Germacrene D

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-12(2)15-10-8-13(3)6-5-7-14(4)9-11-15/h7-8,10,12,15H,3,5-6,9,11H2,1-2,4H3/b10-8-,14-7-
IUPAC Standard InChIKey: GAIBLDCXCZKKJE-BZXLUOIMSA-N
CAS Registry Number: 23986-74-5
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: (S,1Z,6Z)-8-Isopropyl-1-methyl-5-methylenecyclodeca-1,6-diene; D-Germacrene; 1(10),4(14),5-Germacratriene; (-)-Germacrene D; 1,6-Cyclodecadiene, 1-methyl-5-methylene-8-(1-methylethyl)-, [s-(E,E)]-
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Information on this page:
Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5 MS	DB-5	RTX-1	RTX-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	100.
T_end (C)	240.	240.	230.	230.	260.
Heat rate (K/min)	3.	3.	2.	2.	10.
Initial hold (min)					1.
Final hold (min)			5.	5.	10.
I	1485.	1482.	1479.	1479.	1486.
Reference	Pinheiro, de Queiros, et al., 2013	Rodriques, Amorim, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Boukhris, Bouaziz, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega-5	HP-5 MS	HP-5 MS	HP-5 MS	CP-Sil 5 CB
Column length (m)	25.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.15
T_start (C)	50.	80.	40.	50.	50.
T_end (C)	220.	240.	250.	250.	220.
Heat rate (K/min)	3.	4.	3.	7.
Initial hold (min)	1.	3.	1.	1.
Final hold (min)	5.	10.	3.	5.
I	1479.	1475.	1486.	1486.	1490.
Reference	Dell'Agli, Sanna, et al., 2012	Dutra, Pittella, et al., 2012	Jian-Yu, Zhu, et al., 2012	Zouari, Ayadi, et al., 2012	Ameen, Usman, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	DB-5	VF-5 MS	VF-5 MS
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	30.	30.
T_end (C)	240.	180.	240.	260.	260.
Heat rate (K/min)	3.	2.	3.	2.	2.
Initial hold (min)
Final hold (min)				28.	28.
I	1485.	1472.	1480.	1485.	1485.
Reference	Bertoli, Lepnardi, et al., 2011	Hammami, Kamoun, et al., 2011	Karimi, Farmani, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30 MS	CP-Sil 5 CB	Methylsiloxane + 5 % Ph-groups	DB-5	RTX-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.26	0.25	0.25	0.25
T_start (C)	50.	45.	60.	35.	60.
T_end (C)	250.	280.	230.	200.	210.
Heat rate (K/min)	5.	3.	7.	2.	3.
Initial hold (min)	5.		2.
Final hold (min)	10.	22.	20.
I	1474.	1482.	1465.	1475.	1479.
Reference	Menichini, Tundis, et al., 2011	Mothana, Hasson, et al., 2011	Nadim, Malik, et al., 2011	Pattiram, Lasekan, et al., 2011	Prasad, Moulekhi, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	ZB-5	DB-5	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Nitrogen	Nitrogen	Nitrogen	Helium	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	40.	60.	30.	50.
T_end (C)	200.	200.	250.	250.	250.
Heat rate (K/min)	5.	5.	4.	5.	5.
Initial hold (min)	5.	5.	1.	3.	5.
Final hold (min)		5.	10.	10.	5.
I	1494.	1494.	1487.	1521.	1480.
Reference	Vazques, Aimar, et al., 2011	Vazquez, Demmel, et al., 2011	Yousefzadi, Heidari, et al., 2011	Zarai, Kadri, et al., 2011	Abderrahim, Belhamel, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTx-1	RTX-1	DB-5	HP-5
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	300.	230.	230.	250.	240.
Heat rate (K/min)	50.	2.	2.	2.	3.
Initial hold (min)	5.				2.
Final hold (min)	5.	35.	30.
I	1480.	1479.	1479.	1485.	1484.
Reference	Bi Kouame, Bedi, et al., 2010	Dib, Bendahou, et al., 2010	Dib, Djabou, et al., 2010	Ho, Wang, et al., 2010	Kahriman, Tosun, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5 MS	DB-5 MS	DB-1	HP-5
Column length (m)	30.	30.	60.	25.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	70.	40.	60.	40.
T_end (C)	250.	290.	250.	250.	260.
Heat rate (K/min)	5.	5.	5.	4.	4.
Initial hold (min)	3.		15.	1.
Final hold (min)	15.		15.	10.	5.
I	1464.	1489.	1482.	1484.	1491.
Reference	Lazarevic, Palic, et al., 2010	Lazarevic, Radulovic, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Mirjalili, Salehi, et al., 2010	Miyazawa, Kawauchi, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5 MS	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	70.	70.
T_end (C)	240.	220.	220.	290.	290.
Heat rate (K/min)	3.	5.	5.	5.	5.
Initial hold (min)	5.	10.	10.
Final hold (min)				10.
I	1481.	1482.	1483.	1488.	1498.
Reference	Monsef-Esfahani, Miri, et al., 2010	Ogunwande, Flamini, et al., 2010	Ogunwande, Flamini, et al., 2010	Radulovic, Blagojevic, et al., 2010	Radulovic, Dordevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SLB-5 MS	DB-5	DB-5 MS	CP Sil 5 CB
Column length (m)	30.	10.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.10	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.10	0.25	0.25	0.15
T_start (C)	70.	50.	60.	60.	50.
T_end (C)	290.	250.	240.	240.	230.
Heat rate (K/min)	5.	10.	3.	3.	3.
Initial hold (min)
Final hold (min)	10.
I	1486.	1485.	1478.	1478.	1479.
Reference	Radulovic, Dordevic, et al., 2010, 2	Scandinaro, Tranchida, et al., 2010	Scherer, Wagner, et al., 2010	Silva, Pott, et al., 2010	Usman, Zubair, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	ZB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	60.	60.
T_end (C)	220.	220.	250.	230.	240.
Heat rate (K/min)	4.	4.	7.	10.	3.
Initial hold (min)	2.	2.	1.	2.
Final hold (min)	2.	2.	5.	10.
I	1459.	1475.	1491.	1503.	1485.
Reference	Xu, Tang, et al., 2010	Xu, Tang, et al., 2010	Zouari, Zouari, et al., 2010	Alagarmalai, Nestel, et al., 2009	Alim, Goze, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	OV-101	SE-54
Column length (m)	50.	50.	50.	50.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	70.	70.	60.
T_end (C)	220.	220.	220.	220.	260.
Heat rate (K/min)	2.	2.	2.	2.	2.
Initial hold (min)					5.
Final hold (min)					999.
I	1480.	1484.	1486.	1487.	1474.
Reference	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SPB-5	DB-5	HP-5 MS	DB-5
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	Helium	Nitrogen	Helium	Hydrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.53	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.50	0.25	0.25	0.32
T_start (C)	60.	50.	50.	30.	60.
T_end (C)	250.	210.	250.	230.	220.
Heat rate (K/min)	2.	3.	5.	8.	5.
Initial hold (min)	8.	5.	2.	5.	3.
Final hold (min)	15.	45.		10.
I	1497.	1497.	1485.	1500.	1480.
Reference	Farhat, Ginies, et al., 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009	Karlsson, Birgersson, et al., 2009	Kazemi and Akhavani, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5 MS	HP-5	RTX-1	RTX-1
Column length (m)	30.	30.	25.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	35.	50.	60.	60.	60.
T_end (C)	195.	250.	240.	230.	230.
Heat rate (K/min)	2.	2.	3.	2.	2.
Initial hold (min)	5.	5.
Final hold (min)	30.		7.	30.	30.
I	1475.	1520.	1482.	1479.	1480.
Reference	Kim and Chung, 2009	Koba, Sanda, et al., 2009	Maridass, 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	DB-5 MS
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	Helium	Nitrogen	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.32	0.25
T_start (C)	45.	40.	40.	60.	50.
T_end (C)	250.	250.	230.	220.	220.
Heat rate (K/min)	3.	3.	2.	5.	3.
Initial hold (min)	3.	1.		3.	2.
Final hold (min)	5.	10.		5.	70.
