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«gamma»-Muurolene


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1HP-5 MSHP-5HP-5
Column length (m) 60.60.30.25.25.
Carrier gas HeliumHeliumHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.220.220.250.320.32
Phase thickness (mum) 0.250.250.250.520.52
Tstart (C) 60.60.80.40.40.
Tend (C) 230.230.240.280.280.
Heat rate (K/min) 2.2.4.4.4.
Initial hold (min)   3.  
Final hold (min) 5.5.10.10.10.
I 1473.1473.1462.1471.1471.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dutra, Pittella, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DP-5DP-5DB-5CP-Sil 5 CB
Column length (m) 25.30.30.30.30.
Carrier gas HydrogenHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.520.250.250.250.26
Tstart (C) 40.80.80.60.45.
Tend (C) 280.300.300.240.280.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)  1.1.  
Final hold (min) 10.40.40. 22.
I 1471.1435.1435.1477.1475.
ReferenceVelickovic, Ristic, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012Karimi, Farmani, et al., 2011Mothana, Hasson, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5 MSDB-5HP-5SPB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.50.60.
Tend (C) 290.250.240.250.240.
Heat rate (K/min) 5.2.3.5.3.
Initial hold (min)   2.3. 
Final hold (min)    15. 
I 1476.1480.1479.1459.1475.
ReferenceBoix, Victorio, et al., 2010Ho, Wang, et al., 2010Kahriman, Tosun, et al., 2010Lazarevic, Palic, et al., 2010Magalhaes, Lima, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSBP-1SPB-1HP-5 MSHP-5 MS
Column length (m) 60. 30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.25 0.200.250.25
Phase thickness (mum) 0.25 0.200.250.25
Tstart (C) 40.60.70.60.100.
Tend (C) 250.220.220.220.220.
Heat rate (K/min) 5.5.3.5.2.
Initial hold (min) 15.10. 10. 
Final hold (min) 15.30.15.  
I 1479.1478.1462.1477.1477.
ReferenceMesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010Neves, Rosa, et al., 2010Ogunwande, Flamini, et al., 2010Pripdeevech, Chumpolsri, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5 MSDB-1DB-5 MS
Column length (m) 30.30.30.60.30.
Carrier gas HeliumHydrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.70.60.60.
Tend (C) 290.290.290.250.240.
Heat rate (K/min) 5.5.5.4.3.
Initial hold (min)    1. 
Final hold (min) 10. 10.10. 
I 1483.1484.1473.1480.1484.
ReferenceRadulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Safaei-Ghomi, Meshkatalsadat, et al., 2010Silva, Pott, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1-MSDB-1SE-54DB-5HP-5
Column length (m) 60.30.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 30.50.60.50.60.
Tend (C) 200.220.260.250.240.
Heat rate (K/min) 2.4.2.5.3.
Initial hold (min) 4.2.5.2. 
Final hold (min) 35.2.999. 7.
I 1463.1470.1471.1480.1495.
ReferenceTakeoka, Hobbs, et al., 2010Xu, Tang, et al., 2010Dayisoylu and Alma, 2009Ho, Wang, et al., 2009Maridass, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1DB-5DB-55 % Phenyl methyl siloxane
Column length (m) 60.60.30.30.60.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.45.40.90.
Tend (C) 230.230.250.250.225.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)   3.1. 
Final hold (min) 30.30.5.10.3.
I 1474.1474.1474.1478.1482.
ReferenceMuseli, Pau, et al., 2009Museli, Pau, et al., 2009Porto, Decorti, et al., 2009Rahmi-Nasrabadi, Gholivand, et al., 2009Retta, Gattuso, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5 MSDB-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 40.50.40.50.60.
Tend (C) 230.220.250.280.280.
Heat rate (K/min) 2.3.4.9.3.
Initial hold (min)  2.2.3. 
Final hold (min)  70.2.3. 
I 1480.1469.1451.1477.1477.
ReferenceScrivanti, Anton, et al., 2009Shimizu, Imayoshi, et al., 2009Su, Wang, et al., 2009Aicha, Ines, et al., 2008Baziou, Couladis, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52HP-5SLB-5 MSElite-1HP-5 MS
Column length (m) 50.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.100.50.60.50.
