2   N2
Substrate      
Column diameter (mm) 0.250.660.640.320.28
Phase thickness (μm) 0.25    
Tstart (C) 50.60.50.70.80.
Tend (C) 250.170.170.180.170.
Heat rate (K/min) 5.1.1.2.1.
Initial hold (min)  40.   
Final hold (min)   30.  
I 1200.1230.1230.1232.1200.
ReferencePerry, Baxter, et al., 1986Buttery, Xu, et al., 1985Buttery, Kamm, et al., 1984Engel and Tressl, 1983Yamaguchi and Shibamoto, 1980
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

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Miyazawa, M.; Kawauchi, Y.; Utsumi, Y.; Takahashi, T., Character impact odorants of wild edible plant - Cacalia hastata L. var. orientalis - used in Japanese traditional food, J. Oleo Sci., 2010, 59, 10, 527-533, https://doi.org/10.5650/jos.59.527 . [all data]

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Hymete, A.; Rohloff, J.; Iversen, T.-H.; Kjosen, H., Volatile constituents of the roots of Echinops kebericho Mesfin, Flavour Fragr. J., 2007, 22, 1, 35-38, https://doi.org/10.1002/ffj.1746 . [all data]

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Notes

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