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2-Cyclohexen-1-ol, 1-methyl-4-(1-methylethyl)-, cis-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1DB-5CP Sil 5 CBDB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.220.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.230.260.200.240.
Heat rate (K/min) 3.2.5.5.3.
Initial hold (min)     3.
Final hold (min)  35.  5.
I 1129.1106.1126.1118.1110.
ReferenceBaccouri, Ben Temime, et al., 2007Paolini J., Costa J., et al., 2007Sabulal, Dan, et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006Dob, Dahmane, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5HP-5MSHP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.220.250.250.25
Phase thickness (mum) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.250.280.280.
Heat rate (K/min) 5.2.10.3.4.
Initial hold (min) 3. 2. 5.
Final hold (min) 5.20.10.  
I 1121.1108.1129.1098.1120.
ReferenceEsmaeili, Nematollahi, et al., 2006Gonny, Cavaleiro, et al., 2006Liu J.M., Nan P., et al., 2006Pavlovic, Kovacevic, et al., 2006Saroglou, Dorizas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1RTX-1SPB-1HP-5
Column length (m) 30.30.60.30.30.
Carrier gas H2 HeHe 
Substrate      
Column diameter (mm) 0.250.320.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.70.60.
Tend (C) 285.250.230.220.220.
Heat rate (K/min) 4.32.2.3.5.
Initial hold (min)  8.  10.
Final hold (min)   35.15. 
I 1116.1104.1106.1106.1125.
ReferenceVujisic L., Vuckovic I., et al., 2006Dob, Dahmane, et al., 2005Paolini, Costa, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Ceccarini, Macchia, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-1DB-5HP-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.170.250.250.25
Tstart (C) 45.50.60.60.60.
Tend (C) 300.200.240.260.260.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 6.    
Final hold (min) 10.    
I 1120.1099.1124.1122.1122.
ReferenceDugo, Mondello, et al., 2004Fernández-Ocaña, Gómez-Rodríguez, et al., 2004Flamini, Cioni, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSSPB-1BP-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (mum) 0.250.250.20.250.25
Tstart (C) 60.40.70.60.50.
Tend (C) 280.280.220.220.250.
Heat rate (K/min) 4.4.3.5.3.
Initial hold (min) 5.2.   
Final hold (min)   15.13. 
I 1119.1125.1106.1127.1124.
ReferenceKarioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Raina, Kumar, et al., 2004Salido, Valenzuela, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5HP-5RTX-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 60.40.60.60.45.
Tend (C) 240.200.240.280.250.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  5.  6.
Final hold (min) 7.20.   
I 1122.1129.1123.1120.1127.
ReferenceSartoratto, Machado, et al., 2004Yu, Kim, et al., 2004Bader, Flamini, et al., 2003Fokialakis, Melliou, et al., 2003Shellie, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1RTX-5CP Sil 5 CBRTX-5
Column length (m) 30.50.30.30.30.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.45.60.45.
Tend (C) 220.220.300.280.250.
Heat rate (K/min) 5.2.3.2.3.
Initial hold (min) 10. 6.10.6.
Final hold (min)  20.10.40. 
I 1123.1107.1122.1103.1121.
ReferenceFlamini, Cioni, et al., 2002Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5MSBP-1HP-5MSBPX-5
Column length (m) 30.30.50.30.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.220.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.60.60.50.60.
Tend (C) 250.280.220.250.180.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min) 6.5.  5.
Final hold (min)     5.
I 1126.1121.1107.1124.1142.
ReferenceShellie, Mondello, et al., 2002Giamakis, Kretsi, et al., 2001Lota, Serra, et al., 2001Salido, Altarejos, et al., 2001Zabaras and Wyllie, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1CP Sil 5 CBBP-1DB-5
Column length (m) 30.50.25.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.200.220.250.220.26
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 180.230.260.230.225.
Heat rate (K/min) 4.2.5.2.2.
Initial hold (min) 8.    
Final hold (min) 2.35. 35.20.
I 1121.1107.1126.1124.1121.
ReferenceAlonzo, Bosco, et al., 2000Lota, de Rocca Serra, et al., 2000Weyerstahl, Marschall, et al., 1999Mariotti, Costa, et al., 1997Sagrero-Nieves, Bartley, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-101OV-101DB-5
Column length (m) 25.50.50.60.
Carrier gas HeN2N2He
Substrate     
Column diameter (mm) 0.20.250.250.32
Phase thickness (mum) 0.3  1.
Tstart (C) 40.80.80.40.
Tend (C) 200.200.200.220.
Heat rate (K/min) 2.2.2.3.
Initial hold (min)     
Final hold (min)     
I 1142.1128.1130.1145.
ReferencePíry, Príbela, et al., 1995Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Baccouri, Ben Temime, et al., 2007
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Paolini J., Costa J., et al., 2007
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Dob, Dahmane, et al., 2006
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Gonny, Cavaleiro, et al., 2006
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Liu J.M., Nan P., et al., 2006
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Dob, Dahmane, et al., 2005
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Paolini, Costa, et al., 2005
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Flamini, Cioni, et al., 2004
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Moldão-Martins, Beirão-da-Costa, et al., 2004
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Raina, Kumar, et al., 2004
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Salido, Valenzuela, et al., 2004
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Sartoratto, Machado, et al., 2004
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Yu, Kim, et al., 2004
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Characterization of aroma-active compounds of Abies nephrolepis (Khingan fir) needles using aroma extract dilution analysis, Flavour Fragr. J., 2004, 19, 1, 74-79, https://doi.org/10.1002/ffj.1314 . [all data]

