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2-Cyclohexen-1-ol, 1-methyl-4-(1-methylethyl)-, cis-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5RTX-1RTX-1HP-5ZB-1
Column length (m) 60.60.60.30.30.
Carrier gas NitrogenHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.350.220.220.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.45.
Tend (C) 230.230.230.240.230.
Heat rate (K/min) 4.2.2.4.3.
Initial hold (min)    4. 
Final hold (min) 40.30.30.  
I 1128.1108.1108.1126.1099.
ReferenceGauvin-Bialecki and Marodon, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Zhannan, Shiqiong, et al., 2009Mierendorff, Stahl-Biskup, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5MSCol-Elite 5MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumN2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.30.60.
Tend (C) 230.240.250.246.220.
Heat rate (K/min) 3.5.2.3.4.
Initial hold (min) 10.1.8. 5.
Final hold (min) 10.4.15. 20.
I 1121.1121.1139.1126.1132.
ReferenceAdams, Beauchamp, et al., 2007Cheraif, Ben Jannet, et al., 2007Ferhat, Meklati, et al., 2007Gudaityte and Venskutonis R.P., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5 MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.50.50.
Tend (C) 240.280.280.280.280.
Heat rate (K/min) 4.3.3.9.9.
Initial hold (min)    3.3.
Final hold (min)    3.3.
I 1119.1087.1122.1115.1116.
ReferenceSefidkon, Abbasi, et al., 2007Tzakou, Bazos, et al., 2007Vagionas, Graikou, et al., 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5BP-1HP-5HP-5
Column length (m) 30.30.50.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.200.320.220.250.25
Phase thickness (mum) 0.200.250.250.250.25
Tstart (C) 70.60.60.50.60.
Tend (C) 220.246.220.300.220.
Heat rate (K/min) 3.3.2.5.5.
Initial hold (min)    5.10.
Final hold (min) 15. 20.5. 
I 1106.1122.1107.1128.1126.
ReferenceCavaleiro, Pinto, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Fanciullino, Tomi, et al., 2006Figuérédo, Cabassu, et al., 2006Pintore G., Chessa M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5DB-1
Column length (m) 30.30.30.25.60.
Carrier gas HydrogenHydrogenHeN2Helium
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 70.70.60.30.60.
Tend (C) 280.280.200.280.250.
Heat rate (K/min) 4.4.2.3.5.
Initial hold (min) 4.4.   
Final hold (min)   60. 10.
I 1120.1121.1128.1126.1110.
ReferencePino, Marbot, et al., 2006Pino, Marbot, et al., 2006Rout, Naik, et al., 2006Shafi, Jose, et al., 2006Sonboli, Mirjalili, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5HP-5MSDB-5HP-5
Column length (m)  30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 250.250.280.240.300.
Heat rate (K/min) 5.10.3.3.5.
Initial hold (min) 3.2.  5.
Final hold (min) 15.10.  5.
I 1117.1130.1116.1122.1128.
ReferenceStojanovic, Palic, et al., 2006Wang, Yang, et al., 2006Basta, Tzakou, et al., 2005Chaverri and Cicció, 2005Figuérédo, Cabassu, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200HP-5HP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.70.60.60.60.
Tend (C) 280.240.280.280.230.
Heat rate (K/min) 6.5.4.3.3.
Initial hold (min) 2.  5. 
Final hold (min) 10.   20.
I 1140.1121.1118.1119.1122.
ReferenceJirovetz, Buchbauer, et al., 2005Oyedeji, Yani, et al., 2005Sajjadi, 2005Setzer, Noletto, et al., 2005Skoula and Grayer, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5MSDB-5RTX-5Sil
Column length (m) 30.60.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.70.
Tend (C) 230.280.280.240.200.
Heat rate (K/min) 2.4.3.3.4.
Initial hold (min)  4.   
Final hold (min)   30. 10.
I 1126.1119.1085.1119.1127.
ReferenceGonzález, Guerra, et al., 2004Kalvandi, Sefidkon, et al., 2004Marongiu, Piras, et al., 2004Tellez, Khan, et al., 2004Dudai, Larkov, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RSL-200ZB-1HP-5DB-1
Column length (m) 60.30.30.30.50.
Carrier gas HeH2N2HeliumN2
Substrate      
Column diameter (mm) 0.320.320.250.320.25
Phase thickness (mum)  0.250.25 0.25
Tstart (C) 50.40.45.70.95.
Tend (C) 200.280.230.210.240.
Heat rate (K/min) 3.6.3.2.4.
Initial hold (min)  5.   
Final hold (min)  5. 60. 
I 1146.1113.1099.1121.1122.
ReferenceEdris, Shalaby, et al., 2003Jirovetz, Buchbauer, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mookdasanit, Tamura, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-15 % Phenyl methyl siloxaneHP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.70.75.60.
