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3,3,6-Trimethyl-1,4-heptadien-6-ol


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryDB-5999.Asfaw, Licence, et al., 200510. m/0.1 mm/0.1 «mu»m, He, 60. C @ 5. min, 5. K/min, 240. C @ 10. min

Kovats' RI, non-polar column, custom temperature program

View large format table.

Column typeActive phaseIReferenceComment
CapillaryDB-5MS996.Tuberoso, Kowalczyk, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 60C(5min) => 2C/min => 140C= 5C/min => 250C(5min)
CapillaryOV-1991.El-Shazly, Dorai, et al., 200230. m/0.25 mm/0.25 «mu»m, He; Program: 44C(4min) => 3C/min => 74C => 6C/min => 134C => 12C/min => 312C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryRTX-1983.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryDB-5998.Esmaeili, Nematollahi, et al., 200650. m/0.2 mm/0.32 «mu»m, N2, 60. C @ 3. min, 5. K/min, 220. C @ 5. min
CapillaryDB-1987.Dob, Dahmane, et al., 200530. m/0.32 mm/0.25 «mu»m, 50. C @ 8. min, 2. K/min; Tend: 250. C
CapillaryDB-5992.Senatore, Napolitano, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryDB-51000.Bader, Flamini, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5999.Flamini, Luigi Cioni, et al., 200330. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryOV-1990.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 «mu»m, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column typeActive phaseIReferenceComment
CapillaryRTX-Wax1387.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryCarbowax 20M1427.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 «mu»m, H2, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Normal alkane RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryRTX-1991.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 5. min; Tstart: 60. C
CapillaryRTX-1984.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryRTX-1991.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryOV-1987.Nibret and Wink, 200930. m/0.25 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 4. K/min, 300. C @ 10. min
CapillaryUltra 21001.Byun and Shin, 200850. m/0.20 mm/0.11 «mu»m, Helium, 60. C @ 5. min, 2. K/min, 230. C @ 30. min
CapillaryDB-51003.Mosayebi, Amin, et al., 200860. m/0.25 mm/0.25 «mu»m, Nitrogen, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryHP-5MS991.Basta, Pavlovic, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-1984.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.33 «mu»m, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryDB-5998.Chagonda and Chalchat, 200550. m/0.3 mm/0.25 «mu»m, 2. K/min; Tstart: 60. C; Tend: 240. C
CapillaryBP-1982.Blanc, Muselli, et al., 200450. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-5999.Rohloff, Mordal, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 2.5 K/min, 220. C @ 6. min; Tstart: 35. C
CapillaryDB-5996.Senatore, Rigano, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min
CapillaryDB-5MS989.Cherchi, Deidda, et al., 200130. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5999.Tellez, Canel, et al., 199930. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5997.Tellez, Estell, et al., 199730. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column typeActive phaseIReferenceComment
CapillaryRTX-1981.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryHP-1996.Merle, Verdeguer, et al., 200730. m/0.2 mm/0.33 «mu»m, He; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillarySE-52999.Tognolini, Barocelli, et al., 200630. m/0.32 mm/0.15 «mu»m, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
Capillary 991.El-Shazily, Hafez, et al., 2004Program: not specified
CapillarySE-30988.Vinogradov, 2004Program: not specified
CapillaryCP Sil 5 CB988.Weyerstahl, Marschall, et al., 1997N2; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryPolydimethyl siloxanes988.Zenkevich, 1997Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column typeActive phaseIReferenceComment
CapillaryRTX-Wax1390.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryHP-20M1377.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.1 «mu»m, He, 2. K/min, 220. C @ 30. min; Tstart: 60. C
CapillaryBP-201397.Blanc, Muselli, et al., 200450. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1404.Umano, Hagi, et al., 200060. m/0.25 mm/0.25 «mu»m, He, 40. C @ 2. min, 2. K/min; Tend: 200. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column typeActive phaseIReferenceComment
CapillaryCarbowax 20M1405.Merle, Verdeguer, et al., 2007He; Column length: 30. m; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillaryHP Innowax FSP1403.Tabanca N., Demirci B., et al., 200760. m/0.25 mm/0.25 «mu»m, N2; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryInnowax FSC1403.Iscan, Kirimer, et al., 200660. m/0.25 mm/0.25 «mu»m, N2; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryCarbowax 20M1382.Vinogradov, 2004Program: not specified
CapillaryHP-Innowax FSC1403.Kürkcüoglu, Demirci, et al., 200360. m/0.25 mm/0.25 «mu»m, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(40min)
CapillaryHP-Innowax1403.Gören, Demirci, et al., 200160. m/0.25 mm/0.25 «mu»m, He; Program: 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
CapillaryCP-Wax 52CB1382.Vernin, 1991Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Asfaw, Licence, et al., 2005
Asfaw, N.; Licence, P.; Novitskii, A.; Poliakoff, M., Green Chemistry in Ethiopia: the cleaner extraction of essential oils from Artemisia afra: a comparison of clean technology with conventional methodology, Green Chem., 2005, 7, 5, 352-356. [doi:10.1039/b417961g] [all data]

