γ-Elemene


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5 MSDB-5
Column length (m) 30.25.30.30.50.
Carrier gas HeliumNitrogenHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.220.250.250.20
Phase thickness (μm) 0.250.250.320.250.32
Tstart (C) 60.50.60.50.60.
Tend (C) 240.300.250.230.220.
Heat rate (K/min) 3.6.55.3.5.
Initial hold (min)  2.30.10.3.
Final hold (min)  7. 10.5.
I 1437.1426.1431.1434.1431.
ReferenceAlim, Goze, et al., 2009Chieng, Assim, et al., 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Amiri, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5ZB-5HP-5MSHP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas Helium HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.260.250.250.320.25
Tstart (C) 60.60.40.60.40.
Tend (C) 240.220.250.250.260.
Heat rate (K/min) 4.4.3.5.4.
Initial hold (min) 2.5.5.30. 
Final hold (min) 20.20.10.  
I 1438.1430.1421.1431.1429.5
ReferenceFarsam, Amanlou, et al., 2007Mohottalage, Tabacchi, et al., 2007Vichi, Riu-Aumatell, et al., 2007Yassa and Akhani, 2007Zizovic, Stamenic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5CP Sil 5 CBSPB-1
Column length (m) 30.25.30.25.30.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.150.25 0.25
Tstart (C) 60.50.60.50.50.
Tend (C) 220.200.200.230.250.
Heat rate (K/min) 4.4.2.3.4.
Initial hold (min) 5.3.  1.
Final hold (min)   60. 10.
I 1439.1430.1433.1431.1417.
ReferenceMorteza-Semnani K., Akbarzadeh M., et al., 2006Ouamba, Ouabonzi, et al., 2006Rout, Naik, et al., 2006Tesso, König, et al., 2006Wong, Sivasothy, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5SPB-5DB-5
Column length (m) 30.25.30.60.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.150.251.0.25
Tstart (C) 60.40.60.40.60.
Tend (C) 275.220.240.230.300.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)  5. 5.3.
Final hold (min)      
I 1440.1427.1435.1473.1428.
ReferenceAsadipour, Mehrabani, et al., 2005Chagonda and Chalchat, 2005Chaverri and Cicció, 2005Cornu, Kondjoyan, et al., 2005Ferraz, Limberger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1RTX-5 MSHP-5MS
Column length (m) 25.30.50.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.32
Tstart (C) 50.60.95.50.60.
Tend (C) 250.220.240.280.250.
Heat rate (K/min) 3.4.4.8.5.
Initial hold (min) 3.4. 2.3.
Final hold (min) 10.  2. 
I 1434.1439.1429.1442.1436.
ReferenceGhasemi Y., Faridi P., et al., 2005Morteza-Semnani and Saeedi, 2005Pala-Paul, Perez-Alonso, et al., 2005Pellati, Benvenuti, et al., 2005Pourmortazavi, Ghadiri, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSDB-1DB-1
Column length (m) 30.50.30.50.30.
Carrier gas HeN2 N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.90.40.95.50.
Tend (C) 265.240.220.240.265.
Heat rate (K/min) 2.54.3.4.2.5
Initial hold (min) 1. 5. 1.
Final hold (min) 20. 10. 20.
I 1415.1423.1421.1423.1415.
ReferenceSarkhail, Amin, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Vichi, Riu-Aumatell, et al., 2005Palá-Paúl, Velasco-Negueruela, et al., 2004Sarkhail, Amin, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 280.280.210.275.280.
Heat rate (K/min) 4.3.2.4.4.
Initial hold (min)    5. 
Final hold (min)  30.60.  
I 1433.1420.1433.1433.1432.
ReferenceGhasemi, Asghari, et al., 2003Marongiu, Porcedda, et al., 2003Mookdasanit, Tamura, et al., 2003Morteza-Semnani and Saeedi, 2003Sajjadi and Mehregan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-55 % Phenyl methyl siloxaneRSL-200DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.23
Phase thickness (μm) 0.320.250.250.250.20
Tstart (C) 60.60.75.40.50.
Tend (C) 250.240.200.280.200.
Heat rate (K/min) 5.3.3.6.3.
Initial hold (min) 30. 4.5.3.
Final hold (min)   8.5.30.
I 1436.1430.1437.1425.1446.
ReferenceYassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003Cicció and Gómez-Laurito, 2002Jirovetz, Buchbauer, et al., 2002Khallouki, Younos, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101DB-5MSRTX-1DB-1
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.20.250.250.2
Phase thickness (μm) 0.250.50.250.25 
Tstart (C) 60.50.60.60.60.
Tend (C) 240.250.270.300.240.
Heat rate (K/min) 3.2.3.4.3.
Initial hold (min)      
Final hold (min)      
I 1433.1423.1432.1427.1435.5
ReferenceKobaisy, Tellez, et al., 2002Orav, Kailas, et al., 2002Zoghbi, Andrade, et al., 2002Kalemba, Marschall, et al., 2001Santos, Moreira, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBDB-1HP-1CP Sil 5 CB
Column length (m) 60.25.33.60.25.
Carrier gas N2HeN2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.40.500.250.25
Tstart (C) 60.60.50.60.50.
Tend (C) 220.260.135.200.290.
Heat rate (K/min) 3.5.20.4.4.
Initial hold (min) 5.40.2.5. 
Final hold (min) 22.  25. 
I 1440.1425.1442.1438.1482.
ReferenceBailac, Dellacasa, et al., 2000Baser, Özek, et al., 2000Feger, Brandauer, et al., 2000Meccia, Rojas, et al., 2000Bos, Woerdenbag, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBOV-1HP-5SE-54
Column length (m) 25.25.30. 30.
Carrier gas N2He  Hydrogen
Substrate      
Column diameter (mm) 0.320.250.32 0.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.60.40.35.60.
Tend (C) 290.300.270.200.250.
Heat rate (K/min) 4.6.2.6.2.
Initial hold (min)   4.2.5.
Final hold (min)     2.
I 1482.1482.1475.1458.1430.
ReferenceBos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Kökdil, Tanker, et al., 1997Larsen and Frisvad, 1995Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SE-30SE-30
Column length (m) 30.30.
Carrier gas   
Substrate   
Column diameter (mm)   
Phase thickness (μm)   
Tstart (C) 50.50.
Tend (C) 240.240.
Heat rate (K/min) 4.4.
Initial hold (min) 2.2.
Final hold (min) 10.10.
I 1425.1425.
ReferenceRamaswami, Briscese, et al., 1988Ramaswami, Briscese, et al., 1986
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Alim, Goze, et al., 2009
Alim, A.; Goze, I.; Cetin, A.; Atas, A.; Vural, N.; Donmez, E., Antimicrobial activity of the essential oil of Cyclotrichimun niveum (Boiss.) Manden. Et Scheng, African J. Microbiol. Res., 2009, 3, 8, 422-425. [all data]

