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Delorazepam


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryBP-1250.2571.Weston, Japp, et al., 199125. m/0.22 mm/0.25 «mu»m, N2
CapillaryDB-1250.2593.Weston, Japp, et al., 199130. m/0.53 mm/1.5 «mu»m, N2
PackedSE-30240.2569.Musumarra, Scarlata, et al., 1987N2, 1% se-30 on Anachrom ABS(80-100mesh); Column length: 2. m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-12537.MHA, 9999Tstart: 100. C; Tend: 300. C
CapillaryDB-52537.Zamechnik, Ethier, et al., 198915. m/0.25 mm/0.25 «mu»m, He, 150. C @ 1. min, 10. K/min; Tend: 260. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Weston, Japp, et al., 1991
Weston, S.I.; Japp, M.; Partridge, J.; Osselton, M.D., Collection of analytical data for benzodiazepines and benzophenones. Appendix, J. Chromatogr., 1991, 538, 2, 277-284, https://doi.org/10.1016/S0021-9673(01)88848-8 . [all data]

Musumarra, Scarlata, et al., 1987
Musumarra, G.; Scarlata, G.; Romano, G.; Cappello, G.; Clementi, S.; Giulietti, G., Qualitative organic analysis. Part 2. Identification of drugs by principal components analysis of standardized TLC data in four eluent systems and of retention indices on SE 30, J. Anal. Toxicol., 1987, 11, 4, 154-163, https://doi.org/10.1093/jat/11.4.154 . [all data]

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Zamechnik, Ethier, et al., 1989
Zamechnik, J.; Ethier, J.-C.; Neville, G.A., Benzodiazepines- an extensive collection of mass spectra, J. Can. Soc. Forensic Sci., 1989, 22, 3, 233-259, https://doi.org/10.1080/00085030.1989.10757437 . [all data]


Notes

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