2-Cyclohexen-1-ol, 1-methyl-4-(1-methylethyl)-, cis-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1DB-5CP Sil 5 CBDB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.220.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.230.260.200.240.
Heat rate (K/min) 3.2.5.5.3.
Initial hold (min)     3.
Final hold (min)  35.  5.
I 1129.1106.1126.1118.1110.
ReferenceBaccouri, Ben Temime, et al., 2007Paolini J., Costa J., et al., 2007Sabulal, Dan, et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006Dob, Dahmane, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5HP-5MSHP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.220.250.250.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.250.280.280.
Heat rate (K/min) 5.2.10.3.4.
Initial hold (min) 3. 2. 5.
Final hold (min) 5.20.10.  
I 1121.1108.1129.1098.1120.
ReferenceEsmaeili, Nematollahi, et al., 2006Gonny, Cavaleiro, et al., 2006Liu J.M., Nan P., et al., 2006Pavlovic, Kovacevic, et al., 2006Saroglou, Dorizas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1RTX-1SPB-1HP-5
Column length (m) 30.30.60.30.30.
Carrier gas H2 HeHe 
Substrate      
Column diameter (mm) 0.250.320.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.70.60.
Tend (C) 285.250.230.220.220.
Heat rate (K/min) 4.32.2.3.5.
Initial hold (min)  8.  10.
Final hold (min)   35.15. 
I 1116.1104.1106.1106.1125.
ReferenceVujisic L., Vuckovic I., et al., 2006Dob, Dahmane, et al., 2005Paolini, Costa, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Ceccarini, Macchia, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-1DB-5HP-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.170.250.250.25
Tstart (C) 45.50.60.60.60.
Tend (C) 300.200.240.260.260.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 6.    
Final hold (min) 10.    
I 1120.1099.1124.1122.1122.
ReferenceDugo, Mondello, et al., 2004Fernández-Ocaña, Gómez-Rodríguez, et al., 2004Flamini, Cioni, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSSPB-1BP-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (μm) 0.250.250.20.250.25
Tstart (C) 60.40.70.60.50.
Tend (C) 280.280.220.220.250.
Heat rate (K/min) 4.4.3.5.3.
Initial hold (min) 5.2.   
Final hold (min)   15.13. 
I 1119.1125.1106.1127.1124.
ReferenceKarioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Raina, Kumar, et al., 2004Salido, Valenzuela, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5HP-5RTX-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.40.60.60.45.
Tend (C) 240.200.240.280.250.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  5.  6.
Final hold (min) 7.20.   
I 1122.1129.1123.1120.1127.
ReferenceSartoratto, Machado, et al., 2004Yu, Kim, et al., 2004Bader, Flamini, et al., 2003Fokialakis, Melliou, et al., 2003Shellie, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1RTX-5CP Sil 5 CBRTX-5
Column length (m) 30.50.30.30.30.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.45.60.45.
Tend (C) 220.220.300.280.250.
Heat rate (K/min) 5.2.3.2.3.
Initial hold (min) 10. 6.10.6.
Final hold (min)  20.10.40. 
I 1123.1107.1122.1103.1121.
ReferenceFlamini, Cioni, et al., 2002Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5MSBP-1HP-5MSBPX-5
Column length (m) 30.30.50.30.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.220.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 45.60.60.50.60.
Tend (C) 250.280.220.250.180.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min) 6.5.  5.
Final hold (min)     5.
I 1126.1121.1107.1124.1142.
ReferenceShellie, Mondello, et al., 2002Giamakis, Kretsi, et al., 2001Lota, Serra, et al., 2001Salido, Altarejos, et al., 2001Zabaras and Wyllie, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1CP Sil 5 CBBP-1DB-5
Column length (m) 30.50.25.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.200.220.250.220.26
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 180.230.260.230.225.
Heat rate (K/min) 4.2.5.2.2.
Initial hold (min) 8.    
Final hold (min) 2.35. 35.20.
I 1121.1107.1126.1124.1121.
ReferenceAlonzo, Bosco, et al., 2000Lota, de Rocca Serra, et al., 2000Weyerstahl, Marschall, et al., 1999Mariotti, Costa, et al., 1997Sagrero-Nieves, Bartley, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-101OV-101DB-5
Column length (m) 25.50.50.60.
Carrier gas HeN2N2He
Substrate     
Column diameter (mm) 0.20.250.250.32
Phase thickness (μm) 0.3  1.
Tstart (C) 40.80.80.40.
Tend (C) 200.200.200.220.
Heat rate (K/min) 2.2.2.3.
Initial hold (min)     
Final hold (min)     
I 1142.1128.1130.1145.
ReferencePíry, Príbela, et al., 1995Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Salido, Altarejos, et al., 2001
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Mariotti, Costa, et al., 1997
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Sagrero-Nieves, Bartley, et al., 1997
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Píry, Príbela, et al., 1995
Píry, J.; Príbela, A.; Durcanská, J.; Farkas, P., Fractionation of volatiles from blackcurrant (Ribes nigrum L.) by different extractive methods, Food Chem., 1995, 54, 1, 73-77, https://doi.org/10.1016/0308-8146(95)92665-7 . [all data]

Yang, Sugisawa, et al., 1992
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Le Quere and Latrasse, 1990
Le Quere, J.-L.; Latrasse, A., Composition of the Essential Oils of Blackcurrant Buds (Ribes nigrum L.), J. Agric. Food Chem., 1990, 38, 1, 3-10, https://doi.org/10.1021/jf00091a001 . [all data]


Notes

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