Chieng, Assim, et al., 2008
Chieng, T.C.; Assim, Z.B.; Fasihuddin, B.A., Toxicity and antitermite activities of the essential oils from Piper sarmentosum, The Malaysian J. Anal. Sci., 2008, 12, 1, 234-239. [all data]

Yassa and Akhani, 2008
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2008, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Amiri, 2007
Amiri, H., Quantative and qualative changes of essential oil of Salvia bracteata BAnk et Sol. in different growth stages, DARU, 2007, 15, 2, 79-82. [all data]

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Farsam, H.; Amanlou, M.; Taghi-Cheetsaz, N.; Amin, G.R.; Saledi-Sormaghi, M.H., Essential Oil of Chimonanthus fragrans flowers Population of Tehran, DARU, 2007, 15, 3, 129-131. [all data]

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Mohottalage, S.; Tabacchi, R.; Guerin, P.M., Components from Sri Lankan Piper betle L. leaf oil and their analogues showing toxicity against the housefly, Musca domestica, Flavour Fragr. J., 2007, 22, 2, 130-138, https://doi.org/10.1002/ffj.1770 . [all data]

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Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Zizovic, Stamenic, et al., 2007
Zizovic, I.; Stamenic, M.; Ivanovic, J.; Orlovic, A.; Ristic, M.; Djordjevic, S.; Petrovic, S.D.; Skala, D., Supercritical carbon dioxide extraction of sesquiterpenes from valerian root, J. Supercrit. Fluids, 2007, 43, 2, 249-258, https://doi.org/10.1016/j.supflu.2007.05.007 . [all data]

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Morteza-Semnani K.; Akbarzadeh M.; Moshiri K., The essential oil composition of Eupatorium cannabinum L. from Iran, Flavour Fragr. J., 2006, 21, 3, 521-523, https://doi.org/10.1002/ffj.1687 . [all data]

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Wong, Sivasothy, et al., 2006
Wong, K.C.; Sivasothy, Y.; Boey, P.L., Essential oil of Elettariopsis elan C.K. Lim, Flavour Fragr. J., 2006, 21, 3, 562-564, https://doi.org/10.1002/ffj.1654 . [all data]

Asadipour, Mehrabani, et al., 2005
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Chagonda and Chalchat, 2005
Chagonda, L.S.; Chalchat, J.-C., The essential oil of the fruit of Garcinia huillensis Welw. ex. Oliv. from Zimbabwe, Flavour Fragr. J., 2005, 20, 3, 313-315, https://doi.org/10.1002/ffj.1420 . [all data]