I	1485.	1486.	1485.	1485.	1474.
Reference	Porto, Decorti, et al., 2009	Rahimi-Nasrabadi, Gholivand, et al., 2009	Scrivanti, Anton, et al., 2009	Shafaghat and Sadeghi, 2009	Shimizu, Imayoshi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5MS	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	50.	50.	60.
T_end (C)	250.	240.	280.	280.	280.
Heat rate (K/min)	4.	5.	4.	9.	3.
Initial hold (min)	2.			3.
Final hold (min)	2.			3.
I	1489.	1480.	1448.	1470.	1481.
Reference	Su, Wang, et al., 2009	Wannes, Mhamdi, et al., 2009	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Baziou, Couladis, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Ultra 2	DB-5	SE-52	HP-5	DB-5
Column length (m)	50.	25.	50.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.11	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	50.	100.
T_end (C)	230.	300.	280.	300.	300.
Heat rate (K/min)	2.	6.5	3.	3.	20.
Initial hold (min)	5.	2.			2.
Final hold (min)	30.	7.	20.	30.	10.
I	1480.	1488.	1489.	1477.	1459.
Reference	Byun and Shin, 2008	Chieng, Assim, et al., 2008	Djarri, Medjroubi, et al., 2008	Isidorov, Lech, et al., 2008	Khokra, Prakash, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5MS	HP-5	SLB-5 MS	RTX-1	Elite-1
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	240.	100.	50.	60.	60.
T_end (C)	320.	240.	250.	230.	246.
Heat rate (K/min)	20.	5.	3.	2.	3.
Initial hold (min)	1.	2.	2.
Final hold (min)		5.	10.	35.
I	1488.	1480.	1478.	1477.	1475.
Reference	Kowalski, 2008	Lago, Romoff, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Paolini, Tomi, et al., 2008	Raj, Baby, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5 MS	BPX-5	RTX-5
Column length (m)	30.	30.	30.	7.5	20.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.10	0.18
Phase thickness (μm)	0.25	0.25	0.25	10.	0.20
T_start (C)	60.	50.	50.	60.	50.
T_end (C)	250.	280.	240.	240.	280.
Heat rate (K/min)	2.	5.	3.	3.	4.
Initial hold (min)	8.	1.			1.
Final hold (min)	15.	1.
I	1479.	1488.	1518.	1483.	1497.
Reference	Sahraoui, Vian, et al., 2008	Saidana, Mahjoub, et al., 2008	Sarikurkcu, Tepe, et al., 2008	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5MS	HP-5MS	CP Sil 5 CB
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	He	He	N2
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.32
Phase thickness (μm)	0.32	0.32	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	250.	220.	240.	240.	300.
Heat rate (K/min)	5.	5.	3.	3.	4.
Initial hold (min)	30.	3.
Final hold (min)		5.
I	1481.	1478.	1482.	1493.	1479.
Reference	Yassa and Akhani, 2008	Amiri, 2007	Andrade, Oliveira, et al., 2007	Argyropoulou, Daferera, et al., 2007	Baran, von Reuss, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-5MS	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	Helium	N2
Substrate
Column diameter (mm)	0.25	0.26	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	280.	240.	200.	280.	240.
Heat rate (K/min)	3.	3.	1.	4.	5.
Initial hold (min)			1.	5.	1.
Final hold (min)					4.
I	1470.	1482.	1473.	1476.	1480.
Reference	Basta, Pavlovic, et al., 2007	Bos, Woerdenbag, et al., 2007	Calyecac-cortero, Cibrian-Tovar, et al., 2007	Capetanos, Saroglou, et al., 2007	Cheraif, Ben Jannet, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-5 MS	DB-5	HP-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.26	0.25
T_start (C)	70.	60.	60.	60.	60.
T_end (C)	310.	200.	290.	240.	250.
Heat rate (K/min)	3.	2.	3.	4.	2.
Initial hold (min)	5.	2.		2.	8.
Final hold (min)	20.	10.		20.	15.
I	1481.	1474.	1482.	1484.	1473.
Reference	Coelho, Grosso, et al., 2007	Edris, Chizzola, et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	DBP-5	RTX-5 MS	HP-101
Column length (m)	60.	30.	25.	30.	25.
Carrier gas	Nitrogen	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.2
T_start (C)	60.	60.	40.	45.	70.
T_end (C)	250.	240.	250.	210.	200.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)	1.		1.		2.
Final hold (min)	10.	20.	10.
I	1487.	1485.	1456.	1481.	1439.
Reference	Ghasempour, Shirinpour, et al., 2007	Hachicha, Skanji, et al., 2007	Heravi and Sereshti, 2007	Hudaib and Aburjai, 2007	Jerkovic, Mastelic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	RTX-5Sil MS	ZB-5	DB-1
Column length (m)		30.	30.	30.	30.
Carrier gas	He	He	He		Helium
Substrate
Column diameter (mm)		0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	220.	300.	260.	220.	260.
Heat rate (K/min)	5.	3.	5.	4.	2.5
Initial hold (min)			2.	5.	1.
Final hold (min)	6.		10.	20.	20.
I	1480.	1469.	1487.	1482.	1464.
Reference	Kiran, Devi, et al., 2007	Limberger, Scopel, et al., 2007	Matasyoh, Matasyoh, et al., 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5	Methyl Silicone
Column length (m)	30.	30.	30.	25.	50.
Carrier gas	Helium	Helium	He	H2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.33
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	300.	220.	250.	240.	240.
Heat rate (K/min)	3.	4.	5.	3.	3.
Initial hold (min)
Final hold (min)
I	1450.	1486.	1469.	1481.	1480.
Reference	Moreno, Lima, et al., 2007	Morteza-Semnani, Saeedi, et al., 2007	Nori-Shargh, Raftari, et al., 2007	Oliveira, Leitão, et al., 2007	Ozcan and Chalchat, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SPB-5	BPX-5	DB-1	HP-5
Column length (m)	25.	30.	50.	60.	30.
Carrier gas	Helium	He	He	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	1.	0.25	0.25
T_start (C)	100.	50.	50.	60.	40.
T_end (C)	280.	250.	300.	250.	260.
Heat rate (K/min)	4.	2.	4.	4.	4.
Initial hold (min)	3.		1.	1.
Final hold (min)	5.		10.	10.
I	1485.	1477.	1529.	1487.	1476.
Reference	Phutdhawong, Kawaree, et al., 2007	Raal, Orav, et al., 2007	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Ristic, Krivokuca-Dokic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-1	DBP-5	DB-5	DB-1
Column length (m)	60.	60.	25.	30.	60.
Carrier gas	Hydrogen		Helium	He	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	260.	250.	250.	320.	250.
Heat rate (K/min)	4.	5.	3.	10.	5.
Initial hold (min)			1.
Final hold (min)	20.		10.	4.	10.
I	1484.	1479.	1456.	1479.	1494.
Reference	Rojas, Velasco, et al., 2007	Salehi, Asghari, et al., 2007	Sereshti and Samadi, 2007	Smelcerovic, Spiteller, et al., 2007	Sonboli, Kanani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	Elite-5MS	HP-5MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas			He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	210.	250.	280.	280.	280.
Heat rate (K/min)	2.	2.	4.	3.	3.
Initial hold (min)			5.
Final hold (min)	33.	33.	10.
I	1482.	1482.	1485.	1442.	1485.
Reference	Sylvestre, Longtin, et al., 2007	Sylvestre, Pichette, et al., 2007	Tava, Pecetti, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	250.	240.	250.	300.	300.
Heat rate (K/min)	3.	5.	5.	3.	3.
Initial hold (min)	5.	3.	30.
Final hold (min)	10.	10.
I	1462.	1471.	1481.	1465.	1474.
Reference	Vichi, Riu-Aumatell, et al., 2007	Wenguang, Wenlai, et al., 2007	Yassa and Akhani, 2007	Apel, Sobral, et al., 2006	Apel, Sobral, et al., 2006, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	DB-5	HP-5	BP-1