Tend (C) 280.240.250.246.240.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min)  2.2.  
Final hold (min) 20.5.10.  
I 1500.1477.1475.1472.1515.
ReferenceDjarri, Medjroubi, et al., 2008Lago, Romoff, et al., 2008Lo Presti, Sciarrone, et al., 2008Raj, Baby, et al., 2008Sarikurkcu, Tepe, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5OV-1HP-5HP-5 MSCP Sil 5 CB
Column length (m) 20.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.180.250.250.250.32
Phase thickness (mum) 0.200.250.320.250.25
Tstart (C) 50.65.60.50.60.
Tend (C) 280.260.250.230.300.
Heat rate (K/min) 4.6.5.3.4.
Initial hold (min) 1. 30.10. 
Final hold (min)    10. 
I 1490.1527.1477.1477.1472.
ReferenceSkalicka-Wozniak, Los, et al., 2008Wang, Yi, et al., 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Baran, von Reuss, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1Col-Elite 5MSHP-1
Column length (m) 30.30.60.30.30.
Carrier gas HeHeliumNitrogenHeHe
Substrate      
Column diameter (mm) 0.260.260.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.30.60.
Tend (C) 240.290.250.246.240.
Heat rate (K/min) 3.3.4.3.2.
Initial hold (min)   1.  
Final hold (min)   10. 20.
I 1472.1472.1480.1496.1463.
ReferenceBos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Ghasempour, Shirinpour, et al., 2007Gudaityte and Venskutonis R.P., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSZB-5DB-5DB-1SPB-1
Column length (m) 30.30.30.50.30.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 45.60.60.95.70.
Tend (C) 210.220.300.240.220.
Heat rate (K/min) 3.4.3.4.3.
Initial hold (min)  5.   
Final hold (min)  20.  15.
I 1478.1477.1445.1465.1464.
ReferenceHudaib and Aburjai, 2007Mohottalage, Tabacchi, et al., 2007Moreno, Lima, et al., 2007Pala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5DB-5DB-5
Column length (m) 30.60.30.30.30.
Carrier gas HydrogenNitrogenHeliumHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.40.
Tend (C) 250.250.260.320.210.
Heat rate (K/min) 4.4.4.10.2.
Initial hold (min)  1.   
Final hold (min)  10. 4.33.
I 1474.1480.1472.1473.1479.
ReferencePontes, de Olivera, et al., 2007Reza, Ebrahim, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Smelcerovic, Spiteller, et al., 2007Sylvestre, Longtin, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSHP-5 MSHP-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHe He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.50.250.250.250.32
Tstart (C) 40.60.40.40.60.
Tend (C) 280.280.250.240.250.
Heat rate (K/min) 4.3.3.5.5.
Initial hold (min) 5. 5.3.30.
Final hold (min) 10. 10.10. 
I 1478.1480.1454.1473.1477.
ReferenceTava, Pecetti, et al., 2007Vagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Wenguang, Wenlai, et al., 2007Yassa and Akhani, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5BP-1HP-1
Column length (m) 30.30.60.50.50.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.250.250.220.2
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.60.60.60.60.
Tend (C) 300.300.250.220.250.
Heat rate (K/min) 3.3.3.2.2.
Initial hold (min)     4.
Final hold (min)    20.30.
I 1472.1469.1485.1472.1470.
ReferenceApel, Sobral, et al., 2006Apel, Sobral, et al., 2006, 2Bertrand, Comte, et al., 2006Boti, Yao, et al., 2006Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1SPB-1DB-5
Column length (m) 50.50.50.30.30.
Carrier gas HeHeHeHeliumHelium
Substrate      
Column diameter (mm) 0.20.20.20.200.26
Phase thickness (mum) 0.330.330.330.200.25
Tstart (C) 60.60.60.70.60.
Tend (C) 250.250.250.220.290.
Heat rate (K/min) 2.2.2.3.3.
Initial hold (min) 4.4.4.  
