Home Symbol which looks like a small house Up Solid circle with an upward pointer in it

Methanone, [5-chloro-2-[(cyclopropylmethyl)amino]phenyl]phenyl-


Gas Chromatography

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

View large format table.

Column type Active phase Temperature (C) I Reference Comment
CapillaryBP-1200.2349.Japp, Garthwaite, et al., 198825. m/0.22 mm/0.25 «mu»m, N2
PackedSE-30220.2370.Schütz, 1982N2
PackedSE-30250.2398.Schütz, 1982N2

Kovats' RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryCross-Linked Methylsilicone2410.Maurer and Pfleger, 198712. m/0.2 mm/0.33 «mu»m, He, 100. C @ 3. min, 30. K/min, 310. C @ 5. min

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-5MS2410.Augsburger, Rivier, et al., 199830. m/0.25 mm/0.25 «mu»m; Program: not specified
OtherMethyl Silicone2385.Ardrey and Moffat, 1981Program: not specified
OtherMethyl Silicone2407.Ardrey and Moffat, 1981Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Japp, Garthwaite, et al., 1988
Japp, M.; Garthwaite, K.; Geeson, A.V.; Osselton, M.D., Collection of Analytical Data for Benzodiazepines and Benzophenones, J. Chromatogr., 1988, 439, 2, 317-339, https://doi.org/10.1016/S0021-9673(01)83844-9 . [all data]

Schütz, 1982
Schütz, H., Benzodiazepines, Springer-Verlag, New York, 1982, 438. [all data]

Maurer and Pfleger, 1987
Maurer, H.; Pfleger, K., Identification and differentiation of benzodiazepines and their metabolites in urine by computerized gas chromatography-mass spectrometry, J. Chromatogr., 1987, 422, 85-101, https://doi.org/10.1016/0378-4347(87)80442-5 . [all data]

Augsburger, Rivier, et al., 1998
Augsburger, M.; Rivier, L.; Mangin, P., Comparison of different immunoassays and GC-MS screening of benzodiazepines in urine, J. Pharm. Biomed. Anal., 1998, 18, 4-5, 681-687, https://doi.org/10.1016/S0731-7085(98)00266-0 . [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

Go To: Top, Gas Chromatography, References