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2,4,6(1H,3H,5H)-Pyrimidinetrione, 5-ethyl-1,3-dimethyl-5-(3-methylbutyl)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedSE-30180.1614.Gambaro, Mariani, et al., 1982Gas Chrom P (100-120 mesh); Column length: 1.8 m
PackedSE-30180.1617.Gambaro, Mariani, et al., 1982Gas Chrom P (100-120 mesh); Column length: 1.8 m
PackedSE-30180.1617.Gambaro, Mariani, et al., 1982Gas Chrom P (100-120 mesh); Column length: 1.8 m
PackedSE-30180.1630.Gambaro, Mariani, et al., 1982Gas Chrom P (100-120 mesh); Column length: 1.8 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
PackedSE-301600.MHA, 9999Nitrogen, Chromosorb G AW DMCS (80-100 mesh); Column length: 2. m; Tstart: 100. C; Tend: 300. C
CapillaryDB-11590.Sharp, 198715. m/0.25 mm/0.25 «mu»m, He, 130. C @ 1. min, 10. K/min, 290. C @ 10. min

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gambaro, Mariani, et al., 1982
Gambaro, V.; Mariani, R.; Marozzi, E., Flash alkylation for the identification of barbiturates in biological material, J. Anal. Toxicol., 1982, 6, 6, 321-323, https://doi.org/10.1093/jat/6.6.321 . [all data]

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Sharp, 1987
Sharp, M.E., A rapid screening procedure for acidic and neutral drugs in blood by high resolution gas chromatography, J. Anal. Toxicol., 1987, 11, 1, 8-11, https://doi.org/10.1093/jat/11.1.8 . [all data]


Notes

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