Final hold (min) 30.30.30.15. 
I 1466.1474.1475.1464.1472.
ReferenceCastel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006, 2Cavaleiro, Pinto, et al., 2006Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5HP-1DB-5DB-5
Column length (m) 50.30.50.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.20.250.20.250.25
Phase thickness (mum) 0.330.250.330.250.25
Tstart (C) 60.50.60.40.50.
Tend (C) 250.300.250.210.250.
Heat rate (K/min) 2.5.2.2.3.
Initial hold (min)  5. 2. 
Final hold (min) 60.5.40.33.10.
I 1488.1474.1465.1479.1477.
ReferenceFernandez, Pintaric, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Garneau F.X., Collin G., et al., 2006Havlik, Kokoska, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1DB-5DB-5CP-Sil 5 CB
Column length (m) 30.50.30.30.25.
Carrier gas HeliumHeHeHeHydrogen
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 60.60.60.60.50.
Tend (C) 260.220.220.220.230.
Heat rate (K/min) 3.2.4.4.3.
Initial hold (min)    5. 
Final hold (min)  20.   
I 1473.1472.1482.1484.1477.
ReferenceJavidnia, Miri, et al., 2006Lesueur, Ban, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani K., Akbarzadeh M., et al., 2006Olawore, Usman, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5DB-1DB-5DB-5
Column length (m) 30.25.50.30.30.
Carrier gas HeN2N2HydrogenHydrogen
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.250.150.250.250.25
Tstart (C) 50.50.95.70.70.
Tend (C) 250.200.240.280.280.
Heat rate (K/min) 2.4.4.4.4.
Initial hold (min)  3. 4.4.
Final hold (min)      
I 1472.1477.1463.1477.1477.
ReferenceOrav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5CP Sil 5 CBSPB-5
Column length (m) 30.25.30.25.60.
Carrier gas HeH2HeH2He
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum) 0.250.250.25 1.
Tstart (C) 60.60.60.50.40.
Tend (C) 280.240.260.230.230.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)     5.
Final hold (min)     2.
I 1445.1480.1486.1480.1507.
ReferencePitarokili, Tzakou, et al., 2006Potzernheim, Bizzo, et al., 2006Sabulal, Dan, et al., 2006Tesso, König, et al., 2006Tornambe, Cornu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.250.210.240.240.
Heat rate (K/min) 3.10.3.3.3.
Initial hold (min)  2.5.  
Final hold (min)  10.   
I 1450.1494.1474.1477.1477.
ReferenceTzakou, Said, et al., 2006Wang, Yang, et al., 2006Askari and Sefidkon, 2005Chaverri and Cicció, 2005Chaverri and Cicció, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5Polymethylsiloxane, (PMS-20000)HP-5DB-5HP-1
Column length (m) 25.25.25.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.220.200.20.250.2
Phase thickness (mum) 0.25 0.330.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 320.250.240.300.250.
Heat rate (K/min) 5.3.3.3.2.
Initial hold (min) 5.3. 3.60.
Final hold (min)   7.  
I 1480.1489.1477.1472.1483.
ReferenceDickschat, Martens, et al., 2005Dohou, Yamni, et al., 2005Duarte, Figueira, et al., 2005Ferraz, Limberger, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5MSHP-5DB-5
Column length (m) 30.30.25.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.60.50.30.60.
Tend (C) 300.200.250.260.230.
Heat rate (K/min) 5.4.3.2.3.
Initial hold (min) 5.30.3.2. 
Final hold (min) 5. 10.28. 
I 1474.1466.1476.1482.01466.
ReferenceFiguérédo, Cabassu, et al., 2005Gauvin and Smadja, 2005Ghasemi Y., Faridi P., et al., 2005Leffingwell and Alford, 2005Limberger, Sobral, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-1HP-5MSDB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.60.95.60.40.
Tend (C) 280.220.240.280.260.
Heat rate (K/min) 3.4.4.3.2.
Initial hold (min) 30.4.  5.
Final hold (min)     20.
I 1449.1480.1465.1480.1480.