Tend (C) 280.280.220.200.275.
Heat rate (K/min) 4.3.3.3.4.
Initial hold (min)    4. 
Final hold (min)  30.15.8. 
I 1110.1103.1106.1122.1119.
ReferenceShahmir, Ahmadi, et al., 2003Caredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002Ghannadi, Sajjadi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5HP-5DB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHe  N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.80.
Tend (C) 240.250.240.240.225.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)  10.   
Final hold (min)      
I 1122.1123.1124.1127.1107.
ReferenceKobaisy, Tellez, et al., 2002Norouzi-Arasi, Yavari, et al., 2002Novak, Langbehn, et al., 2002Novak, Langbehn, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1DB-1PTE-5OV-101
Column length (m) 60.50.30.60.50.
Carrier gas HeHeN2H2N2
Substrate      
Column diameter (mm) 0.250.220.250.320.25
Phase thickness (mum) 0.250.250.250.3 
Tstart (C) 40.60.80.60.80.
Tend (C) 280.230.225.285.200.
Heat rate (K/min) 4.2.4.4.32.
Initial hold (min) 5.    
Final hold (min)  35.   
I 1105.1107.1092.1121.1130.
ReferenceSefidkon, Jalili, et al., 2002Lota, de Rocca Serra, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001Stojanovic, Palic, et al., 2001Yang, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5SPB-1RTX-1DB-1
Column length (m) 50.30.50.30.50.
Carrier gas N2He N2He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum)  0.250.330.250.25
Tstart (C) 80.60.60.60.70.
Tend (C) 200.240.260.300.240.
Heat rate (K/min) 2.3.4.4.4.
Initial hold (min)      
Final hold (min)      
I 1130.1122.1106.1125.1092.
ReferenceYang, 2001, 2Tellez, Dayan, et al., 2000Choo, Wong, et al., 1999Kalemba, 1999Palá-Paúl, Pérez-Alonso, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSMethyl SiliconeMethyl SiliconeOV-101OV-101
Column length (m) 30.50.50.50.50.
Carrier gas HeN2N2  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.170.17  
Tstart (C) 60.80.80.80.80.
Tend (C) 240.200.200.200.200.
Heat rate (K/min) 3.2.3.2.2.
Initial hold (min)      
Final hold (min)      
I 1124.1111.1117.1128.1130.
ReferenceZoghbi, Andrade, et al., 1999Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101BP-1OV-101
Column length (m) 25.50.50.50.50.
Carrier gas  N2N2H2 
Substrate      
Column diameter (mm) 0.330.250.250.300.30
Phase thickness (mum)      
Tstart (C) 45.80.80.40.40.
Tend (C) 180.200.200.250.230.
Heat rate (K/min) 3.2.2.10.3.5
Initial hold (min) 3.  1.5.
Final hold (min)      
I 1104.1129.1129.1129.1122.
ReferenceWyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Brophy, Davies, et al., 1989Nykanen, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-101
Column length (m) 50.
Carrier gas  
Substrate  
Column diameter (mm) 0.30
Phase thickness (mum)  
Tstart (C) 40.
Tend (C) 230.
Heat rate (K/min) 3.5
Initial hold (min) 5.
Final hold (min)  
I 1144.
ReferenceNykanen, 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gauvin-Bialecki and Marodon, 2009
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Mohottalage, S.; Tabacchi, R.; Guerin, P.M., Components from Sri Lankan Piper betle L. leaf oil and their analogues showing toxicity against the housefly, Musca domestica, Flavour Fragr. J., 2007, 22, 2, 130-138, https://doi.org/10.1002/ffj.1770 . [all data]

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Figuérédo, Cabassu, et al., 2005
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Jirovetz, Buchbauer, et al., 2005
Jirovetz, L.; Buchbauer, G.; Stoyanova, A.; Georgiev, E.V.; Damianova, S.T., Composition, quality control and antimicrobial activity of the essential oil of cumin (Cuminum cyminumL.) seeds from Bulgaria that had been stored for up to 36 years, Int. J. Food Sci. Technol., 2005, 40, 3, 305-310, https://doi.org/10.1111/j.1365-2621.2004.00915.x . [all data]

Oyedeji, Yani, et al., 2005
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Sajjadi, 2005
Sajjadi, S.E., Analysis of the essential oil of Nepeta sintenisii Bornm. from Iran, DARU, 2005, 13, 2, 61-64. [all data]

Setzer, Noletto, et al., 2005
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Notes

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