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Velasco-Negueruela, Pérez-Alonso, et al., 2005
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Vichi, Riu-Aumatell, et al., 2005
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Sarkhail, Amin, et al., 2004
Sarkhail, P.; Amin, G.; Shafiee, A., Composition of the essential oil of Phlomis persica Boiss and Phlomis chorassanica Bunge from Iran, Flavour Fragr. J., 2004, 19, 6, 538-540, https://doi.org/10.1002/ffj.1338 . [all data]

Ghasemi, Asghari, et al., 2003
Ghasemi, N.; Asghari, G.; Ardakani, M.S.; Siahpoush, A., Characterization of volatile constituents from aerial parts of varthemia persica DC (var. persica), Iran. J. Pharm. Res., 2003, 2, 241-243. [all data]

Marongiu, Porcedda, et al., 2003
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Mookdasanit, Tamura, et al., 2003
Mookdasanit, J.; Tamura, H.; Yoshizawa T.; Tokunaga T.; Nakanishi, K., Trace Volatile Compounds in Essential Oil of Citrus Sudachi by Means of Modified Solvent Extraction Method, Food Sci Technol. Res., 2003, 9, 1, 54-61, https://doi.org/10.3136/fstr.9.54 . [all data]

Morteza-Semnani and Saeedi, 2003
Morteza-Semnani, K.; Saeedi, M., Constituents of the essential oil of Commiphora myrrha (Nees) Engl. var. molmol, J. Essent. Oil Res., 2003, 15, 1, 50-51, https://doi.org/10.1080/10412905.2003.9712264 . [all data]

Sajjadi and Mehregan, 2003
Sajjadi, S.E.; Mehregan, I., Chemical composition of the essential oil of Prangos Asperula Boiss. subsp. haussknechtii (Boiss.) Hernst. et Heyn fruits, 2003, retrieved from http://www1.tums.ac.ir/daru/daru2%2020003/Dr%20Sajadi.PDF. [all data]

Yassa, Akhani, et al., 2003
Yassa, N.; Akhani, H.; Aqaahmadi, M.; Salimian, M., Essential oils from two endemic species of Apiaceae from Iran, Z. Naturforsch. C:, 2003, 58, 459-463. [all data]

Zoghbi, Andrade, et al., 2003
Zoghbi, M.G.B.; Andrade, E.H.A.; da Silva, M.H.; Carreira, L.M.M.; Maia, J.G.S., Essential oils from three Myrcia species, Flavour Fragr. J., 2003, 18, 5, 421-424, https://doi.org/10.1002/ffj.1242 . [all data]

Cicció and Gómez-Laurito, 2002
Cicció, J.F.; Gómez-Laurito, J., Volatile constituents of the leaves of Siparuna thecaphora (Siparunaceae) from Turrialba, Costa Rica, Rev. Biol. Trop., 2002, 50, 3/4, 963-967. [all data]

Jirovetz, Buchbauer, et al., 2002
Jirovetz, L.; Buchbauer, G.; Ngassoum, M.B.; Geissler, M., Aroma compound analysis of Piper nigrum and Piper guineense essential oils from Cameroon using solid-phase microextraction-gas chromatography, solid-phase microextraction-gas chromatography-mass spectrometry and olfactometry, J. Chromatogr. A, 2002, 976, 1-2, 265-275, https://doi.org/10.1016/S0021-9673(02)00376-X . [all data]

Khallouki, Younos, et al., 2002
Khallouki, F.; Younos, C.; Soulimani, R.; Bessière, J.M., Chemical composition of the essential oils of Annona cuneata L. and Annona senegalensis Pers. stem barks, Flavour Fragr. J., 2002, 17, 5, 398-400, https://doi.org/10.1002/ffj.1115 . [all data]

Kobaisy, Tellez, et al., 2002
Kobaisy, M.; Tellez, M.R.; Dayan, F.E.; Duke, S.O., Phytotoxicity and volatile constituents from leaves of Callicarpa japonica Thunb., Phytochemistry, 2002, 61, 1, 37-40, https://doi.org/10.1016/S0031-9422(02)00207-8 . [all data]

Orav, Kailas, et al., 2002
Orav, A.; Kailas, T.; Müürisepp, M., Composition of blackcurrant aroma isolated from leaves, buds, and berries of Ribes nigrum L., Proc. Est. Acad. Sci. Chem., 2002, 51, 4, 225-234. [all data]

Zoghbi, Andrade, et al., 2002
Zoghbi, M.G.B.; Andrade, E.H.A.; da Silva, M.H.L.; Maia, J.G.S., Volatile constituents of Lippia lupulina Cham., Flavour Fragr. J., 2002, 17, 1, 29-31, https://doi.org/10.1002/ffj.1032 . [all data]

Kalemba, Marschall, et al., 2001
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Santos, Moreira, et al., 2001
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Notes

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