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Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-

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Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1DB-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.60.60.
Tend (C) 240.246.280.180.280.
Heat rate (K/min) 3.3.5.3.2.
Initial hold (min) 3. 3. 8.
Final hold (min)    15.30.
I 911.931.926.924.925.
ReferenceKartal N., Sokmen M., et al., 2007Adams, González Elizondo, et al., 2006Allegrone, Belliardo, et al., 2006Angioni, Barra, et al., 2006Hazzit, Baaliouamer, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.20.250.260.26
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C)  240.210.246.246.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min)   2.  
Final hold (min)   33.  
I 932.929.933.930.931.
ReferenceLucero, Fredrickson, et al., 2006Oliveira, Leitao, et al., 2006Sylvestre, Pichette, et al., 2006Adams, Morris, et al., 2005Adams and Nguyen, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-5DB-5MSDB-5MSBPX-5
Column length (m) 30.50.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 250.260.240.180.240.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min) 10.2. 15. 
Final hold (min) 5.5.   
I 932.931.929.930.920.
ReferenceAsuming, Beauchamp, et al., 2005Baranauskiene, Venskutonis, et al., 2005Maia, Andrade, et al., 2005Angioni, Barra, et al., 2004El-Ghorab, Mansour, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5MSDB-1DB-5
Column length (m) 30.25.30.50.25.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.70.95.40.
Tend (C) 260.180.250.240.280.
Heat rate (K/min) 3.5.3.4.3.
Initial hold (min)  6.5. 5.
Final hold (min)  15.  5.
I 930.925.921.920.927.
ReferenceLopes, Strobl, et al., 2004Merle, Morón, et al., 2004Siani, Garrido, et al., 2004Velasco-Negueruela, Sanz, et al., 2004Amparo Blázquez, Pérez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5CP Sil 5 CBHP-5
Column length (m) 50.30.30.25.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.251.0.150.25
Tstart (C) 50.50.40.50.60.
Tend (C) 280.280.250.230.280.
Heat rate (K/min) 5.4.5.3.3.
Initial hold (min) 2.2.1.  
Final hold (min) 10.10.   
I 934.934.932.933.919.
ReferenceBaranauskiene, Venskutonis, et al., 2003Baranauskiene, Venskutonis, et al., 2003, 2Bouzouita, Kachouri, et al., 2003Ogunwande, Olawore, et al., 2003Özcan, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 5 CBSE-30BP-1BP-1
Column length (m) 25.25.25.60.25.
Carrier gas N2HeHeN2N2
Substrate      
Column diameter (mm) 0.550.250.220.320.32
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.50.70.60.60.
Tend (C) 220.230.220.220.220.
Heat rate (K/min) 5.3.4.5.5.
Initial hold (min)      
Final hold (min) 15.   15.
I 929.933.918.931.926.
ReferenceSrivastava, Ahmad, et al., 2003Kasali, Adio, et al., 2002Palá-Paúl, Velasco-Negueruela, et al., 2002Raina, Lal, et al., 2002Raina, Srivastava, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSBP-1BP-1DB-1
Column length (m) 25.30.30.25.28.
Carrier gas N2HeN2N2He
Substrate      
Column diameter (mm) 0.550.250.320.550.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.50.
Tend (C) 220.250.220.220.270.
Heat rate (K/min) 5.3.5.5.4.5
Initial hold (min)     1.
Final hold (min) 15. 13.15. 
I 925.928.920.922.924.
ReferenceRaina, Srivastava, et al., 2002, 2Salido, Altarejos, et al., 2002Shawl, Srivastava, et al., 2002Jain, Srivastava, et al., 2001Nagalakshmi, Thangadurai, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1DB-1DB-1SE-54
Column length (m) 50.25.30.30.30.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.550.250.250.26
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.60.40.80.60.
Tend (C) 225.220.260.225.246.
Heat rate (K/min) 4.5.2.4.3.
Initial hold (min)   5.  
Final hold (min)  15.20.  
I 916.924.927.928.931.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2001Raina, Srivastava, et al., 2001Senatore and Rigano, 2001Abella, Cortella, et al., 2000Adams, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54DB-5SE-30HP-5
Column length (m) 30.30.30.25.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.260.260.260.220.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.70.
Tend (C) 240.246.246.220.250.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)      
