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Alloaromadendrene


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5HP-5 MS
Column length (m) 30.25.25.25.30.
Carrier gas HeliumHydrogenHydrogenHydrogen 
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (mum) 0.250.520.520.520.25
Tstart (C) 60.40.40.40.60.
Tend (C) 240.280.280.280.300.
Heat rate (K/min) 3.4.4.4.15.
Initial hold (min)     2.
Final hold (min)  10.10.10.10.
I 1462.1454.1454.1454.1439.
ReferenceRodriques, Amorim, et al., 2013Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Xu, Han, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1HP-5 MSCP-Sil 5 CBElite-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.260.25
Tstart (C) 50.40.50.45.40.
Tend (C) 250.210.180.280.220.
Heat rate (K/min) 7.5.2.3.4.
Initial hold (min) 1.    
Final hold (min) 5.  22. 
I 1487.1464.1448.1465.1503.
ReferenceZouari, Ayadi, et al., 2012Fathi, Sahari, et al., 2011Hammami, Kamoun, et al., 2011Mothana, Hasson, et al., 2011Baharum, Bunawan, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5 MSBP-1HP-5HP-5 MS
Column length (m) 30.60. 30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.40.60.40.60.
Tend (C) 250.250.220.260.220.
Heat rate (K/min) 2.5.5.4.6.
Initial hold (min)  15.10. 3.
Final hold (min)  15.30.5. 
I 1460.1454.1462.1469.1462.
ReferenceHo, Wang, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Safaei-Ghomi and Batooli, 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5DB-5DB-5HP-5
Column length (m) 30.30.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.40.50.70.60.
Tend (C) 240.240.250.240.240.
Heat rate (K/min) 3.3.5.5.3.
Initial hold (min)  1.2.  
Final hold (min)     7.
I 1460.1478.1460.1468.1461.
ReferenceSilva, Pott, et al., 2010de Souza, Lopes, et al., 2010Ho, Wang, et al., 2009Lawal and Oyedelji, 2009Maridass, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-15 % Phenyl methyl siloxaneDB-5DB-5
Column length (m) 60.60.60.30.30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.90.40.40.
Tend (C) 230.230.225.230.240.
Heat rate (K/min) 2.2.3.2.3.
Initial hold (min)     1.
Final hold (min) 30.30.3.  
I 1462.1462.1461.1460.1478.
ReferenceMuseli, Pau, et al., 2009Museli, Pau, et al., 2009Retta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009de Souza, Lopes, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSHP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHelium NitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.60.60.50.50.
Tend (C) 240.300.280.280.230.
Heat rate (K/min) 5.15.3.5.4.
Initial hold (min)  2. 1.4.
Final hold (min)  10. 1.10.
I 1474.1439.1459.1463.1460.
ReferenceWannes, Mhamdi, et al., 2009Xu, Han, et al., 2009Baziou, Couladis, et al., 2008Bousaada, Ammar, et al., 2008Forero, Quijano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSZB-1DB-5 MSRTX-1Elite-1
Column length (m) 30.30.30.60.30.
Carrier gas HeliumNitrogenHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.45.50.60.60.
Tend (C) 250.230.300.230.246.
Heat rate (K/min) 3.3.5.2.3.
Initial hold (min) 2. 5.  
Final hold (min) 10. 5.35. 
I 1464.1452.1454.1451.1454.
ReferenceLo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Noudogbessi, Yedomonhan, et al., 2008Paolini, Tomi, et al., 2008Raj, Baby, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BPX-5DB-5MSHP-5MSDB-5
Column length (m) 30.7.530.30.30.
Carrier gas NitrogenHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.100.250.250.26
Phase thickness (mum) 0.2510.0.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 280.240.240.240.240.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min) 1.    
Final hold (min) 1.    
I 1476.1464.1462.1473.1456.
ReferenceSaidana, Mahjoub, et al., 2008Shellie, 2008Andrade, Oliveira, et al., 2007Argyropoulou, Daferera, et al., 2007Bos, Woerdenbag, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5HP-5MSDB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeliumHeliumHeNitrogen
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (mum) 0.250.250.260.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.290.240.250.250.