ReferenceMarongiu, Piras, et al., 2005Morteza-Semnani and Saeedi, 2005Pala-Paul, Perez-Alonso, et al., 2005Petrakis, Roussis, et al., 2005Senatore, Apostolides Arnold, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSDB-1DB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.300.280.250.280.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min) 5.    
Final hold (min)    10. 
I 1476.1470.1475.1475.1440.
ReferenceSetzer, Noletto, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Slavkovska, Couladis, et al., 2005Sonboli, Salehi, et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-5BP-1DB-1
Column length (m) 50.30.30.50.30.
Carrier gas   H2 N2
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.50.60.50.
Tend (C) 240.220.290.220.200.
Heat rate (K/min) 3.3.4.2.5.
Initial hold (min)  5.   
Final hold (min)  10. 20. 
I 1450.1454.1465.1471.1481.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2005Vichi, Riu-Aumatell, et al., 2005Abreu, Reis, et al., 2004Blanc, Muselli, et al., 2004Fekam Boyom, Fotio, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5HP-5MSDB-5MSNB-30
Column length (m) 30.30.30.30.50.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 300.300.280.280.250.
Heat rate (K/min) 4.3.3.3.2.
Initial hold (min)      
Final hold (min)    30. 
I 1473.1460.1474.1444.1482.
ReferenceKalemba and Thiem, 2004Limberger, Sobral, et al., 2004Malencic, Couladis, et al., 2004Marongiu, Porcedda, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 8 CBDB-5HTDB-1
Column length (m) 30.30.30.27.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.60.50.50.50.
Tend (C) 240.300.200.250.250.
Heat rate (K/min) 3.3.5.2.4.
Initial hold (min)   5.2. 
Final hold (min)    20. 
I 1473.1480.1481.1477.1472.
ReferenceTellez, Khan, et al., 2004Tirillini, Pellegrino, et al., 2004Wang, Guo, et al., 2004Yusufoglu, Celik, et al., 2004Dabiri and Sefidkon, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1RSL-200RSL-200CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeN2H2H2He
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.250.250.250.39
Tstart (C) 60.50.40.40.60.
Tend (C) 220.200.280.280.220.
Heat rate (K/min) 5.5.6.6.5.
Initial hold (min) 20. 5.5. 
Final hold (min) 20. 5.5. 
I 1485.1455.1473.1484.1473.
ReferenceFeizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Ngouana, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Khanavi, Hadjiakhoondi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.240.280.280.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min)   30.30.30.
I 1477.1478.1464.1470.1468.
ReferenceLimberger, Simões-Pires, et al., 2003Maia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003Marongiu, Porcedda, et al., 2003Marongiu, Porcedda, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5DB-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeN2He He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.95.60.40.60.
Tend (C) 275.240.280.260.240.
Heat rate (K/min) 4.4.3.2.3.
Initial hold (min) 5.  5. 
Final hold (min)      
I 1477.1469.1457.1465.1475.
ReferenceMorteza-Semnani and Saeedi, 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pitarokili, Tzakou, et al., 2003Senatore and Bruno, 2003da Silva, Luz, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Cross-Linked MethylsiliconeHP-5HP-5HP-5HP-5
Column length (m) 25.25.25.25.25.
Carrier gas HeH2H2HeliumHelium
Substrate      
Column diameter (mm) 0.20.320.320.320.32
Phase thickness (mum) 0.330.530.530.530.53
Tstart (C) 70.40.40.40.40.
Tend (C) 250.280.280.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min)      
Final hold (min)      
I 1450.1472.1480.1473.1473.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5DB-5
Column length (m) 25.25.25.30.25.
Carrier gas HeliumHeliumHeliumHeN2
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.530.530.530.250.25
Tstart (C) 40.40.40.60.50.
Tend (C) 280.280.280.240.250.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min)      
Final hold (min)     10.
I 1473.1474.1480.1478.1477.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Zoghbi, Andrade, et al., 2003Zrira, Elamrani, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5MSBP-1DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.500.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.280.220.240.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)      
Final hold (min) 30.  10. 
I 1470.1477.1477.1471.1480.
