1H-Cycloprop[e]azulene, 1a,2,3,5,6,7,7a,7b-octahydro-1,1,4,7-tetramethyl-, [1aR-(1aα,7α,7aβ,7bα)]-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5HP-5HP-5HP-5
Column length (m) 30.30.25.25.25.
Carrier gas HeliumHeliumHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.520.520.52
Tstart (C) 60.100.40.40.40.
Tend (C) 240.260.280.280.280.
Heat rate (K/min) 3.10.4.4.4.
Initial hold (min)  1.   
Final hold (min)  10.10.10.10.
I 1499.1500.1489.1489.1489.
ReferenceAlizadeh and Shaabani, 2012Boukhris, Bouaziz, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSHP-5 MSCP-Sil 5 CBRTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.30.50.60.
Tend (C) 210.180.250.200.230.
Heat rate (K/min) 5.2.5.5.2.
Initial hold (min)   3.  
Final hold (min)   10. 30.
I 1493.1485.1534.1502.1491.
ReferenceFathi, Sahari, et al., 2011Hammami, Kamoun, et al., 2011Zarai, Kadri, et al., 2011Hnawia, Menut, et al., 2009Museli, Pau, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5 MSHP-5 MSHP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumNitrogenHelium Helium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.40.50.60.70.
Tend (C) 230.230.220.280.210.
Heat rate (K/min) 2.2.3.3.5.
Initial hold (min)   2. 1.
Final hold (min) 30. 70. 5.
I 1492.1497.1488.1494.1504.
ReferenceMuseli, Pau, et al., 2009Scrivanti, Anton, et al., 2009Shimizu, Imayoshi, et al., 2009Baziou, Couladis, et al., 2008Bouwmeester, de Kraker, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-5 MSDB-5DB-5SPB-1
Column length (m) 7.530.30.30.30.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.100.320.250.250.2
Phase thickness (μm) 10.0.250.250.320.2
Tstart (C) 60.60.60.50.70.
Tend (C) 240.280.300.250.220.
Heat rate (K/min) 3.4.3.5.3.
Initial hold (min)  5.   
Final hold (min)     15.
I 1496.1498.1466.1482.1483.
ReferenceShellie, 2008Capetanos, Saroglou, et al., 2007Moreno, Lima, et al., 2007Nori-Shargh, Raftari, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5AT-5HP-5MSHP-5
Column length (m) 30.30.60.30.30.
Carrier gas Helium HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 280.300.200.250.300.
Heat rate (K/min) 3.3.4.2.5.
Initial hold (min)     5.
Final hold (min)   20. 5.
I 1494.1483.1491.1493.1491.
ReferenceTsokou, Georgopoulos, et al., 2007Apel, Sobral, et al., 2006Borges, Rojas, et al., 2006Farah, Afifi, et al., 2006Figuérédo, Cabassu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-5DB-5DB-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeHydrogenN2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.60.60.70.60.
Tend (C) 250.240.240.280.240.
Heat rate (K/min) 2.5.5.4.4.
Initial hold (min)  2.2.4. 
Final hold (min) 40.    
I 1488.1492.1492.1493.1493.
ReferenceFilippi, Lanfranchi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Pino, Marbot, et al., 2006Trilles, Bombarda, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 8 CBDB-5HP-5DB-1
Column length (m) 25.30.30.30.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 40.80.60.50.50.
Tend (C) 220.200.300.300.250.
Heat rate (K/min) 3.3.3.5.4.
Initial hold (min) 5.5.3.5.5.
Final hold (min)  5. 5. 
I 1502.1487.1486.1491.1492.
ReferenceChagonda and Chalchat, 2005Facey, Porter, et al., 2005Ferraz, Limberger, et al., 2005Figuérédo, Cabassu, et al., 2005Khajeh, Yamini, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5DB-5DB-5
Column length (m) 25.50.30.30.30.
Carrier gas  N2HeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 50.95.40.60.50.
Tend (C) 230.240.260.280.290.
Heat rate (K/min) 3.4.2.3.4.
Initial hold (min)   5.  
Final hold (min)   20.  
I 1494.1487.1493.1458.1487.
ReferenceOgunwande, Olawore, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Senatore, Apostolides Arnold, et al., 2005Tzakou and Constantinidis, 2005Abreu, Reis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 8 CBHP-1HP-5
Column length (m) 30.30.30.50.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.320.20.25
Phase thickness (μm) 0.250.250.250.50.25
Tstart (C) 60.50.50.60.60.
Tend (C) 300.250.200.220.280.
Heat rate (K/min) 3.3.5.2.4.
Initial hold (min)  5.5.  
Final hold (min)    45. 
I 1478.1493.1502.1493.1473.
ReferenceLimberger, Sobral, et al., 2004Sefidkon, Jamzad, et al., 2004Wang, Guo, et al., 2004Fernandez, Lizzani-Cuvelier, et al., 2003Ghassemi, Sajjadi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200HP-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas H2H2He He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.40.60.
Tend (C) 280.280.280.260.280.
Heat rate (K/min) 6.6.3.2.3.
Initial hold (min) 5.5. 5. 
Final hold (min) 5.5.  30.
I 1489.1481.1471.1492.1487.
ReferenceJirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Pitarokili, Tzakou, et al., 2003Senatore and Bruno, 2003Caredda, Marongiu, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSHP-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.100.60.
Tend (C) 280.280.250.240.240.
Heat rate (K/min) 3.3.4.5.3.
Initial hold (min)   5.2. 
Final hold (min)    5. 
I 1495.1495.1493.1481.1493.
ReferenceCongiu, Falconieri, et al., 2002Congiu, Falconieri, et al., 2002Farah, Fechtal. M., et al., 2002Lago, Reis, et al., 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5RSL-200RTX-1DB-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeN2H2N2He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.60.40.60.60.
Tend (C) 250.220.280.300.240.
Heat rate (K/min) 4.5.6.4.3.
Initial hold (min)  10.5.  
Final hold (min)   5. 30.
I 1474.1499.1490.1493.1470.
ReferenceSefidkon, Dabiri, et al., 2002Flamini, Cioni, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Marongiu, Porcedda, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5CP Sil 5 CBDB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.275.230.240.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)      
Final hold (min)      
I 1489.1489.1490.1482.1492.
ReferenceTellez M., Estell R., et al., 2001Maia, Zoghbi, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Oyedeji, Olawore, et al., 1999El-Sakhawy, El-Tantawy, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-1BP-1SE-30
Column length (m) 30.30.50.50.30.
Carrier gas HeHeliumN2H2 
Substrate      
Column diameter (mm) 0.250.250.270.30 
Phase thickness (μm) 0.250.250.2  
Tstart (C) 60.60.80.40.50.
Tend (C) 240.240.240.250.240.
Heat rate (K/min) 3.3.3.10.4.
Initial hold (min)    1.2.
Final hold (min)     10.
I 1492.1493.1494.1497.1484.
ReferenceMaia, Zohhbi, et al., 1998Tellez, Estell, et al., 1997Ramanoelina, Viano, et al., 1994Brophy, Davies, et al., 1989Ramaswami, Briscese, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30
Column length (m) 30.
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 50.
Tend (C) 240.
Heat rate (K/min) 4.
Initial hold (min) 2.
Final hold (min) 10.
I 1484.
ReferenceRamaswami, Briscese, et al., 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Alizadeh and Shaabani, 2012
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Ferraz, Limberger, et al., 2005
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Figuérédo, Cabassu, et al., 2005
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Khajeh, Yamini, et al., 2005
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Pala-Paul, Perez-Alonso, et al., 2005
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Notes

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