Heat rate (K/min) 3.3.4.2.4.
Initial hold (min)   2.8.1.
Final hold (min)   20.15.10.
I 1462.1456.1460.1456.1449.
ReferenceBozin B., Mlmica-Dukic N., et al., 2007Elfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Ghasempour, Shirinpour, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Col-Elite 5MSHP-1SE-30HP-5DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 30.60.40.40.50.
Tend (C) 246.240.250.250.260.
Heat rate (K/min) 3.2.5.5.2.5
Initial hold (min)   5.5.1.
Final hold (min)  20.10.10.20.
I 1467.1443.1461.1459.1440.
ReferenceGudaityte and Venskutonis R.P., 2007Hachicha, Skanji, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Monser-Esfahani, Karamkhani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1HP-5 MSSPB-1
Column length (m) 30.25.50.25.30.
Carrier gas HeliumH2HeHeliumHe
Substrate      
Column diameter (mm) 0.250.20.250.250.2
Phase thickness (mum) 0.250.330.250.250.2
Tstart (C) 60.60.95.100.70.
Tend (C) 300.240.240.280.220.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min)    3. 
Final hold (min)    5.15.
I 1429.1461.1466.1466.1449.
ReferenceMoreno, Lima, et al., 2007Oliveira, Leitão, et al., 2007Pala-Paul, Brophy, et al., 2007Phutdhawong, Kawaree, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-5DB-1DB-5
Column length (m) 30.60.30.60.30.
Carrier gas HeNitrogenHeNitrogen 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.40.
Tend (C) 250.250.320.250.250.
Heat rate (K/min) 2.4.10.5.2.
Initial hold (min)  1.   
Final hold (min)  10.4.10.33.
I 1456.1449.1460.1459.1460.
ReferenceRaal, Orav, et al., 2007Reza, Ebrahim, et al., 2007Smelcerovic, Spiteller, et al., 2007Sonboli, Kanani, et al., 2007Sylvestre, Pichette, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSHP-5 MSHP-5MSHP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeHeliumN2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.50.250.250.250.25
Tstart (C) 40.60.60.60.50.
Tend (C) 280.280.280.280.280.
Heat rate (K/min) 4.3.3.3.9.
Initial hold (min) 5.   3.
Final hold (min) 10.   3.
I 1464.1460.1416.1460.1458.
ReferenceTava, Pecetti, et al., 2007Tsokou, Georgopoulos, et al., 2007Tzakou, Bazos, et al., 2007Vagionas, Graikou, et al., 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5HP-5ZB-5
Column length (m) 30.30.30.60.30.
Carrier gas N2He He 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.40.
Tend (C) 280.300.300.250.300.
Heat rate (K/min) 9.3.3.3.2.
Initial hold (min) 3.    
Final hold (min) 3.    
I 1476.1451.1455.1472.1444.
ReferenceAbdelwahed, Hayder, et al., 2006Apel, Sobral, et al., 2006Apel, Sobral, et al., 2006, 2Bertrand, Comte, et al., 2006Biondi, Sari, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5BP-1DB-1HP-5DB-5
Column length (m) 60.50.60.30.30.
Carrier gas He NitrogenHeHelium
Substrate      
Column diameter (mm) 0.250.220.250.320.26
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 200.220.200.246.290.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min)   1.  
Final hold (min) 20.20.9.  
I 1458.1461.1452.1459.1456.
ReferenceBorges, Rojas, et al., 2006Boti, Yao, et al., 2006Chen, Sheu, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1DB-5DB-1DB-5
Column length (m) 30.50.30.60.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 50.60.40.60.60.
Tend (C) 300.250.210.240.240.
Heat rate (K/min) 5.2.2.5.5.
Initial hold (min) 5. 2.2.2.
Final hold (min) 5.40.33.  
I 1460.1446.1460.1451.1461.
ReferenceFiguérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Garneau F.X., Collin G., et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CP Sil 5 CBHP-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHe HeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.100.