Tuberoso, Kowalczyk, et al., 2005
Tuberoso, C.I.G.; Kowalczyk, A.; Coroneo, V.; Russo, M.T.; Dessì, S.; Cabras, P., Chemical Composition and Antioxidant, Antimicrobial, and Antifungal Activities of the Essential Oil of Achillea ligustica All., J. Agric. Food Chem., 2005, 53, 26, 10148-10153. [doi:10.1021/jf0518913] [all data]

El-Shazly, Dorai, et al., 2002
El-Shazly, A.; Dorai, G.; Wink, M., Composition and antimicrobial activity of essential oil and hexane-ether extract of Tanacetum santolinoides (DC.) Feinbr. and Fertig, Z. Naturforsch., 2002, 57c, 620-623. [all data]

Muselli, Rossi, et al., 2007
Muselli, A.; Rossi, P.-G.; Desjobert, J.-M.; Bernardini, A.-F.; Berti, L.; Costa, J., Chemical composition and antibacterial activity of Otanthus maritimus (L.) Hoffmanns. Link essential oils from Corsica, Flavour Fragr. J., 2007, 22, 3, 217-223. [doi:10.1002/ffj.1787] [all data]

Esmaeili, Nematollahi, et al., 2006
Esmaeili, A.; Nematollahi, F.; Rustaiyan, A.; Moazami, N.; Masoudi, S.; Bamasian, S., Volatile constituents of Achillea pachycephala, A. oxyodonta and A. biebersteinii from Iran, Flavour Fragr. J., 2006, 21, 2, 253-256. [doi:10.1002/ffj.1571] [all data]

Dob, Dahmane, et al., 2005
Dob, T.; Dahmane, D.; Berramdane, T.; Chelghoum, C., Chemical composition of the essential oil of Artemisia campestris L. from Algeria, Pharm. Biol., 2005, 43, 6, 512-514. [doi:10.1080/13880200500220664] [all data]

Senatore, Napolitano, et al., 2005
Senatore, F.; Napolitano, F.; Arnold, N.A.; Bruno, M.; Herz, W., Composition and antimicrobial activity of the essential oil of Achillea falcata L. (Asteraceae), Flavour Fragr. J., 2005, 20, 3, 291-294. [doi:10.1002/ffj.1411] [all data]

Bader, Flamini, et al., 2003
Bader, A.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oil composition of Achillea santolina L. and Achillea biebersteinii Afan. collected in Jordan, Flavour Fragr. J., 2003, 18, 1, 36-38. [doi:10.1002/ffj.1147] [all data]

Flamini, Luigi Cioni, et al., 2003
Flamini, G.; Luigi Cioni, P.; Morelli, I., Differences in the fragrances of pollen, leaves, and floral parts of garland (Chrysanthemum coronarium) and composition of the essential oils from flowerheads and leaves, J. Agric. Food Chem., 2003, 51, 8, 2267-2271. [doi:10.1021/jf021050l] [all data]

Bicchi, Rubiolo, et al., 1998
Bicchi, C.; Rubiolo, P.; Marschall, H.; Weyerstahl, P.; Laurent, R., Constituents of Artemisia roxburghiana Besser essential oil, Flavour Fragr. J., 1998, 13, 1, 40-46. [doi:10.1002/(SICI)1099-1026(199801/02)13:1<40::AID-FFJ688>3.0.CO;2-Z] [all data]