ReferenceCaredda, Marongiu, et al., 2002Congiu, Falconieri, et al., 2002Congiu, Falconieri, et al., 2002Das, Ram, et al., 2002Flamini, Ertugrul, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PTE-5SE-30RSL-200CP Sil 8 CBDB-5
Column length (m) 60.50.30.30.30.
Carrier gas H2HeH2HeHe
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (mum) 0.300.250.250.250.25
Tstart (C) 60.70.40.50.60.
Tend (C) 285.240.280.220.240.
Heat rate (K/min) 4.34.6.3.3.
Initial hold (min)   5.2. 
Final hold (min)   5.  
I 1477.1469.1475.1478.1477.
ReferenceGudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002Juteau, Masotti, et al., 2002Kobaisy, Tellez, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.230.250.25
Phase thickness (mum) 0.250.250.150.250.25
Tstart (C) 60.35.50.60.60.
Tend (C) 150.280.250.240.220.
Heat rate (K/min) 1.3.3.3.4.
Initial hold (min) 3.2.  5.
Final hold (min)  15.   
I 1468.1482.1473.1477.1480.
ReferenceKovacevic and Kac, 2002Krauze-Baranowska, Mardarowicz, et al., 2002Mahmout, Bessière, et al., 2002Maia, da Silva, et al., 2002Morteza-Semnani, Saeedi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5DB-5DB-1DB-1
Column length (m) 30.30.25.60.60.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 60.60.60.40.40.
Tend (C) 250.250.220.250.280.
Heat rate (K/min) 4.4.3.4.4.
Initial hold (min) 10.2.  5.
Final hold (min)  20.   
I 1481.1477.1480.1469.1468.
ReferenceNorouzi-Arasi, Yavari, et al., 2002Pino, Marbot, et al., 2002Schwob, Bessière, et al., 2002Sefidkon, Dabiri, et al., 2002Sefidkon, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5MSDB-5DB-1
Column length (m) 50.30.30.30.60.
Carrier gas N2H2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.40.
Tend (C) 240.280.270.240.280.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)     5.
Final hold (min)      
I 1450.1477.1480.1479.1446.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2002Velickovic, Randjelovic, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Dabiri and Sefidkon, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5BP-1RTX-1
Column length (m) 60.30.30.30.30.
Carrier gas HeN2N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.220.220.220.300.
Heat rate (K/min) 4.5.5.5.4.
Initial hold (min) 5.10.10.  
Final hold (min)      
I 1455.1477.1477.1473.1471.
ReferenceDabiri and Sefidkon, 2001Flamini, Cioni, et al., 2001Gallori, Flamini, et al., 2001Gupta, Mallavarapu, et al., 2001Kalemba, Marschall, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1RTX-5DB-5MSOV-101DB-5
Column length (m) 25.30.30.50.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.20.25
Phase thickness (mum) 0.110.250.250.50.25
Tstart (C) 60.60.60.50.60.
Tend (C) 190.150.240.250.270.
Heat rate (K/min) 2.51.3.2.3.
Initial hold (min) 3.3.   
Final hold (min) 1. 30.  
I 1459.1468.1443.1474.1480.
ReferenceKovacevic and Kac, 2001Kovacevic and Kac, 2001Marongiu, Porcedda, et al., 2001Orav, Kailas, et al., 2001Palmeira, Conserva, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101OV-101DB-1HP-5
Column length (m) 30.50.50.60.30.
Carrier gas HeN2N2N2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25  0.250.25
Tstart (C) 60.80.80.60.40.
Tend (C) 240.200.200.220.280.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min)    5.10.
Final hold (min)    22.10.
I 1476.1479.1479.1496.1474.
ReferenceTellez M., Estell R., et al., 2001Yang, 2001Yang, 2001, 2Bailac, Dellacasa, et al., 2000Bicalho, Pereira, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-1DB-5DB-5
Column length (m) 60.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.60.
Tend (C) 200.240.280.220.240.
Heat rate (K/min) 4.3.4.4.3.
Initial hold (min) 5. 5.5. 
Final hold (min) 25.    
I 1484.1477.1474.1474.1476.