Tend (C) 240.240.220.260.240.
Heat rate (K/min) 5.5.3.5.5.
Initial hold (min) 2.2. 2.2.
Final hold (min)   3.13.5.
I 1451.1461.1460.1465.1461.
ReferenceGohari A.R., Hadjiakhoondi A., et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Hymete, Rohloff, et al., 2006Kucuk, Gulec, et al., 2006Lago, Soares, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5DB-5CP-Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas N2HeHeHeHydrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 50.60.60.50.50.
Tend (C) 300.220.220.250.230.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min)  5.5.  
Final hold (min)      
I 1449.1462.1462.1467.1462.
ReferenceLis and Milczarek, 2006Morteza-Semnani K., Akbarzadeh M., et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Najafpour Navaei, Mirza, et al., 2006Olawore, Usman, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5MSHP-5
Column length (m) 25.30.30.30.25.
Carrier gas N2HeHydrogenHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.60.70.60.60.
Tend (C) 200.220.280.280.240.
Heat rate (K/min) 4.5.4.3.3.
Initial hold (min) 3.10.4.  
Final hold (min)      
I 1467.1451.1462.1423.1464.
ReferenceOuamba, Ouabonzi, et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Potzernheim, Bizzo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SPB-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.25. 25.25.
Carrier gas HeN2HeH2 
Substrate      
Column diameter (mm) 0.250.2 0.250.25
Phase thickness (mum) 0.250.33   
Tstart (C) 40.30.50.50.50.
Tend (C) 260.280.250.230.230.
Heat rate (K/min) 2.3.5.3.3.
Initial hold (min) 5. 3.  
Final hold (min) 20. 15.  
I 1461.1472.1461.1462.1463.
ReferenceSenatore, Landolfi, et al., 2006Shafi, Jose, et al., 2006Stojanovic, Palic, et al., 2006Tesso, König, et al., 2006Tesso, Kubeczka, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-5DB-5DB-5DB-5
Column length (m) 25.30.50.30.30.
Carrier gas N2N2 HeHe
Substrate      
Column diameter (mm) 0.30.250.30.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 210.240.240.240.300.
Heat rate (K/min) 2.4.2.3.3.
Initial hold (min) 5.   3.
Final hold (min)      
I 1478.1453.1465.1456.1459.
ReferenceTonzibo, Coffy, et al., 2006Trilles, Bombarda, et al., 2006Chagonda and Chalchat, 2005Chaverri and Cicció, 2005Ferraz, Limberger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5DB-5MSDB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.520.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 30.240.230.280.220.
Heat rate (K/min) 4.4.3.3.4.
Initial hold (min) 3.  30.5.
Final hold (min) 15.    
I 1461.1455.1444.1432.1460.
ReferenceFerretti, Maggi, et al., 2005Jovanovic, Kitic, et al., 2005Limberger, Sobral, et al., 2005Marongiu, Piras, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBCP Sil 5 CBHP-5MSDB-5
Column length (m) 30.25.25.30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.150.150.25 
Tstart (C) 60.50.50.60.40.
Tend (C) 220.230.230.280.240.
Heat rate (K/min) 4.3.3.4.4.
Initial hold (min) 4.    
Final hold (min)      
I 1461.1464.1464.1459.1460.
ReferenceMorteza-Semnani and Saeedi, 2005Ogunwande, Olawore, et al., 2005Olawore, Ogunwande, et al., 2005Sajjadi S.E. and Eskandari B., 2005Sefidkon and Jamzad, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSRTX-1BP-1
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 260.300.280.250.220.
Heat rate (K/min) 2.3.3.5.5.
Initial hold (min) 5.    
Final hold (min) 20.  10.15.
I 1461.1455.1460.1470.1467.
ReferenceSenatore, Apostolides Arnold, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Slavkovska, Couladis, et al., 2005Sonboli A., Fakhari A.R., et al., 2005Srivastava, Srivastava, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5CP Sil 5 CBDB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeN2He 
Substrate      
Column diameter (mm) 0.250.320.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.90.60.