Column length (m)	30.	25.	30.	60.	50.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.22
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	40.	80.	50.	60.	60.
T_end (C)	260.	270.	265.	250.	220.
Heat rate (K/min)	4.	10.	2.5	3.	2.
Initial hold (min)	5.		1.
Final hold (min)			20.		20.
I	1472.	1483.	1485.	1491.	1478.
Reference	Askari and Sefidkon, 2006	Ayoub, Al-Azizi, et al., 2006	Bazargani, Almasirad, et al., 2006	Bertrand, Comte, et al., 2006	Boti, Yao, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	SPB-1	HP-5	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	Helium	He	N2
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.20	0.25	0.25	0.25
T_start (C)	60.	70.	50.	70.	60.
T_end (C)	280.	220.	300.	230.	230.
Heat rate (K/min)	3.	3.	5.	2.	3.
Initial hold (min)			5.	2.
Final hold (min)		15.		20.	15.
I	1490.	1466.	1485.	1476.	1480.
Reference	Bozin, Mimicá-Dukic, et al., 2006	Cavaleiro, Pinto, et al., 2006	Champagnat, Figueredo, et al., 2006	Choi, 2006	Damjanovic, Skala, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	BP-1	HP-1	HP-5
Column length (m)	30.	30.	50.	50.	30.
Carrier gas		Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.26	0.22	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	280.	290.	220.	250.	300.
Heat rate (K/min)	4.	3.	2.	2.	5.
Initial hold (min)					5.
Final hold (min)			20.	60.	5.
I	1478.	1482.	1480.	1470.	1481.
Reference	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Fanciullino, Tomi, et al., 2006	Fernandez, Pintaric, et al., 2006	Figuérédo, Cabassu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-5	DB-1	DB-5	DB-1
Column length (m)	50.	30.	60.	30.	60.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	250.	210.	240.	240.	240.
Heat rate (K/min)	2.	2.	5.	5.	5.
Initial hold (min)		2.	2.	2.	2.
Final hold (min)	40.	33.
I	1473.	1482.	1489.	1480.	1489.
Reference	Filippi, Lanfranchi, et al., 2006	Garneau F.X., Collin G., et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5MS	BP-1	Methyl Silicone
Column length (m)	30.	30.	30.		25.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25		0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	60.	90.
T_end (C)	240.	240.	260.	220.	220.
Heat rate (K/min)	5.	4.	4.	5.	7.
Initial hold (min)	2.				2.
Final hold (min)				6.
I	1480.	1480.	1480.	1480.	1491.
Reference	Gohari A.R., Hadjiakhoondi A., et al., 2006	Ibañez and Usubillaga, 2006	Ibanez and Usubillaga, 2006	Kiran, Bhavani, et al., 2006	Kitchlu, Bakshi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-1	HP-5	DB-1	CP Sil 5 CB
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	He	He		N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	100.	70.	50.
T_end (C)	260.	300.	240.	230.	300.
Heat rate (K/min)	5.	4.	5.	2.	4.
Initial hold (min)	2.		2.	2.
Final hold (min)	13.		5.	20.
I	1481.	1481.	1480.	1474.	1470.
Reference	Kucuk, Gulec, et al., 2006	Kula, Izydorczyk, et al., 2006	Lago, Soares, et al., 2006	Lan Phi N.T., Nishiyama C., et al., 2006	Lis and Milczarek, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	5 % Phenyl methyl siloxane	DB-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	200.	280.	250.	220.	220.
Heat rate (K/min)	5.	3.	3.	4.	4.
Initial hold (min)			5.		5.
Final hold (min)		30.
I	1481.	1457.	1485.	1488.	1488.
Reference	Martin, Joseph, et al., 2006	Marongiu, Piras, et al., 2006	Mirza, Navaei, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	CP-Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.15
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	260.	220.	250.	250.	230.
Heat rate (K/min)	4.	4.	4.	3.	3.
Initial hold (min)	4.	5.		5.
Final hold (min)
I	1488.	1488.	1487.	1483.	1482.
Reference	Morteza-Semnani, Saeedi, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Najafpour Navaei, Mirza, et al., 2006	Navaei and Mirza, 2006	Olawore, Usman, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	SE-52	DB-1	HP-5
Column length (m)	30.	25.	50.	50.	30.
Carrier gas	He	N2	Helium	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.15		0.25	0.25
T_start (C)	50.	50.	50.	95.	60.
T_end (C)	250.	200.	240.	240.	220.
Heat rate (K/min)	2.	4.	3.	4.	5.
Initial hold (min)		3.			10.
Final hold (min)
I	1474.	1487.	1480.	1466.	1487.
Reference	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006	Ozcan, Chalchat, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Pintore G., Chessa M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Hydrogen	Hydrogen	H2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	50.	60.	60.
T_end (C)	280.	280.	280.	280.	240.
Heat rate (K/min)	4.	4.	4.	3.	3.
Initial hold (min)	4.	4.	2.
Final hold (min)			10.
I	1480.	1482.	1480.	1451.	1484.
Reference	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Sauri-Duch, et al., 2006	Pitarokili, Tzakou, et al., 2006	Potzernheim, Bizzo, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-1	DB-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	70.	40.	40.
T_end (C)	200.	280.	230.	250.	260.
Heat rate (K/min)	2.	4.	2.	4.	2.
Initial hold (min)			2.		5.
Final hold (min)	60.		20.		20.
I	1479.	1482.	1477.	1473.	1478.
Reference	Rout, Naik, et al., 2006	Sajjadi, 2006	Sawamura, Onishi, et al., 2006	Sefidkon, Jamzad, et al., 2006	Senatore, Landolfi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	DB-5	DB-1	CP Sil 5 CB
Column length (m)	30.	25.	30.	60.	25.
Carrier gas	He	N2	H2	Helium
Substrate
Column diameter (mm)	0.25	0.2	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.18	0.25
T_start (C)	60.	30.	60.	60.	50.
T_end (C)	280.	280.	240.	250.	230.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)	5.
Final hold (min)				10.
I	1481.	1499.	1479.	1480.	1482.
Reference	Setzer, Noletto, et al., 2006	Shafi, Jose, et al., 2006	Silva, Oliveira, et al., 2006	Sonboli, Mirjalili, et al., 2006	Tesso, Kubeczka, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	HP-5	SPB-1	SPB-1	HP-5
Column length (m)	25.	25.	50.	30.	30.
Carrier gas	N2	H2	He	He	He
Substrate
Column diameter (mm)	0.3	0.32	0.2	0.25	0.32
Phase thickness (μm)	0.15	0.52	0.33	0.25	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	210.	280.	220.	250.	260.
Heat rate (K/min)	2.	2.5	4.	4.	5.
Initial hold (min)	5.	5.	1.	1.	2.
Final hold (min)			10.	10.	14.
I	1508.	1480.	1471.	1458.	1480.
Reference	Tonzibo, Coffy, et al., 2006	Wang, Kong, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yayli, Gülec, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	HP-5MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	260.	275.	210.	280.	240.
Heat rate (K/min)	5.	4.	3.	3.	3.
Initial hold (min)	2.		5.
Final hold (min)	14.
I	1483.	1487.	1472.	1456.	1481.
Reference	Yayli, Gülec, et al., 2006	Asadipour, Mehrabani, et al., 2005	Askari and Sefidkon, 2005	Basta, Tzakou, et al., 2005	Busman, Zoghbi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	Methyl Silicone
Column length (m)	50.	25.	30.	30.	60.
Carrier gas			He	He	He
Substrate
Column diameter (mm)	0.3	0.25	0.25	0.25	0.3
Phase thickness (μm)	0.25	0.15	0.25	0.25
T_start (C)	60.	40.	60.	60.	50.
