γ-Muurolene


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxHP-InnowaxBP-20Supelcowax-10DB-Wax
Column length (m) 60.60. 30.30.
Carrier gas HeliumHeliumNitrogenHeliumHydrogen
Substrate      
Column diameter (mm) 0.220.25 0.200.25
Phase thickness (μm) 0.250.25 0.200.25
Tstart (C) 60.60.60.70.30.
Tend (C) 230.220.200.220.230.
Heat rate (K/min) 2.5.5.3.8.
Initial hold (min)  1.  5.
Final hold (min) 5.5. 15.10.
I 1667.1692.1692.1678.1689.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Feng, Cui, et al., 2011Mishra, Chaudhary, et al., 2010Neves, Rosa, et al., 2010Karlsson, Birgersson, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxDB-WaxHP-InnowaxCP-Wax 52CBTC-FFAP
Column length (m) 60.60.30.30. 
Carrier gas HeliumHeliumHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.40.60.
Tend (C) 230.220.240.220.220.
Heat rate (K/min) 2.3.2.3.3.
Initial hold (min)  2. 1. 
Final hold (min) 30.70.20.2.30.
I 1664.1695.1693.1701.1687.
ReferenceMuseli, Pau, et al., 2009Shimizu, Imayoshi, et al., 2009Hachicha, Skanji, et al., 2007Hymete, Rohloff, et al., 2007Kurose, Okamura, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-FFAPDB-WaxSupelcowax-10Supelcowax-10Supelcowax-10
Column length (m)  60.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.320.20.250.25
Phase thickness (μm) 0.250.250.20.250.25
Tstart (C) 60.70.70.40.40.
Tend (C) 220.220.220.210.250.
Heat rate (K/min) 3.4.3.2.3.
Initial hold (min)     5.
Final hold (min) 30. 15.33.10.
I 1685.1675.1683.1690.1723.
ReferenceKurose, Okamura, et al., 2007Pala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007Sylvestre, Longtin, et al., 2007Vichi, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20Supelcowax 10Supelcowax-10DB-WaxBP-20
Column length (m) 50.30.30.30.50.
Carrier gas  Helium HeHe
Substrate      
Column diameter (mm) 0.220.200.250.250.22
Phase thickness (μm) 0.250.200.250.250.25
Tstart (C) 60.70.40.50.60.
Tend (C) 220.220.210.250.220.
Heat rate (K/min) 2.3.2.3.2.
Initial hold (min)   2.  
Final hold (min) 20.15.33.10.20.
I 1683.1683.1690.1692.1685.
ReferenceBoti, Yao, et al., 2006Cavaleiro, Pinto, et al., 2006Garneau F.X., Collin G., et al., 2006Havlik, Kokoska, et al., 2006Lesueur, Ban, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-20MSupelcowax-10Carbowax 20MSupelcowaxSupelcowax-10
Column length (m) 30.30.50.60.30.
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.20.250.20.20.25
Phase thickness (μm) 0.250.250.250.20.25
Tstart (C) 50.50.60.60.40.
Tend (C) 250.220.250.230.220.
Heat rate (K/min) 2.4.2.4.3.
Initial hold (min)  1.60.30.5.
Final hold (min)  10.  10.
I 1685.1680.1652.1668.1723.
ReferenceOrav, Raal, et al., 2006Wong, Lim, et al., 2006Fernandez, Lizzani-Cuvelier, et al., 2005Gauvin and Smadja, 2005Vichi, Riu-Aumatell, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20Innowax FSCSupelcowax-10InnowaxHP-Innowax
Column length (m) 50.60.50.60.50.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm) 0.220.250.20.250.2
Phase thickness (μm) 0.25 0.25 0.2
Tstart (C) 60.60.70.60.70.
Tend (C) 220.220.230.220.190.
Heat rate (K/min) 2.4.2.4.5.
Initial hold (min)  10. 10. 
Final hold (min) 20.  10. 
I 1677.1704.1688.1704.1698.
ReferenceBlanc, Muselli, et al., 2004Lourens, Reddy, et al., 2004Orav, Stulova, et al., 2004Suleimenov, Atazharova, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxDB-WaxPEG-20MCarbowax 20MCarbowax 20M
Column length (m) 60.60.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.220.22
Phase thickness (μm) 0.50.25 0.250.25
Tstart (C) 40.45.70.60.60.
Tend (C) 180.240.250.220.220.
Heat rate (K/min) 5.3.2.2.2.
Initial hold (min) 5.    
Final hold (min) 20.    
I 1729.1689.1693.1695.1710.
ReferenceGalindo-Cuspinera, Lubran, et al., 2002Christoph, 2001Orav, Kailas, et al., 2001Vernin, Lageot, et al., 2001Vernin, Lageot, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxHP Innowax FSPInnowaxHP-Innowax
Column length (m) 60.60.60.60.60.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.60.
Tend (C) 230.200.220.220.220.
Heat rate (K/min) 5.2.   
Initial hold (min) 2.2.10.10.10.
Final hold (min)   10.  
I 1685.1679.1704.1704.1704.
ReferencePaniandy, Chane-Ming, et al., 2000Umano, Hagi, et al., 2000Kaya, Baser, et al., 1999Kaya, Baser, et al., 1999, 2Kaya, Baser, et al., 1999, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxNB-351DB-WaxDB-WaxHP-Innowax
Column length (m) 60.25.30.30.60.
Carrier gas HeH2N2N2He
Substrate      
Column diameter (mm) 0.250.30.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 60.70.45.45.50.
Tend (C) 240.250.220.220.220.
Heat rate (K/min) 4.5.3.3.5.
Initial hold (min)  2.  5.
Final hold (min)      
I 1698.1692.1720.1701.1676.
ReferenceNgassoum, Yonkeu, et al., 1999Onocha, Ekundayo, et al., 1999Molleken U., Sinnwell V., et al., 1998Mölleken, Sinnwell, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCSupelcowax-10PEG-20MDB-WaxDB-Wax
Column length (m) 60.30.50.60.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.25  0.500.25
Tstart (C) 60.60.70.50.50.
Tend (C) 220.240.250.250.180.
Heat rate (K/min) 4.4.2.8.2.5
Initial hold (min) 10.  1.5.
Final hold (min) 10.  6. 
I 1700.1711.1693.1691.1655.
ReferenceTümen, Baser, et al., 1998Zunino, Novillo-Newton, et al., 1997Orav, Kailas, et al., 1996Sagrero-Nieves and Bartley, 1996Stashenko, Torres, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxFFAPCarbowax 20MDB-Wax
Column length (m) 45.60.50.50.60.
Carrier gas Hydrogen  H2He
Substrate      
Column diameter (mm) 0.320.32 0.320.32
Phase thickness (μm) 1.0  0.150.25
Tstart (C) 60.50.50.70.30.
Tend (C) 200.230.180.210.180.
Heat rate (K/min) 2.4.10.2.2.
Initial hold (min) 5. 1. 4.
Final hold (min)  10.   
I 1669.1683.1710.1666.1664.
ReferenceKollmannsberger, Nitz, et al., 1992Binder, Benson, et al., 1990Brophy, Davies, et al., 1989Gaydou, Faure, et al., 1989Takeoka and Butter, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Supelcowax-10Carbowax 20MCarbowax 20M
Column length (m) 60.30.30.150.150.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.32  0.660.64
Phase thickness (μm) 0.25    
Tstart (C) 30.50.50.60.50.
Tend (C) 180.240.240.170.170.
Heat rate (K/min) 2.4.4.1.1.
Initial hold (min) 4.2.2.40.30.
Final hold (min)  10.10.  
I 1665.1691.1691.1655.1655.
ReferenceTakeoka and Butter, 1989Ramaswami, Briscese, et al., 1988Ramaswami, Briscese, et al., 1986Buttery, Xu, et al., 1985Buttery, Parker, et al., 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
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Galindo-Cuspinera, Lubran, et al., 2002
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Christoph, 2001
Christoph, F., Chemische Zuzammensetzung und antimikrobielle Eigenschaften der ätherischen Öle von Leptospermum scoparium J. R. et G. Forst. und anderer Teebaumöle der Gattungen Kunzea, Leptospermum und Melaleuca unter besonderer Berücksichtigung von Handelsölen, Dissertation, University of Hamburg, Germany, 2001, 196. [all data]