Tend (C) 280.280.200.220.220.
Heat rate (K/min) 3.3.5.7.2.
Initial hold (min)    2. 
Final hold (min)    5.20.
I 1416.1432.1450.1464.1459.
ReferenceTzakou, Bazos, et al., 2005Tzakou and Constantinidis, 2005Agnaniet, Menut, et al., 2004Agnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5SE-54DB-5RTX-1
Column length (m) 30.60.30.30.30.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.60.
Tend (C) 200.280.260.300.300.
Heat rate (K/min) 5.4.2.3.4.
Initial hold (min)  4.5.  
Final hold (min)      
I 1468.1461.1449.1443.1458.
ReferenceFekam Boyom, Fotio, et al., 2004Kalvandi, Sefidkon, et al., 2004Kilic, Hafizoglu, et al., 2004Limberger, Sobral, et al., 2004Lis, Boczek, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5MSNB-30HP-5MSDB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.40.
Tend (C) 280.275.250.280.250.
Heat rate (K/min) 3.4.2.4.2.
Initial hold (min)     5.
Final hold (min) 30.   20.
I 1422.1464.1456.1459.1460.
ReferenceMarongiu, Porcedda, et al., 2004Mehrabani, Asadipour, et al., 2004Raal, Paaver, et al., 2004Sajjadi and Shahpiri, 2004Senatore, Rigano, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BPX-5HP-5MSHP-5RTX-5Sil
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 60.60.60.60.70.
Tend (C) 300.250.275.220.200.
Heat rate (K/min) 3.3.4.5.4.
Initial hold (min)  5. 10. 
Final hold (min)  10.  10.
I 1460.1485.1461.1478.1459.
ReferenceTirillini, Pellegrino, et al., 2004Vilaseca, Guy, et al., 2004Afsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Dudai, Larkov, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5RSL-200RSL-200
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.40.40.
Tend (C) 200.280.280.280.280.
Heat rate (K/min) 5.4.4.6.6.
Initial hold (min)    5.5.
Final hold (min)    5.5.
I 1455.1461.1430.1460.1461.
ReferenceFekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003Ghassemi, Sajjadi, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5DB-5CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 60.60.60.60.50.
Tend (C) 250.240.280.275.230.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)    5. 
Final hold (min)   30.  
I 1472.1461.1459.1478.1448.
ReferenceLimberger, Simões-Pires, et al., 2003Maia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003Morteza-Semnani and Saeedi, 2003Oyedeji, Ekundayo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5NB-30DB-5DB-5
Column length (m) 50.30.50.30.30.
Carrier gas N2H2HeN2He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.50.250.25
Tstart (C) 95.60.50.40.60.
Tend (C) 240.280.250.230.240.
Heat rate (K/min) 4.4.2.2.3.
Initial hold (min)  10.   
Final hold (min)  40.   
I 1462.1461.1460.1463.1461.
ReferencePerez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Raal, Arak, et al., 2003Rotman, Ahumada, et al., 2003da Silva, Luz, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5
Column length (m) 60.60.60.25.25.
Carrier gas    H2H2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.530.53
Tstart (C) 40.40.40.40.40.
Tend (C) 250.250.250.280.280.
Heat rate (K/min) 5.5.5.4.4.
Initial hold (min) 15.15.15.  
Final hold (min)      
I 1465.1465.1465.1455.1460.
ReferenceStashenko, Jaramillo, et al., 2003Stashenko, Jaramillo, et al., 2003Stashenko, Jaramillo, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 25.25.25.25.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (mum) 0.530.530.530.530.25
Tstart (C) 40.40.40.40.60.
Tend (C) 280.280.280.280.240.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min)      
Final hold (min)      
I 1456.1457.1458.1460.1463.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Zoghbi, Andrade, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-55 % Phenyl methyl siloxaneDB-5MSBPX-5
Column length (m) 25.30.30.30. 
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.60.75.60.40.
Tend (C) 250.280.200.280.260.