T_end (C)	240.	220.	240.	240.	240.
Heat rate (K/min)	2.	3.	3.	3.	3.
Initial hold (min)		5.
Final hold (min)
I	1480.	1480.	1481.	1489.	1482.
Reference	Chagonda and Chalchat, 2005	Chagonda and Chalchat, 2005, 2	Chaverri and Cicció, 2005	Chaverri and Cicció, 2005	Chalchat and Özcan, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX5	HP-5	CP Sil 8 CB	DB-1	DB-5
Column length (m)	25.	25.	30.	60.	30.
Carrier gas	Helium	He	He	N2	He
Substrate
Column diameter (mm)	0.22	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	80.	60.	60.
T_end (C)	320.	240.	200.	250.	300.
Heat rate (K/min)	5.	3.	3.	5.	3.
Initial hold (min)	5.		5.		3.
Final hold (min)		7.	5.	10.
I	1490.	1479.	1461.	1492.	1475.
Reference	Dickschat, Bode, et al., 2005	Duarte, Figueira, et al., 2005	Facey, Porter, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005	Ferraz, Limberger, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-5	HP-5	HP-5MS	HP-5MS
Column length (m)	50.	30.	30.	30.	25.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	250.	30.	300.	200.	250.
Heat rate (K/min)	2.	4.	5.	4.	3.
Initial hold (min)	60.	3.	5.	30.	3.
Final hold (min)		15.	5.		10.
I	1472.	1485.	1481.	1476.	1480.
Reference	Fernandez, Lizzani-Cuvelier, et al., 2005	Ferretti, Maggi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Gauvin and Smadja, 2005	Ghasemi Y., Faridi P., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	CP Sil 5 CB	CP Sil 5 CB	HP-5	DB-1
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	N2	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.25
T_start (C)	60.	60.	60.	40.	50.
T_end (C)	300.	250.	250.	240.	265.
Heat rate (K/min)	3.	5.	5.	4.	2.5
Initial hold (min)					1.
Final hold (min)		10.	10.		20.
I	1476.	1491.	1494.	1461.	1463.
Reference	Grombone-Guaratini, Silva-Brandão, et al., 2005	Jassbi, Mehrdad, et al., 2005	Jassbi, Mehrdad, et al., 2005	Jovanovic, Kitic, et al., 2005	Khanavi, Ghasemian, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-5MS	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He		Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	35.	60.	50.
T_end (C)	250.	280.	280.	280.	250.
Heat rate (K/min)	4.	4.	4.	3.	3.
Initial hold (min)	5.	2.	2.	30.	10.
Final hold (min)					5.
I	1479.	1488.	1488.	1454.	1492.
Reference	Khajeh, Yamini, et al., 2005	Kowalski and Wolski, 2005	Kowalski, 2005	Marongiu, Piras, et al., 2005	Melkani, Dev, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.15
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	220.	220.	250.	230.
Heat rate (K/min)	4.	4.	4.	3.	3.
Initial hold (min)	5.	5.	4.	5.
Final hold (min)
I	1485.	1480.	1482.	1480.	1478.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005, 2	Morteza-Semnani and Saeedi, 2005	Najafpour Navaei, Mirza, et al., 2005	Olawore, Ogunwande, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5MS	DB-1	CP Sil 5 CB
Column length (m)	30.	50.	30.	60.	30.
Carrier gas	He	N2		He	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	95.	60.	50.	40.
T_end (C)	250.	240.	280.	250.	220.
Heat rate (K/min)	5.	4.	3.	4.	4.
Initial hold (min)	0.5				1.
Final hold (min)	2.
I	1482.	1476.	1485.	1472.	1485.
Reference	Özel, Gögüs, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Petrakis, Roussis, et al., 2005	Rasooli and Owlia, 2005	Rohloff and Bones, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	HP-5MS	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	280.	275.	280.	220.
Heat rate (K/min)	5.	4.	4.	4.	3.
Initial hold (min)					4.
Final hold (min)
I	1480.	1479.	1481.	1480.	1485.
Reference	Saeidnia, Gohari, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005	Sajjadi, 2005	Salehi, Sefidkon, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	DB-5	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	50.	40.	40.	60.
T_end (C)	250.	265.	240.	260.	280.
Heat rate (K/min)	5.	2.5	4.	2.	3.
Initial hold (min)		1.		5.	5.
Final hold (min)	10.	20.		20.
I	1484.	1465.	1478.	1478.	1481.
Reference	Salehi, Sonboli, et al., 2005	Sarkhail, Amin, et al., 2005	Sefidkon and Jamzad, 2005	Senatore, Apostolides Arnold, et al., 2005	Setzer, Noletto, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	PE-5	DB-5	HP-5MS	RTX-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	230.	230.	280.	25.
Heat rate (K/min)	3.	5.	3.	3.	5.
Initial hold (min)		2.
Final hold (min)		4.	20.		10.
I	1475.	1479.	1485.	1480.	1485.
Reference	Simoes-Pires C.A., Debenedetti S., et al., 2005	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Sonboli, Salehi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BP-1	DB-5	RTX-5	HP-5 MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2			He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.50
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	250.	220.	210.	220.	260.
Heat rate (K/min)	5.	5.	2.	3.	3.
Initial hold (min)			2.
Final hold (min)	10.	15.	33.		20.
I	1484.	1475.	1486.	1479.	1480.
Reference	Sonboli, Salehi, et al., 2005, 2	Srivastava, Srivastava, et al., 2005	Stevanovic, Garneau, et al., 2005	Szafranek, Chrapkowska, et al., 2005	Topçu, Barla, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-5 MS	DB-1	HP-5MS
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	He	He	Helium	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	90.	40.
T_end (C)	280.	280.	240.	240.	220.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)					5.
Final hold (min)					10.
I	1442.	1449.	1485.	1460.	1462.
Reference	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005	Urdampilleta, Amat, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Vichi, Riu-Aumatell, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5	HP-5	HP-5	CP Sil 5 CB
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	He	Helium	He	He	N2
Substrate
Column diameter (mm)	0.2	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.32	0.25
T_start (C)	50.	40.	60.	60.	50.
T_end (C)	220.	250.	260.	250.	200.
Heat rate (K/min)	4.	5.	5.	5.	5.
Initial hold (min)	3.	2.	2.	3.
Final hold (min)	30.	5.	13.
I	1479.	1472.	1481.	1489.	1482.
Reference	Wong, Lee, et al., 2005	N/A	Yayli, Yasar, et al., 2005	Aghel, Yamini, et al., 2004	Agnaniet, Menut, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	N2	N2	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	90.	60.	50.	40.	60.
T_end (C)	220.	240.	200.	230.	240.
Heat rate (K/min)	7.	2.	5.	2.	3.
Initial hold (min)	2.
Final hold (min)	5.
I	1471.	1485.	1484.	1480.	1480.
Reference	Agnihotri, Thappa, et al., 2004	Cicció, 2004	Fekam Boyom, Fotio, et al., 2004	González, Guerra, et al., 2004	JAvidnia, Mojab, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	SE-54	DB-5	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	50.
T_end (C)	280.	300.	260.	300.	230.
Heat rate (K/min)	4.	4.	2.	3.	5.
Initial hold (min)	4.		5.		2.
Final hold (min)					10.
I	1481.	1480.	1472.	1455.	1456.
Reference	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Lago, de Ávila, et al., 2004	Li and Jiang, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	DB-5	HP-5MS	BP-1