Bader, Flamini, et al., 2003
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Fokialakis, Melliou, et al., 2003
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Shellie, Marriott, et al., 2003
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Flamini, Cioni, et al., 2002
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Lota, de Rocca Serra, et al., 2002
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Jacquemond, C.; Casanova, J., Volatile components of peel and leaf oils of lemon and lime species, J. Agric. Food Chem., 2002, 50, 4, 796-805, https://doi.org/10.1021/jf010924l . [all data]

Mondello, Zappia, et al., 2002
Mondello, L.; Zappia, G.; Cotroneo, A.; Bonaccorsi, I.; Chowdhury, J.U.; Yusuf, M.; Dugo, G., Studies on the essential oil-bearing plants of Bangladesh. Part VIII. Composition of some Ocimum oils O. basilicum L. var. purpurascens; O. sanctum L. green; O. sanctum L. purple; O. americanum L., citral type; O. americanum L., camphor type, Flavour Fragr. J., 2002, 17, 5, 335-340, https://doi.org/10.1002/ffj.1108 . [all data]

Pino, Marbot, et al., 2002
Pino, J.A.; Marbot, R.; Bello, A., Volatile compounds of Psidium salutare (H.B.K.) Berg. fruit, J. Agric. Food Chem., 2002, 50, 18, 5146-5148, https://doi.org/10.1021/jf0116303 . [all data]

Shellie, Mondello, et al., 2002
Shellie, R.; Mondello, L.; Marriott, P.; Dugo, G., Characterisation of lavender essential oils by using gas chromatography-mass spectrometry with correlation of linear retention indices and comparison with comprehensive two-dimensional gas chromatography, J. Chromatogr. A, 2002, 970, 1-2, 225-234, https://doi.org/10.1016/S0021-9673(02)00653-2 . [all data]

Giamakis, Kretsi, et al., 2001
Giamakis, A.; Kretsi, O.; Chinou, I.; Spyropoulos, C.G., Eucalyptus camaldulensis: volatiles from immature flowers and high production of 1,8-cineole and «beta»-pinene by in vitro cultures, Phytochemistry, 2001, 58, 2, 351-355, https://doi.org/10.1016/S0031-9422(01)00193-5 . [all data]

Lota, Serra, et al., 2001
Lota, M.-L.; Serra, D.R.; Jacquemond, C.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of sour orange, Flavour Fragr. J., 2001, 16, 2, 89-96, https://doi.org/10.1002/1099-1026(200103/04)16:2<89::AID-FFJ950>3.0.CO;2-D . [all data]

Salido, Altarejos, et al., 2001
Salido, S.; Altarejos, J.; Nogueras, M.; Sánchez, A., Chemical composition of the essential oil of Artemisia herba-alba Asso ssp. valentina (Lam.) Marcl., J. Essent. Oil Res., 2001, 13, 4, 221-224, https://doi.org/10.1080/10412905.2001.9699675 . [all data]

Zabaras and Wyllie, 2001
Zabaras, D.; Wyllie, S.G., Quantitative analysis of terpenoids in the gas phase using headspace solid-phase microextraction (HS-SPME), Flavour Fragr. J., 2001, 16, 6, 411-416, https://doi.org/10.1002/ffj.1025 . [all data]

Alonzo, Bosco, et al., 2000
Alonzo, G.; Bosco, S.F.D.; Palazzolo, E.; Saiano, F.; Tusa, N., Citrus somatic hybrid leaf essential oil, Flavour Fragr. J., 2000, 15, 4, 258-262, https://doi.org/10.1002/1099-1026(200007/08)15:4<258::AID-FFJ906>3.0.CO;2-F . [all data]

Lota, de Rocca Serra, et al., 2000
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of mandarins from Citrus reticulata Blanco, Biochem. Syst. Ecol., 2000, 28, 1, 61-78, https://doi.org/10.1016/S0305-1978(99)00036-8 . [all data]

Weyerstahl, Marschall, et al., 1999
Weyerstahl, P.; Marschall, H.; Wahlburg, H.-C.; Christiansen, C.; Rustaiyan, A.; Mirdjalili, F., Constituents of the essential oil of Pulicaria gnaphalodes (Vent.) Boiss. from Iran, Flavour Fragr. J., 1999, 14, 2, 121-130, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<121::AID-FFJ790>3.0.CO;2-K . [all data]

Mariotti, Costa, et al., 1997
Mariotti, J.P.; Costa, J.; Bianchini, A.; Bernardini, A.F.; Casanova, J., Composition and variability of the essential oil of Stachys glutinosa L. from Corsica (France), Flavour Fragr. J., 1997, 12, 3, 205-209, https://doi.org/10.1002/(SICI)1099-1026(199705)12:3<205::AID-FFJ636>3.0.CO;2-I . [all data]

Sagrero-Nieves, Bartley, et al., 1997
Sagrero-Nieves, L.; Bartley, J.P.; Griselda Espinosa, B.; Dominguez, X.A.; Julia Verde S., Essential oil composition of Aristolochia brevipes Benth., Flavour Fragr. J., 1997, 12, 6, 401-403, https://doi.org/10.1002/(SICI)1099-1026(199711/12)12:6<401::AID-FFJ673>3.0.CO;2-D . [all data]

Píry, Príbela, et al., 1995
Píry, J.; Príbela, A.; Durcanská, J.; Farkas, P., Fractionation of volatiles from blackcurrant (Ribes nigrum L.) by different extractive methods, Food Chem., 1995, 54, 1, 73-77, https://doi.org/10.1016/0308-8146(95)92665-7 . [all data]

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Le Quere, J.-L.; Latrasse, A., Composition of the Essential Oils of Blackcurrant Buds (Ribes nigrum L.), J. Agric. Food Chem., 1990, 38, 1, 3-10, https://doi.org/10.1021/jf00091a001 . [all data]


Notes

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