Orav, Kailas, et al., 2001
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Vernin, Lageot, et al., 2001
Vernin, G.; Lageot, C.; Gaydou, E.M.; Parkanyi, C., Analysis of the essential oil of Lippia graveolens HBK from El Salvador, Flavour Fragr. J., 2001, 16, 3, 219-226, https://doi.org/10.1002/ffj.984 . [all data]

Paniandy, Chane-Ming, et al., 2000
Paniandy, J.-C.; Chane-Ming, J.; Pierbattesti, J.-C., Chemical Composition of the Essential Oil and Headspace Solid-Phase Microextraction of the Guava Fruit (Psidium guajava L.), J. Essent. Oil Res., 2000, 12, 153-158. [all data]

Umano, Hagi, et al., 2000
Umano, K.; Hagi, Y.; Nakahara, K.; Shoji, A.; Shibamoto, T., Volatile chemicals identified in extracts from leaves of Japanese mugwort (Artemisia princeps Pamp.), J. Agric. Food Chem., 2000, 48, 8, 3463-3469, https://doi.org/10.1021/jf0001738 . [all data]

Kaya, Baser, et al., 1999
Kaya, A.; Baser, K.H.C.; Koca, F., Essential oils of Acinos troodi (Post) Leblebici subsp. vardaranus Leblebici and subsp. grandiflorus Hartvig Strid, Flavour Fragr. J., 1999, 14, 1, 50-54, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<50::AID-FFJ783>3.0.CO;2-7 . [all data]

Kaya, Baser, et al., 1999, 2
Kaya, A.; Baser, K.H.C.; Demirci, B.; Koca, F., The essential oil of Acinos alpinus (L.) Moench growing in Turkey, Flavour Fragr. J., 1999, 14, 1, 55-59, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<55::AID-FFJ784>3.0.CO;2-Q . [all data]

Kaya, Baser, et al., 1999, 3
Kaya, A.; Baser, K.H.C.; Tümen, G.; Koca, F., The essential oil of Acinos suaveolens (Sm.) G. Don fil. Acinos arvensis (Lam.) Dandy and Acinos rotundifolius Pers. growing wild in Turkey, Flavour Fragr. J., 1999, 14, 1, 60-64, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<60::AID-FFJ785>3.0.CO;2-0 . [all data]

Ngassoum, Yonkeu, et al., 1999
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Notes

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