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	N2		He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	300.	300.	210.	280.	220.
Heat rate (K/min)	3.	4.	2.	3.	5.
Initial hold (min)			2.
Final hold (min)			33.
I	1464.	1480.	1483.	1477.	1481.
Reference	Limberger, Sobral, et al., 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004	Malencic, Couladis, et al., 2004	Mallavarapu, Kulkarni, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	DB-1	NB-30	NB-30
Column length (m)	30.	30.	60.	50.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	275.	280.	270.	250.	250.
Heat rate (K/min)	4.	3.	4.	2.	2.
Initial hold (min)
Final hold (min)
I	1483.	1490.	1476.	1478.	1478.
Reference	Mehrabani, Asadipour, et al., 2004	Mimica-Dukic, Bozin, et al., 2004	Nik, Mirza, et al., 2004	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	NB-30	DB-1	DB-5	HP-5MS
Column length (m)	30.	50.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	50.	50.	35.	60.
T_end (C)	220.	250.	250.	220.	280.
Heat rate (K/min)	3.	2.	4.	2.5	4.
Initial hold (min)
Final hold (min)				6.
I	1473.	1478.	1472.	1485.	1472.
Reference	Palá-Paúl, Brophy, et al., 2004	Raal, Paaver, et al., 2004	Rasooli and Razzaghi Abyaneh, 2004	Rohloff, Mordal, et al., 2004	Sadeghpour, Asghari, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-1	DB-1	HP-1	DB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	50.	40.	40.	40.
T_end (C)	280.	265.	280.	260.	250.
Heat rate (K/min)	4.	2.5	4.	2.	2.
Initial hold (min)		1.	5.	5.	5.
Final hold (min)		20.		20.	20.
I	1478.	1465.	1473.	1476.	1476.
Reference	Sajjadi and Shahpiri, 2004	Sarkhail, Amin, et al., 2004	Sefidkon and Shaabani, 2004	Senatore, Napolitano, et al., 2004	Senatore, Rigano, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	CP Sil 5 CB	DB-5	BPX-5
Column length (m)	25.	30.	20.	30.	25.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.5	0.25	0.25	0.25	1.
T_start (C)	30.	60.	100.	60.	60.
T_end (C)	280.	300.	270.	300.	250.
Heat rate (K/min)	3.	3.	8.	3.	3.
Initial hold (min)			2.		5.
Final hold (min)					10.
I	1499.	1474.	1468.	1485.	1510.
Reference	Shafi, Nambiar, et al., 2004	Suyenaga, Apel, et al., 2004	Thappa, Bakshi, et al., 2004	Tirillini, Pellegrino, et al., 2004	Vilaseca, Guy, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5	HP-5MS	Methyl Silicone
Column length (m)	30.	30.	30.	30.	12.5
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	100.	60.	50.
T_end (C)	275.	220.	240.	280.	270.
Heat rate (K/min)	4.	5.	5.	3.	4.
Initial hold (min)		10.	2.
Final hold (min)			5.
I	1479.	1482.	1480.	1478.	1468.
Reference	Afsharypuor and Jahromy, 2003	Bertoli, Menichini, et al., 2003	Chaves, Lago, et al., 2003	Couladis, Özcan, et al., 2003	Curini, Bianchi, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-1	HP-5MS	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	250.	220.	200.	275.	280.
Heat rate (K/min)	4.	5.	5.	4.	4.
Initial hold (min)		20.
Final hold (min)		20.
I	1472.	1487.	1461.	1481.	1480.
Reference	Dabiri and Sefidkon, 2003	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	Methyl Silicone	RSL-200	RSL-200	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	H2	H2	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	40.	35.
T_end (C)	275.	250.	280.	280.	280.
Heat rate (K/min)	4.	2.	6.	6.	5.
Initial hold (min)		2.	5.	5.	2.5
Final hold (min)		5.	5.	5.
I	1485.	1476.	1481.	1469.	1470.
Reference	Hajhashemi, Ghannadi, et al., 2003	Jayaprakasha, Rao, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Kanjilal, Kotoky, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	250.	240.	280.	280.
Heat rate (K/min)	5.	3.	3.	3.	3.
Initial hold (min)
Final hold (min)				30.	30.
I	1472.	1478.	1482.	1469.	1476.
Reference	Lago, de Ávila, et al., 2003	Limberger, Simões-Pires, et al., 2003	Maia, Taveira, et al., 2003	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	DB-1	DB-1	HP-5
Column length (m)	50.	25.	60.	60.	30.
Carrier gas	He		He	He	Helium
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.39	0.25	0.25
T_start (C)	50.	60.	50.	50.	70.
T_end (C)	220.	220.	270.	270.	210.
Heat rate (K/min)	3.	5.	4.	4.	2.
Initial hold (min)	2.
Final hold (min)					60.
I	1486.	1480.	1472.	1476.	1479.
Reference	Masotti, Juteau, et al., 2003	Mazloomifar, Saber-Tehrani, et al., 2003	Mirza and Nik, 2003	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CP Sil 5 CB	DB-1	DB-5	HP-5
Column length (m)	50.	25.	50.	30.	30.
Carrier gas	He	H2	N2	H2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.15	0.25	0.25	0.25
T_start (C)	50.	50.	95.	60.	60.
T_end (C)	250.	230.	240.	280.	280.
Heat rate (K/min)	2.	3.	4.	4.	3.
Initial hold (min)				10.
Final hold (min)				40.
I	1467.	1466.	1471.	1480.	1461.
Reference	Orav, Kailas, et al., 2003	Oyedeji, Ekundayo, et al., 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	NB-30	HP-5	HP-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.5	0.25	0.25	0.25
T_start (C)	75.	50.	60.	60.	40.
T_end (C)	220.	250.	280.	280.	260.
Heat rate (K/min)	3.	2.	4.	4.	2.
Initial hold (min)	4.				5.
Final hold (min)
I	1474.	1478.	1482.	1479.	1480.
Reference	Priestap, van Baren, et al., 2003	Raal, Arak, et al., 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2	Senatore and Bruno, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	HP-5	DB-1	HP-5
Column length (m)	60.	60.	60.	60.	25.
Carrier gas	He			N2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.53
T_start (C)	50.	40.	40.	70.	40.
T_end (C)	280.	250.	250.	230.	280.
Heat rate (K/min)	4.	5.	5.	2.	4.
Initial hold (min)		15.	15.	2.
Final hold (min)				20.
I	1473.	1480.	1480.	1481.	1477.
Reference	Shahmir, Ahmadi, et al., 2003	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003	Tu, Onishi, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.32	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	4.	4.	5.	3.
Initial hold (min)				30.
Final hold (min)
I	1477.	1479.	1485.	1482.	1481.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	CP Sil 5 CB	DB-5	OV-101
Column length (m)	25.	60.	25.	30.	25.
Carrier gas	N2	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.249	0.32
Phase thickness (μm)	0.25	0.25	0.4	0.25
T_start (C)	50.	50.	60.	60.	50.
T_end (C)	250.	280.	260.	300.	200.
Heat rate (K/min)	4.	4.	5.	3.	5.
Initial hold (min)
Final hold (min)	10.		40.	5.
I	1480.	1473.	1471.	1477.	1486.
Reference	Zrira, Elamrani, et al., 2003	Ahmadi, Mirza, et al., 2002	Azaz. D., Demirci, et al., 2002	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	5 % Phenyl methyl siloxane	DB-5MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	75.	60.	60.
T_end (C)	280.	220.	200.	280.	280.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			4.
Final hold (min)	30.	15.	8.
I	1474.	1467.	1485.	1483.	1483.
Reference	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Cicció and Gómez-Laurito, 2002	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	DB-1	SE-30	RSL-200
Column length (m)	25.	30.	30.	50.	30.
Carrier gas	N2	He	H2	He	H2
Substrate
Column diameter (mm)	0.50	0.25	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	70.	40.
