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11-Methyltricosane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryApiezon L100.2332.Rappoport and Gäumann, 1973 

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS2335.Steinmetz, Schmolz, et al., 200330. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 150. C; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS2333.2Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryMethyl Silicone2336.Kaib, Jmhasly, et al., 2004Program: 80C(1.5min) =.40C/min => 160C => 2.5C/min => 280C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-12336.Mutis, Parra, et al., 200930. m/0.22 mm/0.25 «mu»m, Helium, 5. K/min, 290. C @ 15. min; Tstart: 40. C
CapillaryBP-12338.Mutis, Parra, et al., 200930. m/0.22 mm/0.25 «mu»m, Helium, 5. K/min, 290. C @ 15. min; Tstart: 40. C
CapillaryOV-12338.2Krkosova, Kubinec, et al., 2007100. m/0.32 mm/0.25 «mu»m, Helium, 5. K/min, 310. C @ 5. min; Tstart: 30. C
CapillaryDexsil 3002334.Lockey, 19785. K/min; Column length: 15. m; Tstart: 50. C; Tend: 370. C
CapillaryDexsil 3002334.Lockey, 19785. K/min; Column length: 15. m; Tstart: 50. C; Tend: 370. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCP Sil 5 CB2337.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 «mu»m, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)
CapillarySqualane2333.Petrov, 1984Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Rappoport and Gäumann, 1973
Rappoport, S.; Gäumann, T., 114. L'indice de rétention des alcanes isomères en chromatographie en phase gazeuse, Helv. Chim. Acta, 1973, 56, 3, 1145-1158, https://doi.org/10.1002/hlca.19730560338 . [all data]

Steinmetz, Schmolz, et al., 2003
Steinmetz, I.; Schmolz, E.; Ruther, J., Cuticular lipids as trail pheromone in a social wasp, Proc. R. Soc. London B:, 2003, 270, 1513, 385-391, https://doi.org/10.1098/rspb.2002.2256 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Kaib, Jmhasly, et al., 2004
Kaib, M.; Jmhasly, P.; Wilfert, L.; Durka, W.; Franke, S.; Francke, W.; Leuthold, R.H.; Brandl, R., Cuticular hydrocarbons and aggression in the termite Macrotermes Subhyalinus, J. Chem. Ecol., 2004, 30, 2, 365-385, https://doi.org/10.1023/B:JOEC.0000017983.89279.c5 . [all data]

Mutis, Parra, et al., 2009
Mutis, A.; Parra, L.; Palma, R.; Pardo, F.; Perich, F.; Quiroz, A., Evidence of contact pheromone use in mating behavior of the raspberry weevil (Coleoptera: Corculionidae), Environ. Entomol., 2009, 38, 1, 192-197, https://doi.org/10.1603/022.038.0124 . [all data]

Krkosova, Kubinec, et al., 2007
Krkosova, Z.; Kubinec, R.; Addova, G.; Jurdakova, H.; Blasko, J.; Ostrovsky, I.; Sojak, L., Gas chromatographic - mass spectrometric characterization of monomethylalkanes from fuel diesel, Petroleum Coal, 2007, 49, 3, 51-62. [all data]

Lockey, 1978
Lockey, K.H., The adult cuticular hydrocarbons of Tenebrio Molitor L. and Tenebrio Obscurus F. (Coleoptera: Tenebrionidae), Insect Biochem., 1978, 8, 4, 237-250, https://doi.org/10.1016/0020-1790(78)90032-X . [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]

Petrov, 1984
Petrov, A.A., Hydrocarbons of petroleum, Nauka (publishing house), Moscow, 1984, 263. [all data]


Notes

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