Pyridine, 2-(1-methyl-2-pyrrolidinyl)-


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxane5 % Phenyl methyl siloxaneDB-5MSSF-96BP-1
Column length (m) 25.25.30.40.12.
Carrier gas     He
Substrate      
Column diameter (mm) 0.200.20 0.280.22
Phase thickness (μm) 0.330.33  0.25
Program 50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min)50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min)not specified75C => 3C/min => 190C(25min) => 3C/min => 210C120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)
I 1362.1375.1346.1337.1331.
ReferenceGrigoriev and Savchuk, 2010Grigoriev and Savchuk, 2010Polzin, Stanfill, et al., 2007Kawasaki, Matsui, et al., 1998Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryOtherCapillary
Active phase BP-1Methyl SiliconeApieson L / KOH
Column length (m) 12.  
Carrier gas He  
Substrate    
Column diameter (mm) 0.22  
Phase thickness (μm) 0.25  
Program not specifiednot specifiednot specified
I 1340.1348.1346.
ReferenceStowell and Wilson, 1985Ardrey and Moffat, 1981Caddy, Fish, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Grigoriev and Savchuk, 2010
Grigoriev, A.M.; Savchuk, S.A., Correlation of the parameters of screening libraries of the gas-chromatographic retention data, Rus. J. Anal. Chem. (Engl. Transl.), 2010, 65, 4, 388-397. [all data]

Polzin, Stanfill, et al., 2007
Polzin, G.M.; Stanfill, S.B.; Brown, C.R.; Ashley, D.L.; Watson, C.H., Determination of eugenol, anethole, and coumarin in the mainstream cigarette smoke of Indonesian clove cigarettes, Food Chem. Toxicol., 2007, 45, 10, 1948-1953, https://doi.org/10.1016/j.fct.2007.04.012 . [all data]

Kawasaki, Matsui, et al., 1998
Kawasaki, W.; Matsui, K.; Akakabe, Y.; Itai, N.; Kajiwara, T., Long-chain aldehyde-forming activity in tobacco leaves, Phytochemistry, 1998, 49, 6, 1565-1568, https://doi.org/10.1016/S0031-9422(98)00236-2 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]

Caddy, Fish, et al., 1973
Caddy, B.; Fish, F.; Scott, D., Chromatographic screening for drugs of abuse using capillary columds. II. Peak identification on support coated open tubular columns for a series of central nervous system stimulating drugs, Chromatographia, 1973, 6, 7, 293-300, https://doi.org/10.1007/BF02269329 . [all data]


Notes

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