T_end (C)	220.	240.	245.	240.	280.
Heat rate (K/min)	5.	3.	3.	4.	6.
Initial hold (min)			20.		5.
Final hold (min)	10.				5.
I	1480.	1482.	1452.	1485.	1487.
Reference	Das, Ram, et al., 2002	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Jirovetz, Buchbauer, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	CP Sil 8 CB	DB-5	DB-1	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	H2	He		He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.23	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	50.	50.	40.	50.	60.
T_end (C)	280.	220.	210.	200.	240.
Heat rate (K/min)	6.	3.	2.	3.	3.
Initial hold (min)	5.	2.	2.	3.
Final hold (min)	5.		33.	30.
I	1475.	1484.	1485.	1472.	1479.
Reference	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002	Kabouss, Charrouf, et al., 2002	Khallouki, Younos, et al., 2002	Kobaisy, Tellez, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	DB-5	HP-5	DB-5
Column length (m)	30.	25.	30.	30.	25.
Carrier gas	He	He	He		N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.23
Phase thickness (μm)	0.25		0.25	0.25	0.15
T_start (C)	35.	50.	60.	60.	50.
T_end (C)	280.	200.	250.	275.	250.
Heat rate (K/min)	3.	5.	3.	4.	3.
Initial hold (min)	2.			4.
Final hold (min)	15.
I	1488.	1487.	1476.	1472.	1479.
Reference	Krauze-Baranowska, Mardarowicz, et al., 2002	Kuiate, Bessière, et al., 2002	Limberger, Simões-Pires, et al., 2002	Lockwood, Asghari, et al., 2002	Mahmout, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	OV-101	CP Sil 5 CB	DB-1
Column length (m)	30.	30.	25.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	240.	240.	200.	220.	250.
Heat rate (K/min)	3.	3.	5.	5.	4.
Initial hold (min)					10.
Final hold (min)
I	1480.	1480.	1478.	1480.	1486.
Reference	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Menut, Bessière, et al., 2002	Monfared, Davarani, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-5MS	HP-1	DB-5
Column length (m)	50.	50.	30.	50.	25.
Carrier gas	He	N2	He	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.32	0.25	0.2
Phase thickness (μm)	0.5	0.25	0.25	0.25
T_start (C)	50.	80.	40.	90.	60.
T_end (C)	250.	225.	280.	220.	220.
Heat rate (K/min)	2.	4.	4.	3.	3.
Initial hold (min)
Final hold (min)			5.
I	1470.	1464.	1489.	1475.	1486.
Reference	Orav, Kailas, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Phutdhawong, Korth, et al., 2002	Priestap, van Baren, et al., 2002	Schwob, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	HP-5	DB-1
Column length (m)	60.	60.	50.	30.	60.
Carrier gas	He	He	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	40.	50.
T_end (C)	250.	280.	240.	280.	250.
Heat rate (K/min)	4.	4.	3.	4.	4.
Initial hold (min)		5.			5.
Final hold (min)
I	1476.	1474.	1451.	1480.	1495.
Reference	Sefidkon, Dabiri, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velickovic, Randjelovic, et al., 2002	Yamini, Sefidkon, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	DB-1	Optima-1	HP-5
Column length (m)	30.	30.	60.	25.	30.
Carrier gas	He	He	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.248	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	270.	240.	220.	250.	220.
Heat rate (K/min)	3.	3.	3.	3.	5.
Initial hold (min)			5.	3.	10.
Final hold (min)			22.
I	1481.	1483.	1485.	1470.	1481.
Reference	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Bailac, Dellacasa, et al., 2001	Brun, Bessière, et al., 2001	Campeol, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	HP-5	HP-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	220.	280.	280.	220.	220.
Heat rate (K/min)	3.	4.	4.	5.	5.
Initial hold (min)	5.	5.	5.	10.	10.
Final hold (min)	15.
I	1487.	1481.	1483.	1481.	1481.
Reference	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Flamini, Cioni, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	Optima-5	RTX-1	CBP-1	DB-1
Column length (m)	30.	30.	30.	25.	60.
Carrier gas	N2	He	N2	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	50.	60.	50.	50.
T_end (C)	220.	250.	300.	210.	270.
Heat rate (K/min)	5.	3.	4.	3.	4.
Initial hold (min)		3.		2.
Final hold (min)
I	1480.	1484.	1482.	1483.	1471.
Reference	Gupta, Mallavarapu, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Kalemba, Marschall, et al., 2001	Ly, Yamauchi, et al., 2001	Mirza, Ahmadi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	DB-5	DB-5
Column length (m)	50.	50.	30.	60.	30.
Carrier gas	He	He	N2	He	H2
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.5		0.25		0.25
T_start (C)	50.	50.	80.	50.	60.
T_end (C)	250.	250.	225.	250.	285.
Heat rate (K/min)	2.	2.	4.	3.	3.
Initial hold (min)				5.
Final hold (min)
I	1471.	1470.	1450.	1480.	1477.
Reference	Orav, Kailas, et al., 2001	Orav and Kann, 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Rousis, Papadogianni, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	CP Sil 5 CB	CP-Sil 5 CB	HP-5 MS	PTE-5
Column length (m)	30.	25.	25.	30.	60.
Carrier gas	He	He	Nitrogen	Helium	H2
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.39	0.39	0.25	0.3
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	220.	220.	250.	285.
Heat rate (K/min)	3.	5.	5.	5.	4.3
Initial hold (min)				2.
Final hold (min)				5.
I	1483.0	1478.	1478.	1484.	1480.
Reference	Santos, Moreira, et al., 2001	Sayyah, Kamalinejad, et al., 2001	Sayyah, Kamalinejad, et al., 2001, 2	Shang, Hu, et al., 2001	Stojanovic, Palic, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP Sil 5 CB	DB-1	RSL-200
Column length (m)	30.	25.	25.	33.	60.
Carrier gas	He	He	He	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.4	0.4	0.50	0.25
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	240.	260.	260.	135.	250.
Heat rate (K/min)	3.	5.	5.	20.	6.
Initial hold (min)		40.	40.	2.
Final hold (min)
I	1479.	1472.	1472.	1490.	1471.
Reference	Tellez M., Estell R., et al., 2001	Baser, Özek, et al., 2000	Baser, Özek, et al., 2000	Feger, Brandauer, et al., 2000	Jirovetz, Puschmann, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	OV-101	OV-101	DB-1
Column length (m)	30.	25.	50.	25.	60.
Carrier gas	N2	N2	Nitrogen	N2	N2
Substrate
Column diameter (mm)	0.22	0.33	0.25	0.25	0.25
Phase thickness (μm)	0.25	1.0			0.25
T_start (C)	70.	60.	40.	50.	75.
T_end (C)	230.	275.	200.	200.	220.
Heat rate (K/min)	4.	4.	2.	5.	4.
Initial hold (min)	2.		10.		1.
Final hold (min)	20.				8.
I	1470.	1473.	1480.	1481.	1492.
Reference	Mitiku, Sawamura, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Tamura, Boonbumrung, et al., 2000	Ayedoun, Adéoti, et al., 1999	Bailac, Dellacasa, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	OV-1	OV-1	OV-1	RTX-1
Column length (m)	25.	25.	25.	25.	30.
Carrier gas	Hydrogen	Hydrogen	Hydrogen	Hydrogen	N2
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.30	0.30	0.30	0.30	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	200.	200.	200.	200.	300.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)	1.	1.	1.	1.
Final hold (min)	10.	10.	10.	10.
I	1453.	1453.	1454.	1455.	1480.