Heat rate (K/min) 4.3.3.3.5.
Initial hold (min)   4.  
Final hold (min) 10.30.8.  
I 1462.1452.1460.1461.1475.
ReferenceZrira, Elamrani, et al., 2003Caredda, Marongiu, et al., 2002Cicció and Gómez-Laurito, 2002Congiu, Falconieri, et al., 2002Diaz and Kite, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SE-30OV-101HP-5
Column length (m) 30.30.50.25.30.
Carrier gas N2N2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 50.50.70.50.100.
Tend (C) 250.250.240.200.240.
Heat rate (K/min) 4.4.4.5.5.
Initial hold (min)  5.  2.
Final hold (min)     5.
I 1461.1462.1463.1465.1445.
ReferenceFarah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Iñigo, Palá-Paúl, et al., 2002Kuiate, Bessière, et al., 2002Lago, Reis, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5DB-5MS
Column length (m) 30.30.25.30.30.
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.250.250.230.250.25
Phase thickness (mum) 0.250.250.150.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 250.275.250.240.240.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  4.   
Final hold (min)      
I 1434.1451.1459.1461.1463.
ReferenceLimberger, Simões-Pires, et al., 2002Lockwood, Asghari, et al., 2002Mahmout, Bessière, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1DB-1DB-5MSDB-5
Column length (m) 50.60.60.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 90.40.40.60.60.
Tend (C) 220.280.280.270.240.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min)  5.5.  
Final hold (min)      
I 1458.1454.1456.1461.1460.
ReferencePriestap, van Baren, et al., 2002Sefidkon, Jalili, et al., 2002Sefidkon, 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5MSSPB-5DB-1DB-1
Column length (m) 60.30.60.60.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.2480.250.320.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.40.40.40.
Tend (C) 220.240.220.280.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min) 5. 5.5.5.
Final hold (min) 22. 15.  
I 1465.1455.1481.1458.1466.
ReferenceBailac, Dellacasa, et al., 2001Cherchi, Deidda, et al., 2001Cornu, Carnat, et al., 2001Dabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5BP-1RSL-200OV-101
Column length (m) 30.30.30.30.50.
Carrier gas N2N2N2H2He
Substrate      
Column diameter (mm) 0.250.250.250.320.2
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.60.40.50.
Tend (C) 220.220.220.280.250.
Heat rate (K/min) 5.5.5.6.2.
Initial hold (min) 10.10. 5. 
Final hold (min)    5. 
I 1461.1461.1463.1477.1464.
ReferenceFlamini, Cioni, et al., 2001Gallori, Flamini, et al., 2001Gupta, Mallavarapu, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Orav and Kann, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-1HP-1
Column length (m) 30.30.30.30.60.
Carrier gas HeN2H2 He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.80.60.45.60.
Tend (C) 270.225.285.300.200.
Heat rate (K/min) 3.4.3.15.4.
Initial hold (min)    2.5.
Final hold (min)    5.25.
I 1460.1441.1458.1495.1475.
ReferencePalmeira, Conserva, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001Hedin, McKibben, et al., 2000Meccia, Rojas, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5OV-101SE-30OV-101
Column length (m) 25.30.50.25.25.
Carrier gas N2HeNitrogenHeN2
Substrate      
Column diameter (mm) 0.330.250.250.20.25
Phase thickness (mum) 1.00.25   
Tstart (C) 60.60.40.60.50.
Tend (C) 275.275.200.230.200.
Heat rate (K/min) 4.4.2.3.5.
Initial hold (min)   10.  
Final hold (min)      
I 1460.1456.1462.1413.1462.
ReferenceMohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2Tamura, Boonbumrung, et al., 2000Ali N.A.M. and Jantan, 1999Ayedoun, Adéoti, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CP Sil 5 CBDB-1DB-5SE-30
Column length (m) 25.25.50.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum)   0.250.250.20
Tstart (C) 60.50.70.40.60.
Tend (C) 230.230.240.250.200.
Heat rate (K/min) 3.3.4.2.3.