Final hold (min)      
I 931.931.931.920.929.
ReferenceAdams, 2000, 2Adams, 2000, 3Adams, 2000, 4Kardali, Velasco-Negueruela, et al., 2000Ramos, Siani, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5OV-101DB-5
Column length (m) 30.30.30.25.30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.320.260.320.25
Phase thickness (mum) 0.25 0.25 0.33
Tstart (C) 60.50.60.50.40.
Tend (C) 280.250.246.200.260.
Heat rate (K/min) 3.3.3.5.2.
Initial hold (min)  5.  5.
Final hold (min)     20.
I 931.930.931.925.905.
ReferenceRoussis, Tsoukatou, et al., 2000Tzakou, Harvala, et al., 2000Adams, 1999Kuiate, Zollo, et al., 1999Senatore and de Feo, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1BP-1Methyl SiliconeDB-1
Column length (m) 30.50.50.30.60.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 240.260.260.250.250.
Heat rate (K/min) 3.2.2.2.3.
Initial hold (min)    2.5.
Final hold (min)    5.10.
I 928.926.938.934.924.
Referenceda Silva, Andrade, et al., 1999Vera and Chane-Ming, 1999Vera and Chane-Ming, 1999Adegoke, Rao, et al., 1998Bylaite, Venskutonis, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum) 0.250.250.250.251.
Tstart (C) 40.40.40.60.50.
Tend (C) 250.250.250.240.220.
Heat rate (K/min) 2.2.2.4.3.
Initial hold (min) 5.5.5.  
Final hold (min) 20.20.20.  
I 905.905.905.927.928.
Referencede Feo, Porta, et al., 1998Senatore, Urrunaga Soria, et al., 1998Senatore, 1998Zoghbi, Andrade, et al., 1998Breheret, Talou, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5SE-30OV-101
Column length (m) 30.30.30.25.50.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.230.250.250.20.25
Phase thickness (mum)  0.250.25 0.2
Tstart (C) 50.40.60.60.80.
Tend (C) 200.250.240.180.200.
Heat rate (K/min) 3.2.3.3.2.
Initial hold (min)  5. 10. 
Final hold (min)  20. 1.60.
I 923.905.930.928.930.
ReferenceFiorini, Fourasté, et al., 1997Senatore, Urrunaga Soria, et al., 1997Tellez, Estell, et al., 1997Jantan, Ahmad, et al., 1996Padrayuttawat, Tamura, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5DB-5DB-5OV-101
Column length (m) 25.30.30.30.25.
Carrier gas N2   N2
Substrate      
Column diameter (mm) 0.2   0.25
Phase thickness (mum)      
Tstart (C) 60.40.40.40.50.
Tend (C) 180.210.210.210.200.
Heat rate (K/min) 3.2.2.2.5.
Initial hold (min) 10.2.2.2. 
Final hold (min) 1.120.120.120. 
I 926.934.933.933.926.
ReferenceJantan, Ali, et al., 1995Loayza, Abujder, et al., 1995Loayza, Abujder, et al., 1995Loayza, Abujder, et al., 1995Menut, Molangui, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase SE-54BP-1DB-1DB-1
Column length (m) 30.50.60.60.
Carrier gas HeH2HeHe
Substrate     
Column diameter (mm) 0.250.330.250.25
Phase thickness (mum) 0.25 1.1.
Tstart (C) 0.65.40.40.
Tend (C) 250.220.250.250.
Heat rate (K/min) 12.5.12.4.
Initial hold (min) 12.2.4. 
Final hold (min)     
I 923.930.949.940.
ReferenceRembold, Wallner, et al., 1989Ekundayo, Laakso, et al., 1988Burns and Tingey, 1983Burns and Tingey, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kartal N., Sokmen M., et al., 2007
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Raina, Lal, et al., 2002
Raina, V.K.; Lal, R.K.; Tripathi, S.; Khan, M.; Syamasundar, K.V.; Srivastava, S.K., Erratum. Essential oil composition of genetically diverse stocks of Murraya koenigii from India, Flavour Fragr. J., 2002, 17, 5, 404, https://doi.org/10.1002/ffj.1139 . [all data]

Raina, Srivastava, et al., 2002
Raina, V.K.; Srivastava, S.K.; Syamasunder, K.V., The essential oil of 'greater galangal' [Alpinia galanga (L.) Willd.] from the lower Himalayan region of India, Flavour Fragr. J., 2002, 17, 5, 358-360, https://doi.org/10.1002/ffj.1105 . [all data]

Raina, Srivastava, et al., 2002, 2
Raina, V.K.; Srivastava, S.K.; Jain, N.; Ahmad, A.; Syamasundar, K.V.; Aggarwal, K.K., Essential oil composition of Curcuma longa L. cv. Roma from the plains of northern India, Flavour Fragr. J., 2002, 17, 2, 99-102, https://doi.org/10.1002/ffj.1053 . [all data]

Salido, Altarejos, et al., 2002
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Shawl, Srivastava, et al., 2002
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Notes

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