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2H-Pyran-3-ol, tetrahydro-2,2,6-trimethyl-6-(4-methyl-3-cyclohexen-1-yl)-, [3S-[3«alpha»,6«alpha»(R*)]]-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1758.8Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1672.Jian-Yu, Zhu, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 3. min
CapillaryDB-51744.Apel, Sobral, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-51746.Masotti, Juteau, et al., 200350. m/0.2 mm/0.25 «mu»m, He, 50. C @ 2. min, 3. K/min; Tend: 220. C
CapillaryNB-301734.Raal, Arak, et al., 200350. m/0.2 mm/0.5 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryOV-1011730.Orav, Kailas, et al., 200150. m/0.2 mm/0.5 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryOV-11698.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11702.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11702.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11702.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryOptima-5MS1735.HEuskin, Godin, et al., 200930. m/0.32 mm/0.25 «mu»m, Helium; Program: 40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySW-102400.Raal, Arak, et al., 200350. m/0.20 mm/0.25 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryPEG-20M2400.Orav, Kailas, et al., 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 70. C; Tend: 250. C
CapillaryCW 20M2359.Bicchi, Binello, et al., 199925. m/0.32 mm/0.25 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 220. C @ 10. min
CapillaryCW 20M2388.Bicchi, Binello, et al., 199925. m/0.32 mm/0.25 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 220. C @ 10. min

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Jian-Yu, Zhu, et al., 2012
Jian-Yu, S.; Zhu, L.; Tian, Y.-J., Chemical composition and antimicrobial activities of essential oil of Matricaria songarica, Int. J. Agriculture Biology, 2012, 14, 1, 107-110. [all data]

Apel, Sobral, et al., 2006
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of four Plinia species (Myrtaceae), Flavour Fragr. J., 2006, 21, 3, 565-567, https://doi.org/10.1002/ffj.1638 . [all data]

Masotti, Juteau, et al., 2003
Masotti, V.; Juteau, F.; Bessière, J.M.; Viano, J., Seasonal and phenological variations of the essential oil from the narrow endemic species Artemisia molinieri and its biological activities, J. Agric. Food Chem., 2003, 51, 24, 7115-7121, https://doi.org/10.1021/jf034621y . [all data]

Raal, Arak, et al., 2003
Raal, A.; Arak, E.; Orav, A.; Ivask, K., Comparison of essential oil content of Matricaria recutita L. from different origins, Ars Pharm., 2003, 44, 2, 159-165, retrieved from http://www.ugr.es/~ars/abstract/44-159-03.pdf. [all data]

Orav, Kailas, et al., 2001
Orav, A.; Kailas, T.; Ivask, K., Volatile constituents of Matricaria recutita L. from Estonia, Proc. Est. Acad. Sci. Chem., 2001, 50, 39-45. [all data]

Bicchi, Binello, et al., 1999
Bicchi, C.; Binello, A.; D'Amato, A.; Rubiolo, P., Reliability of Van den Dool retention indices in the analysis of essential oils, J. Chromatogr. Sci., 1999, 37, 8, 288-294, https://doi.org/10.1093/chromsci/37.8.288 . [all data]

HEuskin, Godin, et al., 2009
HEuskin, S.; Godin, B.; Leroy, P.; Quentin C.; Wathelet, J.-P.; Verheggen, F.; Haubruge, E.; Lognay, G., Fast gas chromatography characterization of purified semiochemicals from essential oils of Matricaria chamomilla L. (Asteraceae) and Nepeta cataria L. (Lamiaceae), J. Chromatorg. A., 2009, 1216, 14, 2768-2775, https://doi.org/10.1016/j.chroma.2008.09.109 . [all data]


Notes

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