ReferenceMeccia, Rojas, et al., 2000Tellez, Dayan, et al., 2000Sefidkon, Dabiri, et al., 1999Sefidkon and Khajavi, 1999Tellez, Canel, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SPB-5DB-5DB-5HP-1
Column length (m) 50.50.30.30.60.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.220.320.250.250.25
Phase thickness (mum) 1.0.250.250.250.25
Tstart (C) 100.60.60.60.50.
Tend (C) 220.240.240.240.280.
Heat rate (K/min) 1.3.3.3.4.
Initial hold (min) 1.   5.
Final hold (min)  20.   
I 1474.1484.1478.1477.1494.
ReferenceCamciuc, Bessière, et al., 1998Doneanu and Anitescu, 1998Maia, Zohhbi, et al., 1998Santos, Andrade, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5OV-1DB-1DB-5
Column length (m) 25.30.30. 30.
Carrier gas  He  Helium
Substrate      
Column diameter (mm) 0.320.250.32 0.25
Phase thickness (mum)  0.250.25 0.25
Tstart (C) 50.65.40.80.60.
Tend (C) 200.300.270.220.240.
Heat rate (K/min) 5.4.2.6.3.
Initial hold (min)  2.4.  
Final hold (min)      
I 1475.1487.1497.1469.1476.
ReferenceZollo, Biyiti, et al., 1998Elias, Simoneit, et al., 1997Kökdil, Tanker, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-1HP-1
Column length (m) 30.30.50.60.25.
Carrier gas He HeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum)  0.25 0.500.25
Tstart (C) 60.60.50.50.60.
Tend (C) 240.300.250.250.220.
Heat rate (K/min) 4.4.2.8.4.
Initial hold (min)  2. 1.2.
Final hold (min)  5. 6.20.
I 1471.1473.31471.1490.1466.
ReferenceZunino, Novillo-Newton, et al., 1997Gawdzik, Mardarowicz, et al., 1996Orav, Kailas, et al., 1996Sagrero-Nieves and Bartley, 1996Thanh, Dung, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Methyl SiliconeMethyl SiliconeCP Sil 5 CBOV-101
Column length (m) 60.50.50.25.52.
Carrier gas HeN2N2 Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.26
Phase thickness (mum) 0.250.170.17  
Tstart (C) 50.80.80.60.40.
Tend (C) 250.200.200.280.200.
Heat rate (K/min) 3.52.3.5.3.
Initial hold (min) 5.   0.
Final hold (min)     0.
I 1492.1486.1489.1475.1481.
ReferenceStashenko, Torres, et al., 1995Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Tkachenko and Zenkevich, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-1OV-101OV-101OV-101
Column length (m) 30.60.50.50.50.
Carrier gas Hydrogen N2N2N2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.25    
Tstart (C) 60.50.80.80.80.
Tend (C) 250.230.200.200.200.
Heat rate (K/min) 2.4.2.2.2.
Initial hold (min) 5.    
Final hold (min) 2.10.   
I 1470.1469.1475.1480.1475.
ReferenceKollmannsberger, Nitz, et al., 1992Binder, Benson, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Sugisawa, Yang, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1OV-101OV-101
Column length (m) 50.60.60.50.50.
Carrier gas N2HeHe  
Substrate      
Column diameter (mm) 0.250.320.320.300.30
Phase thickness (mum)      
Tstart (C) 80.30.30.40.40.
Tend (C) 200.210.210.230.230.
Heat rate (K/min) 2.2.2.3.53.5
Initial hold (min)  4.4.5.5.
Final hold (min)      
I 1480.1464.1465.1485.1498.
ReferenceSugisawa, Yang, et al., 1989Takeoka and Butter, 1989Takeoka and Butter, 1989Nykanen, 1986Nykanen, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-3
Column length (m) 150.
Carrier gas  
Substrate  
Column diameter (mm) 0.66
Phase thickness (mum)  
Tstart (C) 20.
Tend (C) 170.
Heat rate (K/min) 1.
Initial hold (min)  
Final hold (min)  
I 1470.
ReferenceButtery, Xu, et al., 1985
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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