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Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-

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Kovats' RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSBP-1BP-1BP-1OV-1
Column length (m) 30.25.25.30.15.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.250.250.250.320.317
Phase thickness (mum) 0.250.250.250.250.25
Program 60C(5min) => 2C/min => 140C= 5C/min => 250C(5min)60C => 5C/min => 220C(5min) => 3C/min => 245C(5min)60C => 5C/min => 220C (5min) => 3C/min => 245 C (5min)60C => 5.5C/min => 220C => 3.5C/min => 245C50C(4min) => (4C/min) => 90C => (10C/min)=300C(10min)
I 929.923.925.928.919.
ReferenceTuberoso, Kowalczyk, et al., 2005Dwivedi, Khan, et al., 2004Khan, Srivastava, et al., 2003Rao, Kaul, et al., 2003El-Shazly, Dorai, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1BP-1HP-5HP-5AT-5
Column length (m) 30.30.30.30.60.
Carrier gas HeN2H2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program 44C(4min) => 3C/min => 74C => 6C/min => 134C => 12C/min => 312C60 C 5 C/min -> 220 C (5 min) 3 C/min -> 245 C (5 min)60 0C (8 min) 3 K/min -> 180 0C 20 K/min (20 min)50 0C 5 K/min -> 140 0C 2 K/min -> 170 0C60 C 4K/min -> 200 C 10 K/min -> 280 C
I 919.925.922.931.928.
ReferenceEl-Shazly, Dorai, et al., 2002, 2Khan, Srivastava, et al., 2002Frizzo, Serafini, et al., 2001Novak, Zitterl-Eglseer, et al., 2001Khouri, Usubillaga, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5DB-5Methyl SiliconeSF-96SF-96
Column length (m) 60.30.25.127.150.
Carrier gas He    
Substrate      
Column diameter (mm) 0.250.26 0.750.75
Phase thickness (mum) 0.250.25   
Program 60 C (1 min) 4 K/min -> 200 C 10 K/min -> 280 Cnot specified50 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0Cnot specifiednot specified
I 931.931.924.928.931.
ReferenceRojas and Usubillaga, 2000Adams, 1998Machado, Militao, et al., 1995Okamoto, Ellison, et al., 1981Malingré and Maarse, 1974
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tuberoso, Kowalczyk, et al., 2005
Tuberoso, C.I.G.; Kowalczyk, A.; Coroneo, V.; Russo, M.T.; Dessì, S.; Cabras, P., Chemical Composition and Antioxidant, Antimicrobial, and Antifungal Activities of the Essential Oil of Achillea ligustica All., J. Agric. Food Chem., 2005, 53, 26, 10148-10153, https://doi.org/10.1021/jf0518913 . [all data]

Dwivedi, Khan, et al., 2004
Dwivedi, S.; Khan, M.; Srivastava, S.K.; Syamasunnder, K.V.; Srivastava, A., Essential oil composition of different accessions of Mentha × piperita L. grown on the northern plains of India, Flavour Fragr. J., 2004, 19, 5, 437-440, https://doi.org/10.1002/ffj.1333 . [all data]

Khan, Srivastava, et al., 2003
Khan, M.; Srivastava, S.K.; Jain, N.; Syamasundar, K.V.; Yadav, A.K., Chemical composition of fruit and stem essential oils of Lantana camara from northern India, Flavour Fragr. J., 2003, 18, 5, 376-379, https://doi.org/10.1002/ffj.1197 . [all data]

Rao, Kaul, et al., 2003
Rao, B.R.R.; Kaul, P.N.; Syamasundar, K.V.; Ramesh, S., Comparative composition of decanted and recovered essential oils of Eucalyptus citriodora Hook, Flavour Fragr. J., 2003, 18, 2, 133-135, https://doi.org/10.1002/ffj.1157 . [all data]

El-Shazly, Dorai, et al., 2002
El-Shazly, A.; Dorai, G.; Wink, M., Chemical composition and biological activity of the essential oils of Senecio aegyptus var. discoideus Boiss., Z. Naturforsch., 2002, 57c, 434-439. [all data]

El-Shazly, Dorai, et al., 2002, 2
El-Shazly, A.; Dorai, G.; Wink, M., Composition and antimicrobial activity of essential oil and hexane-ether extract of Tanacetum santolinoides (DC.) Feinbr. and Fertig, Z. Naturforsch., 2002, 57c, 620-623. [all data]

Khan, Srivastava, et al., 2002
Khan, M.; Srivastava, S.K.; Syamasundar, K.V.; Singh, M.; Naqvi, A.A., Chemical composition of leaf and flower essential oil of Lantana camara from India, Flavour Fragr. J., 2002, 17, 1, 75-77, https://doi.org/10.1002/ffj.1047 . [all data]

Frizzo, Serafini, et al., 2001
Frizzo, C.D.; Serafini, L.A.; Dellacassa, E.; Lorenzo, D.; Moyna, P., Essential oil of Baccharis uncinella DC. from Southern Brazil, Flavour Fragr. J., 2001, 16, 4, 286-288, https://doi.org/10.1002/ffj.998 . [all data]

Novak, Zitterl-Eglseer, et al., 2001
Novak, J.; Zitterl-Eglseer, K.; Deans, S.G.; Franz, C.M., Essential oils of different cultivars of Cannabis sativa L. and their antimicrobial activity, Flavour Fragr. J., 2001, 16, 4, 259-262, https://doi.org/10.1002/ffj.993 . [all data]

Khouri, Usubillaga, et al., 2000
Khouri, N.; Usubillaga, A.; Rojas, L.B.; Galarraga, F., The essential oil of Espeletia weddellii Sch. Bip. ex Wedd., Flavour Fragr. J., 2000, 15, 4, 263-265, https://doi.org/10.1002/1099-1026(200007/08)15:4<263::AID-FFJ907>3.0.CO;2-Q . [all data]

Rojas and Usubillaga, 2000
Rojas, L.B.; Usubillaga, A., Composition of the essential oil fo Satureja brownei (SW.) Briq. from Venezuela, Flavour Fragr. J., 2000, 15, 1, 21-22, https://doi.org/10.1002/(SICI)1099-1026(200001/02)15:1<21::AID-FFJ861>3.0.CO;2-G . [all data]

Adams, 1998
Adams, R.P., The essential oils and chemotaxonomy of Juniperus sect. Juniperus, Biochem. Syst. Ecol., 1998, 26, 6, 637-645, https://doi.org/10.1016/S0305-1978(98)00020-9 . [all data]

Machado, Militao, et al., 1995
Machado, S.M.F.; Militao, J.S.L.T.; Facundo, V.A.; Ribeiro, A.; de Morais, S.M.; de Alencar, J.W.; Filho, R.B., Essential Oil of Conyza sumatrensis (Retz) Walk, J. Essent. Oil Res., 1995, 7, 1, 83-84, https://doi.org/10.1080/10412905.1995.9698470 . [all data]

Okamoto, Ellison, et al., 1981
Okamoto, R.A.; Ellison, B.O.; Kepner, R.E., Volatile terpenes in Sequoia sempervirens foliage. Changes in composition during maturation, J. Agric. Food Chem., 1981, 29, 2, 324-326, https://doi.org/10.1021/jf00104a026 . [all data]

Malingré and Maarse, 1974
Malingré, T.M.; Maarse, H., Composition of the essential oil of Mentha aquatica, Phytochemistry, 1974, 13, 8, 1531-1535, https://doi.org/10.1016/0031-9422(74)80322-5 . [all data]


Notes

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