2-Cyclohexen-1-ol, 1-methyl-4-(1-methylethyl)-, trans-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CP Sil 5 CBBP-1HP-5HP-5MS
Column length (m) 60.30.50.30.30.
Carrier gas HeN2HeHeH2
Substrate      
Column diameter (mm) 0.220.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.50.
Tend (C) 230.200.220.250.285.
Heat rate (K/min) 2.5.2.10.4.3
Initial hold (min)    2. 
Final hold (min) 35. 20.10. 
I 1123.1138.1124.1148.1140.
ReferencePaolini J., Costa J., et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006Gonny, Cavaleiro, et al., 2006Liu J.M., Nan P., et al., 2006Vujisic L., Vuckovic I., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-1DB-5SPB-1HP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.40.70.60.
Tend (C) 260.230.260.220.220.
Heat rate (K/min) 2.2.2.3.5.
Initial hold (min) 5. 5. 10.
Final hold (min) 20.35.20.15. 
I 1083.1123.1140.1129.1142.
Referencede Feo, Urrunaga Soria, et al., 2005Paolini, Costa, et al., 2005Senatore, Napolitano, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Ceccarini, Macchia, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-1DB-5DB-5MSSPB-1
Column length (m) 30.25.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.2
Phase thickness (μm) 0.250.170.250.250.2
Tstart (C) 45.50.60.40.70.
Tend (C) 300.200.240.280.220.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min) 6.  2. 
Final hold (min) 10.   15.
I 1139.1113.1142.1144.1120.
ReferenceDugo, Mondello, et al., 2004Fernández-Ocaña, Gómez-Rodríguez, et al., 2004Flamini, Cioni, et al., 2004Mardarowicz, Wianowska, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5SPB-1RTX-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.20.25
Phase thickness (μm) 0.250.330.250.20.25
Tstart (C) 50.60.60.70.45.
Tend (C) 250.240.240.220.250.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)     6.
Final hold (min)  7. 15. 
I 1144.1140.1142.1120.1146.
ReferenceSalido, Valenzuela, et al., 2004Sartoratto, Machado, et al., 2004Bader, Flamini, et al., 2003Cavaleiro, Salgueiro, et al., 2003Shellie, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5BP-1RTX-5CP Sil 5 CB
Column length (m) 30.30.50.30.30.
Carrier gas HeN2HeHeH2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.45.60.
Tend (C) 280.220.220.300.280.
Heat rate (K/min) 4.5.2.3.2.
Initial hold (min) 5.10. 6.10.
Final hold (min)   20.10.40.
I 1140.1145.1123.1125.1117.
ReferenceSkaltsa, Demetzos, et al., 2003Flamini, Cioni, et al., 2002Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSBPX-5HP-5BP-1
Column length (m) 30.30.50.30.50.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.220.200.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 250.280.180.180.230.
Heat rate (K/min) 3.4.4.4.2.
Initial hold (min)  5.5.8. 
Final hold (min)   5.2.35.
I 1144.1140.1162.1140.1123.
ReferenceSalido, Altarejos, et al., 2001Skaltsa, Mavrommati, et al., 2001Zabaras and Wyllie, 2001Alonzo, Bosco, et al., 2000Lota, de Rocca Serra, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBBP-1Methyl SiliconeHP-101
Column length (m) 30.25.50.25.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.220.20.25
Phase thickness (μm) 0.25 0.250.3 
Tstart (C) 50.60.60.40.70.
Tend (C) 280.260.230.200.200.
Heat rate (K/min) 4.5.2.2.3.
Initial hold (min) 5.    
Final hold (min)   35.  
I 1138.1109.1108.1128.1128.
ReferenceLazari, Skaltsa, et al., 1999Weyerstahl, Marschall, et al., 1999Mariotti, Costa, et al., 1997Píry, Príbela, et al., 1995Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-101OV-101DB-5
Column length (m) 50.50.60.
Carrier gas N2N2He
Substrate    
Column diameter (mm) 0.250.250.32
Phase thickness (μm)   1.
Tstart (C) 80.80.40.
Tend (C) 200.200.220.
Heat rate (K/min) 2.2.3.
Initial hold (min)    
Final hold (min)    
I 1111.1112.1124.
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Paolini J., Costa J., et al., 2007
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Flamini, Cioni, et al., 2004
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References