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Ephedrine


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedCapillaryCapillaryCapillaryPacked
Active phase SE-30DB-1DB-5BP-1OV-1
Column length (m) 2.30.15.12.2.
Carrier gas NitrogenHeHeHe 
Substrate Chromosorb G AW DMCS (80-100 mesh)   Gas Chrom P
Column diameter (mm)  0.250.250.22 
Phase thickness (mum)  0.250.20.25 
Tstart (C) 100.40.100.120.120.
Tend (C) 300.250.150.280.200.
Heat rate (K/min)  25.10.8.2.5
Initial hold (min)  2.   
Final hold (min)  5.   
I 1363.1363.1339.1350.1350.
ReferenceMHA, 9999Yashiki, Kojima, et al., 1995Phillips, Logan, et al., 1990Stowell and Wilson, 1985Marozzi, Gambaro, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase SE-30SE-30SE-30
Column length (m) 2.2.2.
Carrier gas  NitrogenN2
Substrate Gas Chrom PChromosorb W AW DMS (80-100 mesh)Chromosorb W AW DMS
Column diameter (mm)    
Phase thickness (mum)    
Tstart (C) 120.130.130.
Tend (C) 200.290.290.
Heat rate (K/min) 2.58.8.
Initial hold (min)  2.2.
Final hold (min)  8.8.
I 1370.1370.1370.
ReferenceMarozzi, Gambaro, et al., 1982Peel and Perrigo, 1976Peel and Perrigo, 1975
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Yashiki, Kojima, et al., 1995
Yashiki, M.; Kojima, T.; Miyazaki, T.; Nagasawa, N.; Iwasaki, Y.; Hara, K., Detection of amphetamines in urine using head space-solid phase microextraction and chemical ionization selected ion monitoring, Forensic Sci. Int., 1995, 76, 3, 169-177, https://doi.org/10.1016/0379-0738(95)01819-0 . [all data]

Phillips, Logan, et al., 1990
Phillips, A.M.; Logan, B.K.; Stafford, D.T., Further applications for capillary gas chromatography in routine quantitative toxicological analyses, J. Hi. Res. Chromatogr., 1990, 13, 11, 754-758, https://doi.org/10.1002/jhrc.1240131106 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]

Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can. Soc. Forens. Sci. J., 1976, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]

Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]


Notes

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