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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1OV-1OV-1
Column length (m) 25.25.25.25.25.
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.100.100.100.100.10
Tstart (C) 160.160.160.160.160.
Tend (C) 240.240.240.240.240.
Heat rate (K/min) 1.1.1.31.31.5
Initial hold (min) 1.1.1.1.1.
Final hold (min)      
I 1925.1928.1929.1933.1926.
Referencede Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1SP-2100SP-2100
Column length (m) 25.25.25.  
Carrier gas    H2H2
Substrate      
Column diameter (mm) 0.320.320.32  
Phase thickness (mum) 0.100.100.10  
Tstart (C) 160.160.160.170.170.
Tend (C) 240.240.240.  
Heat rate (K/min) 1.52.2.2.4.
Initial hold (min) 1.1.1.  
Final hold (min)      
I 1928.1930.1933.1932.181939.62
Referencede Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991de Paoli, Taccheo-Barbina, et al., 1991Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100SP-2100SP-2100CP Sil 5 CB
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 170.170.170.170.170.
Tend (C)      
Heat rate (K/min) 6.2.4.6.4.
Initial hold (min)      
Final hold (min)      
I 1948.721946.471950.511959.901961.08
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m) 1.8
Carrier gas N2
Substrate Chromosorb W
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 130.
Tend (C) 290.
Heat rate (K/min) 8.
Initial hold (min) 2.
Final hold (min) 8.
I 1940.
ReferencePerrigo and Peel, 1981
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

de Paoli, Taccheo-Barbina, et al., 1991
de Paoli, M.; Taccheo-Barbina, M.; Bontempelli, G., Gas chromatographic system for the identification of halogenated pesticides by retention indices using n-alkanes as standards, J. Chromatogr., 1991, 547, 355-365, https://doi.org/10.1016/S0021-9673(01)88659-3 . [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W., The use of retention indices and temperature-programmed gas chromatography in analytical toxicology, J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References