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

Museli, Pau, et al., 2009
Museli, A.; Pau, M.; Desjobert, J.-M.; Foddai, M.; Usai, M.; Costa, J., Volatile constituents of Achllea ligustica All. by HS-SPME/GC/GC-MS. Comparison with essential oils obtained by hydrodistillation from Corsica and Sardinia, Chromatographia, 2009, 69, 5/6, 575-585. [doi:10.1365/s10337-008-0939-1] [all data]

Nibret and Wink, 2009
Nibret, E.; Wink, M., Volatile components of four Ethiopian Artemisia species extracts and their in vitro antipatrypanosomal and cytotoxic activities, Phytomedicine, 2009, 00, 0, 000-000. [all data]

Byun and Shin, 2008
Byun, Y.; Shin, S., Analysis of compounds and activity of essential oil from Chrysanthemum zawadskii var. latilobum and C. indicum agaunst antibiotic-resistant pathogenic bacteria, Nat. Prod. Sci., 2008, 14, 2, 138-142. [all data]

Mosayebi, Amin, et al., 2008
Mosayebi, M.; Amin, G.; Arzani, H.; Azarnivand, H.; Maleki, M.; Shafaghat, A., Effect of habitat on essential oil of Achillea filipendula L. in Iran, Asian J. Plant Sci., 2008, 7, 8, 779-781. [doi:10.3923/ajps.2008.779.781] [all data]

Basta, Pavlovic, et al., 2007
Basta, A.; Pavlovic, M.; Couladis, M.; Tzakou, O., Essential oil composition of the flowerheads of Chrysanthemum coronarium L. from Greece, Flavour Fragr. J., 2007, 22, 3, 197-200. [doi:10.1002/ffj.1781] [all data]

Filippi, Lanfranchi, et al., 2006
Filippi, J.-J.; Lanfranchi, D.-A.; Prado, S.; Baldovini, N.; Meierhenrich, U.J., Composition, Enantiomeric Distribution, and Antibacterial Activity of the Essential Oil of Achillea ligustica All. from Corsica, J. Agric. Food Chem., 2006, 54, 17, 6308-6313. [doi:10.1021/jf060752y] [all data]

Chagonda and Chalchat, 2005
Chagonda, L.S.; Chalchat, J.-C., The essential oil of wild and cultivated Hoslundia opposita Vahl. from Zimbabwe, Flavour Fragr. J., 2005, 20, 2, 193-195. [doi:10.1002/ffj.1402] [all data]

Blanc, Muselli, et al., 2004
Blanc, M.-C.; Muselli, A.; Bradesi, P.; Casanova, J., Chemical composition and variability of the essential oil of Inula graveolens from Corsica, Flavour Fragr. J., 2004, 19, 4, 314-319. [doi:10.1002/ffj.1304] [all data]

Rohloff, Mordal, et al., 2004
Rohloff, J.; Mordal, R.; Dragland, S., Chemotypical variation of tansy (Tanacetum vulgare L.) from 40 different locations in Norway, J. Agric. Food Chem., 2004, 52, 6, 1742-1748. [doi:10.1021/jf0352430] [all data]

Senatore, Rigano, et al., 2004
Senatore, F.; Rigano, D.; de Fusco, R.; Bruno, M., Composition of the essential oil from flowerheads of Chrysanthemum coronarium L. (Asteraceae) growing wild in Southern Italy, Flavour Fragr. J., 2004, 19, 2, 149-152. [doi:10.1002/ffj.1285] [all data]

Cherchi, Deidda, et al., 2001
Cherchi, G.; Deidda, D.; de Gioannis, B.; Marongiu, B.; Pompei, R.; Porcedda, S., Extraction of Santolina insularis essential oil by supercritical carbon dioxide: influence of some process parameters and biological activity, Flavour Fragr. J., 2001, 16, 1, 35-43. [doi:10.1002/1099-1026(200101/02)16:1<35::AID-FFJ942>3.0.CO;2-Y] [all data]