Reference	Bicchi, Binello, et al., 1999	Bicchi, Binello, et al., 1999	Bicchi, Binello, et al., 1999	Bicchi, Binello, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	OV-101	OV-1	DB-1
Column length (m)	25.	25.	50.	25.	50.
Carrier gas	He		N2	H2	He
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.25
Phase thickness (μm)	0.25			0.25	0.25
T_start (C)	50.	50.	80.	40.	70.
T_end (C)	290.	200.	200.	220.	240.
Heat rate (K/min)	4.	5.	1.	3.	4.
Initial hold (min)				5.
Final hold (min)			20.	5.
I	1477.	1487.	1491.	1462.	1450.
Reference	Koulman, 1999	Kuiate, Zollo, et al., 1999	Menon, Chacko, et al., 1999	Oberhofer, Nikiforov, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	DB-1	DB-1	DB-5
Column length (m)	25.	25.	60.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.39	0.12	0.25	0.25	0.25
T_start (C)	60.	80.	40.	50.	60.
T_end (C)	220.	275.	280.	220.	240.
Heat rate (K/min)	5.	5.	4.	4.	3.
Initial hold (min)	5.	2.	5.
Final hold (min)	20.	10.
I	1481.	1457.	1481.	1485.	1480.
Reference	Rustaiyan, Masoudi, et al., 1999	Rycroft, Cole, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Mirza, 1999	Tellez, Canel, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SPB-5	DB-5	OV-1	DB-5
Column length (m)	50.	50.	30.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.32	0.25	0.32	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	100.	60.	60.	50.	60.
T_end (C)	220.	240.	240.	250.	240.
Heat rate (K/min)	1.	3.	3.	10.	3.
Initial hold (min)	1.			5.
Final hold (min)		20.		20.
I	1460.	1491.	1480.	1476.	1482.
Reference	Camciuc, Bessière, et al., 1998	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Kökdil, Kurucu, et al., 1998	Maia, Zohhbi, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-1	OV-101	CP Sil 5 CB
Column length (m)	25.	30.	60.	25.	25.
Carrier gas	He	Helium	He		He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.33	0.25	0.25		0.25
T_start (C)	70.	60.	50.	50.	60.
T_end (C)	290.	240.	280.	200.	300.
Heat rate (K/min)	3.	3.	4.	5.	6.
Initial hold (min)	8.		5.
Final hold (min)	20.
I	1501.	1481.	1473.	1481.	1465.
Reference	Poiana, Sicari, et al., 1998	Santos, Andrade, et al., 1998	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-1	OV-1	DB-1	DB-5
Column length (m)	30.	30.	30.		30.
Carrier gas	He	He			Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32		0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	65.	40.	40.	80.	60.
T_end (C)	300.	270.	270.	220.	240.
Heat rate (K/min)	4.	2.	2.	6.	3.
Initial hold (min)	2.	4.	4.
Final hold (min)
I	1464.	1461.	1460.	1474.	1480.
Reference	Elias, Simoneit, et al., 1997	Kökdil, Kurucu, et al., 1997	Kökdil, Tanker, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	DB-1	DB-1	HP-1
Column length (m)	30.	23.	60.	60.	25.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.32
Phase thickness (μm)		0.17	0.50	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	240.	250.	250.	250.	220.
Heat rate (K/min)	4.	5.	8.	2.5	4.
Initial hold (min)		3.	1.	5.	2.
Final hold (min)		30.	6.		20.
I	1480.	1470.	1473.	1486.	1470.
Reference	Zunino, Novillo-Newton, et al., 1997	Ayedoun, Adeoti, et al., 1996	Sagrero-Nieves and Bartley, 1996	Stashenko, Puertas, et al., 1996	Thanh, Dung, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	OV-1	HP-5	HP-5
Column length (m)	60.	60.	50.
Carrier gas	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.27
Phase thickness (μm)	0.25	0.25	0.2
T_start (C)	50.	70.	80.	40.	40.
T_end (C)	250.	270.	240.	210.	210.
Heat rate (K/min)	3.5	2.5	3.	2.	2.
Initial hold (min)	5.	5.
Final hold (min)
I	1475.	1477.	1485.	1481.	1482.
Reference	Stashenko, Torres, et al., 1995	Tirado, Stashenko, et al., 1995	Ramanoelina, Viano, et al., 1994	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	Methyl Silicone	Methyl Silicone	OV-101	OV-101
Column length (m)	50.	50.	50.	52.	52.
Carrier gas	H2	N2	N2	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.26	0.26
Phase thickness (μm)	0.3	0.17	0.17
T_start (C)	65.	80.	80.	40.	40.
T_end (C)	300.	200.	200.	200.	200.
Heat rate (K/min)	2.	2.	3.	3.	3.
Initial hold (min)	5.			0.	0.
Final hold (min)				0.	0.
I	1467.	1469.	1469.	1468.	1466.
Reference	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Tkachenko and Zenkevich, 1993	Tkachenko and Zenkevich, 1993, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-1	DB-1	DB-1	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Hydrogen	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25		0.32
Phase thickness (μm)	0.25	1.0	1.0
T_start (C)	60.	40.	40.	80.	50.
T_end (C)	250.	250.	250.	220.	230.
Heat rate (K/min)	2.	3.	3.	4.	4.
Initial hold (min)	5.
Final hold (min)	2.	30.	30.		10.
I	1473.	1485.	1490.	1473.	1473.
Reference	Kollmannsberger, Nitz, et al., 1992	Peppard, 1992	Peppard, 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Binder, Benson, et al., 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	RSL-150	OV-101	OV-101
Column length (m)		60.	30.	50.	50.
Carrier gas				N2	N2
Substrate
Column diameter (mm)		0.32	0.32	0.25	0.25
Phase thickness (μm)			0.20
T_start (C)	50.	50.	30.	80.	80.
T_end (C)	230.	230.	200.	200.	200.
Heat rate (K/min)	4.	4.	3.	2.	2.
Initial hold (min)
Final hold (min)	10.	10.
I	1473.	1473.	1472.	1487.	1487.
Reference	Binder, Turner, et al., 1990	Binder, Turner, et al., 1990, 2	Ronse and De Pooter, 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-1	SE-30	OV-3	OV-101
Column length (m)	60.	50.	30.	150.	50.
Carrier gas		He		He
Substrate
Column diameter (mm)	0.32	0.20		0.66	0.30
Phase thickness (μm)		0.20
T_start (C)	50.	30.	50.	30.	40.
T_end (C)	250.	220.	240.	170.	230.
Heat rate (K/min)	4.	2.	4.	1.	3.5
Initial hold (min)	0.1		2.		5.
Final hold (min)	5.		10.
I	1472.	1472.	1468.	1495.	1475.
Reference	Binder and Flath, 1989	de Pooter, Nicolai, et al., 1988	Ramaswami, Briscese, et al., 1988	Buttery, Flath, et al., 1986	Nykanen, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-1	OV-1	OV-101
Column length (m)	50.	50.	40.		30.
Carrier gas			He	He	He
Substrate
Column diameter (mm)	0.30	0.30	0.5		0.5
Phase thickness (μm)			0.75		0.8
T_start (C)	40.	40.	30.	40.	40.
T_end (C)	230.	230.	220.	220.	220.
Heat rate (K/min)	3.5	3.5	3.	2.	2.
Initial hold (min)	5.	5.
Final hold (min)
I	1492.	1496.	1470.	1473.	1471.
Reference	Nykanen, 1986	Nykanen, 1986	de Pooter, de Buyck, et al., 1986	De Pooter, De Buyck, et al., 1986	De Pooter and Schamp, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	SE-30
Column length (m)	30.	30.	30.
Carrier gas	He	He
Substrate
Column diameter (mm)	0.5	0.5
Phase thickness (μm)	0.8	0.8
T_start (C)	40.	40.	50.
T_end (C)	220.	220.	240.
Heat rate (K/min)	2.	2.	4.
Initial hold (min)			2.
Final hold (min)			10.
I	1471.	1472.	1468.
Reference	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	Ramaswami, Briscese, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Priestap, H.A.; van Baren, C.M.; Lira, P.D.L.; Prado, H.J.; Neugebauer, M.; Mayer, R.; Bandoni, A.L., Essential oils from aerial parts of Aristolochia gibertii Hook., Flavour Fragr. J., 2002, 17, 1, 69-71, https://doi.org/10.1002/ffj.1044 . [all data]

