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2-Chlorobenzalmalononitrile


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
PackedSE-301516.Ramsey, Lee, et al., 1980He, Chromosorb G HP (80-100 mesh); Column length: 1.5 m; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-541564.Kostiainen, 200025. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min, 280. C @ 10. min
CapillarySE-541561.6Salehuddin, 199725. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min, 280. C @ 1. min
CapillarySE-541562.09Salehuddin, 199725. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min, 280. C @ 1. min
CapillarySE-541562.09Salehuddin, 199725. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min, 280. C @ 1. min
CapillarySE-541554.28Kaipainen, Kostiainen, et al., 199225. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min; Tend: 280. C
CapillarySE-541554.40Kaipainen, Kostiainen, et al., 199225. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 10. K/min; Tend: 280. C
CapillaryDB-51555.1D'Agostino and Provost, 198515. m/0.32 mm/0.25 «mu»m, He, 50. C @ 2. min, 10. K/min; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPolydimethyl siloxane1555.Staples, 2006Program: not specified
OtherMethyl Silicone1516.Ardrey and Moffat, 1981Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ramsey, Lee, et al., 1980
Ramsey, J.D.; Lee, T.D.; Osselton, M.D.; Moffat, A.C., Gas-liquid chromatographic retention indices of 296 non-drug substances on SE-30 or OV-1 likely to be encountered in toxicological analyses, J. Chromatogr., 1980, 184, 2, 185-206, https://doi.org/10.1016/S0021-9673(00)85641-1 . [all data]

Kostiainen, 2000
Kostiainen, O., Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention in Encyclopedia of Analytical Chemistry, Meyers, R.A., ed(s)., John Wiley Sons Ltd, Chichester, 2000, 963-979. [all data]

Salehuddin, 1997
Salehuddin, S.M., Study of chemical warfare agens by retention index method with dual-channel high resolution gas chromatography and high performance liquid chromatography, J. Bangladesh Acad. Sci., 1997, 21, 2, 159-164. [all data]

Kaipainen, Kostiainen, et al., 1992
Kaipainen, A.; Kostiainen, O.; Riekkola, M.-L., Identification of chemical warfare agents in air samples using capillary column gas chromatography with three simultaneous detectors, J. Microcolumn Sep., 1992, 4, 3, 245-251, https://doi.org/10.1002/mcs.1220040311 . [all data]

D'Agostino and Provost, 1985
D'Agostino, P.A.; Provost, L.R., Gas chromatographic retention indices of chemical warfare agents and simulants, J. Chromatogr., 1985, 331, 47-54, https://doi.org/10.1016/0021-9673(85)80005-4 . [all data]

Staples, 2006
Staples, E.J., Creating a compound library for chemical warfare agents for the ZNose, 2006, retrieved from http://www.estcal.com/TechPapers/Security/CWA-Libraries.pdf. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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