Tellez, Canel, et al., 1999
Tellez, M.R.; Canel, C.; Rimando, A.M.; Duke, S.O., Differential accumulation of isoprenoids in glanded and glandless Artemisia annua L, Phytochemistry, 1999, 52, 6, 1035-1040. [doi:10.1016/S0031-9422(99)00308-8] [all data]

Tellez, Estell, et al., 1997
Tellez, M.R.; Estell, R.E.; Frederickson, E.L.; Havstad, K.M., Essntial oil of Flourensia cernua DC, J. Essent. Oil Res., 1997, 9, 6, 619-624. [doi:10.1080/10412905.1997.9700799] [all data]

Merle, Verdeguer, et al., 2007
Merle, H.; Verdeguer, M.; Blázquez, M.A.; Boira, H., Chemical composition of the essential oils from Eriocephalus africanus L. var. africanus populations growing in Spain, Flavour Fragr. J., 2007, 22, 6, 461-464. [doi:10.1002/ffj.1821] [all data]

Tognolini, Barocelli, et al., 2006
Tognolini, M.; Barocelli, E.; Ballabeni, V.; Bruni, R.; Bianchi, A.; Chiavarini, M.; Impicciatore, M., Comparative screening of plant essential oils: Phenylpropanoid moiety as basic core for antiplatelet activity, Life Sciences, 2006, 78, 13, 1419-1432. [doi:10.1016/j.lfs.2005.07.020] [all data]

El-Shazily, Hafez, et al., 2004
El-Shazily, A.M.; Hafez, S.S.; Wink, M., Comparative study of the essential oils and extracts of Achillea fragrantissima (Forssk.) Sch. Bip. and Achillea santolina L. (Asteraceae) from Egypt, Pharmazie, 2004, 59, 226-230. [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Weyerstahl, Marschall, et al., 1997
Weyerstahl, P.; Marschall, H.; Seelmann, I.; Rustaiyan, A., Constituents of the essential oil of Achillea eriophora DC, Flavour Fragr. J., 1997, 12, 2, 71-78. [doi:10.1002/(SICI)1099-1026(199703)12:2<71::AID-FFJ620>3.0.CO;2-E] [all data]

Zenkevich, 1997
Zenkevich, I.G., Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons, Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]

Umano, Hagi, et al., 2000
Umano, K.; Hagi, Y.; Nakahara, K.; Shoji, A.; Shibamoto, T., Volatile chemicals identified in extracts from leaves of Japanese mugwort (Artemisia princeps Pamp.), J. Agric. Food Chem., 2000, 48, 8, 3463-3469. [doi:10.1021/jf0001738] [all data]

Tabanca N., Demirci B., et al., 2007
Tabanca N.; Demirci B.; Crockett S.L.; Baser K.H.C.; Wedge D.E., Chemical composition and antifungal activity of Arnica longifolia, Aster hesperius, and Chrysothamnus nauseosus essential oils, J. Agric. Food Chem., 2007, 55, 21, 8430-8435. [doi:10.1021/jf071379c] [all data]

Iscan, Kirimer, et al., 2006
Iscan, G.; Kirimer, N.; Kurkcuoglu, M.; Arabaci, T.; Kupeli, E.; Baser, K.H.C., Biological Activity and Composition of the Essential Oils of Achillea schischkinii Sosn. and Achillea aleppica DC. subsp. aleppica, J. Agric. Food Chem., 2006, 54, 1, 170-173. [doi:10.1021/jf051644z] [all data]

Kürkcüoglu, Demirci, et al., 2003
Kürkcüoglu, M.; Demirci, B.; Tabanca, N.; Özek, T.; Baser, K.H.C., The essential oil of Achillea falcata L., Flavour Fragr. J., 2003, 18, 3, 192-194. [doi:10.1002/ffj.1176] [all data]

Gören, Demirci, et al., 2001
Gören, N.; Demirci, B.; Baser, K.H.C., Composition of the essential oils of Tanacetum spp. from Turkey, Flavour Fragr. J., 2001, 16, 3, 191-194. [doi:10.1002/ffj.976] [all data]

Vernin, 1991
Vernin, G., Volatile constituents of the essential oil of Santolina chamaecyparissus L., J. Essent. Oil Res., 1991, 3, 1, 49-53. [doi:10.1080/10412905.1991.9697907] [all data]


Notes

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