Schwob, Bessière, et al., 2002
Schwob, I.; Bessière, J.-M.; Viano, J., Composition of the essential oils of Hypericum perforatum L. from southeastern France, C.R. Acad. Sci. Ser. 3:, 2002, 325, 781-785. [all data]

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Sefidkon, F.; Dabiri, M.; Alamshahi, A., Analysis of the essential oil of Nepeta fissa C.A. Mey from Iran, Flavour Fragr. J., 2002, 17, 2, 89-90, https://doi.org/10.1002/ffj.1045 . [all data]

Sefidkon, 2002
Sefidkon, F., Essential oil of Lantana camara L. occurring in Iran, Flavour Fragr. J., 2002, 17, 1, 78-80, https://doi.org/10.1002/ffj.1048 . [all data]

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Velickovic, D.T.; Randjelovic, N.V.; Ristic, M.S.; Smelcerovic, A.A.; Velickovic, A.S., Chemical composition and antimicrobial action of the ethanol extracts of Salvia pratensis L., Salvia glutinosa L. and Salvia aethiopis L., J. Serb. Chem. Soc., 2002, 67, 10, 639-646, https://doi.org/10.2298/JSC0210639V . [all data]

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Yamini, Y.; Sefidkon, F.; Pourmortazavi, S.M., Comparison of essential oil composition of Iranian fennel (Foeniculum vulgare) obtained by supercritical carbon dioxide extraction and hydrodistillation methods, Flavour Fragr. J., 2002, 17, 5, 345-348, https://doi.org/10.1002/ffj.1117 . [all data]

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Cornu, A.; Carnat, A.-P.; Martin, B.; Coulon, J.-B.; Lamaison, J.-L.; Berdagué, J.-L., Solid-phase microextraction of volatile components from natural grassland plants, J. Agric. Food Chem., 2001, 49, 1, 203-209, https://doi.org/10.1021/jf0008341 . [all data]

Dabiri and Sefidkon, 2001
Dabiri, M.; Sefidkon, F., Analysis of the essential oil from aerial parts of Perovskia atriplicifolia Benth. at different stages of plant growth, Flavour Fragr. J., 2001, 16, 6, 435-438, https://doi.org/10.1002/ffj.988 . [all data]

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Gupta, Mallavarapu, et al., 2001
Gupta, R.; Mallavarapu, G.R.; Banerjee, S.; Kumar, S., Characteristics of an isomenthone-rich somaclonal mutant isolated in a geraniol-rich rose-scented geranium accession of Pelargonium graveolens, Flavour Fragr. J., 2001, 16, 5, 319-324, https://doi.org/10.1002/ffj.1002 . [all data]

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Jacquemond-Collet, I.; Bessière, J.-M.; Hannedouche, S.; Bertrand, C.; Fourasté, I.; Moulis, C., Identification of the alkaloids of Galipea officinalis by gas chromatography-mass spectrometry, Phytochem. Anal., 2001, 12, 5, 312-319, https://doi.org/10.1002/pca.594 . [all data]

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Kalemba, D.; Marschall, H.; Bradesi, P., Constituents of the essential oil of Solidago gigantea Ait. (giant goldenrod), Flavour Fragr. J., 2001, 16, 1, 19-26, https://doi.org/10.1002/1099-1026(200101/02)16:1<19::AID-FFJ940>3.0.CO;2-U . [all data]

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Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

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Mirza, M.; Ahmadi, L.; Tayebi, M., Volatile constituents of Hymenocrater incanus Bunge, an Iranian endemic species, Flavour Fragr. J., 2001, 16, 4, 239-240, https://doi.org/10.1002/ffj.983 . [all data]

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Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

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Santos-Gomes, P.C.; Fernandes-Ferreira, M., Organ- and season-dependent variation in the essential oil composition of Salvia officinalis L. cultivated at two different sites, J. Agric. Food Chem., 2001, 49, 6, 2908-2916, https://doi.org/10.1021/jf001102b . [all data]

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Shang, C.; Hu, Y.; Deng, C.; Hu, K., Rapid determination of volatile constituents of Michelia alba flowers by gas chromatography - mass spectrometry with solid-phase microextraction, J. Chromatogr. A, 2001, 942, 1-2, 283-288, https://doi.org/10.1016/S0021-9673(01)01382-6 . [all data]

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Feger, W.; Brandauer, H.; Ziegler, H., Sesquiterpene hydrocarbons of cold-pressed lime oils, Flavour Fragr. J., 2000, 15, 4, 281-284, https://doi.org/10.1002/1099-1026(200007/08)15:4<281::AID-FFJ916>3.0.CO;2-W . [all data]

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Jirovetz, L.; Puschmann, C.; Stojanova, A.; Metodiev, S.; Buchbauer, G., Analysis of the essential oil volatiles of Douglas fir (Pseudotsuga menziesii) from Bulgaria, Flavour Fragr. J., 2000, 15, 6, 434-437, https://doi.org/10.1002/1099-1026(200011/12)15:6<434::AID-FFJ935>3.0.CO;2-0 . [all data]

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Mitiku, S.B.; Sawamura, M.; Itoh, T.; Ukeda, H., Volatile components of peel cold-pressed oils of two cultivars of sweet orange (Citrus sinensis (L.) Osbeck) from Ethiopia, Flavour Fragr. J., 2000, 15, 4, 240-244, https://doi.org/10.1002/1099-1026(200007/08)15:4<240::AID-FFJ902>3.0.CO;2-F . [all data]

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Mohagheghzadeh, A.; Shams-Ardakani, M.; Ghannadi, A., Linalol-rich essential oil of Zataria multiflora Boiss. (Lamiaceae), Flavour Fragr. J., 2000, 15, 2, 119-122, https://doi.org/10.1002/(SICI)1099-1026(200003/04)15:2<119::AID-FFJ878>3.0.CO;2-V . [all data]

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Tamura, H.; Boonbumrung, S.; Yoshizawa, T.; Varanyanond, W., Volatile components of the essential oil in the pulp of four yellow mangoes (Mangifera indica L.) in Thailand, Food Sci. Technol. Res., 2000, 6, 1, 68-73, https://doi.org/10.3136/fstr.6.68 . [all data]

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Kalemba, D., Constituents of the essential oil of Artemisia asiatica Nakai, Flavour Fragr. J., 1999, 14, 3, 173-176, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<173::AID-FFJ805>3.0.CO;2-Q . [all data]

Koulman, 1999
Koulman, A., Podophyllotoxin: a study of biosynthesis, evolution, function, and use of podophyllotoxin and related lignans, University Library Groningen, Nederlands, 1999, 188, retrieved from http://www.ub.rug.nl/eldoc/dis/science/a.koulman/. [all data]

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Rycroft, D.S.; Cole, W.J.; Aslam, N.; Lamont, Y.M.; Gabriel, R., Killarniensolide, methyl orsellinates and 9,10-dihydrophenanthrenes from the liverwort Plagiochila killarniensis from Scotland and the Azores, Phytochemistry, 1999, 50, 7, 1167-1173, https://doi.org/10.1016/S0031-9422(98)00664-5 . [all data]

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Sefidkon, F.; Dabiri, M.; Rahimi-Bidgoly, A., The effect of distillation methods and stage of plant growth on the essential oil content and composition of Thymus kotschyanus Boiss. Hohen, Flavour Fragr. J., 1999, 14, 6, 405-408, https://doi.org/10.1002/(SICI)1099-1026(199911/12)14:6<405::AID-FFJ853>3.0.CO;2-M . [all data]

Sefidkon and Mirza, 1999
Sefidkon, F.; Mirza, M., Chemical composition of the essential oils of two Salvia species from Iran, Salvia virgata Jacq. and Salvia syriaca L., Flavour Fragr. J., 1999, 14, 1, 45-46, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<45::AID-FFJ774>3.0.CO;2-S . [all data]

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Tellez, M.R.; Canel, C.; Rimando, A.M.; Duke, S.O., Differential accumulation of isoprenoids in glanded and glandless Artemisia annua L, Phytochemistry, 1999, 52, 6, 1035-1040, https://doi.org/10.1016/S0031-9422(99)00308-8 . [all data]

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Camciuc, M.; Bessière, J.M.; Vilarem, G.; Gaset, A., Volatile components in okra seed coat, Phytochemistry, 1998, 48, 2, 311-315, https://doi.org/10.1016/S0031-9422(97)01127-8 . [all data]

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Ayedoun, Adeoti, et al., 1996
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Binder and Flath, 1989
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de Pooter, de Buyck, et al., 1986
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De Pooter, De Buyck, et al., 1986
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De Pooter and Schamp, 1986
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Ramaswami, Briscese, et al., 1986
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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