Initial hold (min) 10.  5.4.
Final hold (min)    60. 
I 1413.1462.1441.1470.1488.
ReferenceMohd and Jantan, 1999Oyedeji, Olawore, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Porta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-1DB-1OV-101
Column length (m) 25.30.60.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.20
Phase thickness (mum) 0.390.250.25  
Tstart (C) 60.40.50.60.80.
Tend (C) 220.220.220.230.240.
Heat rate (K/min) 5.4.4.3.6.
Initial hold (min) 5.5.   
Final hold (min) 20.  5. 
I 1460.1457.1464.1453.1462.
ReferenceRustaiyan, Masoudi, et al., 1999Sefidkon and Khajavi, 1999Sefidkon and Mirza, 1999Shafiee, Javidnia, et al., 1999Zenkevich, Kosman, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSOV-101OV-1DB-5HP-1
Column length (m) 30.50.50.30.60.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 60.100.50.60.50.
Tend (C) 240.220.250.240.280.
Heat rate (K/min) 3.1.10.3.4.
Initial hold (min)  1.5. 5.
Final hold (min)   20.  
I 1459.1446.1464.1461.1477.
ReferenceZoghbi, Andrade, et al., 1999Camciuc, Bessière, et al., 1998Kökdil, Kurucu, et al., 1998Santos, Andrade, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5OV-1DB-1HP-1
Column length (m) 25.30.30. 25.
Carrier gas  He  Helium
Substrate      
Column diameter (mm) 0.320.250.32 0.32
Phase thickness (mum)  0.250.25 0.25
Tstart (C) 50.65.40.80.60.
Tend (C) 200.300.270.220.220.
Heat rate (K/min) 5.4.2.6.4.
Initial hold (min)  2.4. 2.
Final hold (min)     20.
I 1462.1466.1437.1454.1451.
ReferenceZollo, Biyiti, et al., 1998Elias, Simoneit, et al., 1997Kökdil, Tanker, et al., 1997Salgueiro, Vila, et al., 1997Thanh, Dung, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-1HP-101DB-1RSL-150
Column length (m) 52.50.50.60.30.
Carrier gas HeN2H2  
Substrate      
Column diameter (mm) 0.260.270.320.320.32
Phase thickness (mum)  0.20.3 0.20
Tstart (C) 50.80.65.50.30.
Tend (C) 220.240.300.230.200.
Heat rate (K/min) 3.3.2.4.3.
Initial hold (min)   5.  
Final hold (min)    10. 
I 1478.1460.1448.1455.1460.
ReferenceDzumayev, Tsibulskaya, et al., 1995Ramanoelina, Viano, et al., 1994Demarne and van der Walt, 1993Binder, Benson, et al., 1990Ronse and De Pooter, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1BP-1SE-30SE-30
Column length (m) 25.60.50.40.30.
Carrier gas   H2He 
Substrate      
Column diameter (mm) 0.330.320.300.50 
Phase thickness (mum)    0.75 
Tstart (C) 45.50.40.30.50.
Tend (C) 180.250.250.220.240.
Heat rate (K/min) 3.4.10.3.4.
Initial hold (min) 3.0.11. 2.
Final hold (min)  5.  10.
I 1451.1454.1465.1456.1452.
ReferenceWyllie, Brophy, et al., 1990Binder and Flath, 1989Brophy, Davies, et al., 1989de Pooter, de Buyck, et al., 1989Ramaswami, Briscese, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101SE-30SE-30+IgepalSE-30+Igepal
Column length (m) 50.50.30.100.100.
Carrier gas      
Substrate      
Column diameter (mm) 0.300.30 0.250.25
Phase thickness (mum)      
Tstart (C) 40.40.50.70.70.
Tend (C) 230.230.240.170.170.
Heat rate (K/min) 3.53.54.1.1.
Initial hold (min) 5.5.2.  
Final hold (min)   10.  
I 1458.1476.1452.1478.1479.
ReferenceNykanen, 1986Nykanen, 1986Ramaswami, Briscese, et al., 1986Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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