Benzo[b]chrysene

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Lee's RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxane5 % Phenyl methyl siloxaneHP-5HP-5DB-5
Column length (m)   60.30.30.
Carrier gas   He  
Substrate      
Column diameter (mm)   0.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 50.80.35.50.40.
Tend (C) 250.300.300.280.280.
Heat rate (K/min) 2.8.3.4.4.
Initial hold (min)  2. 2.2.
Final hold (min)  10. 20.5.
I 497.66498.50498.84496.78498.84
ReferenceSkrbic and Onjia, 2006Skrbic and Onjia, 2006Marynowski, Pieta, et al., 2004Piao, Chu, et al., 1999Wise, Benner, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SE-52SE-52
Column length (m) 20.12.
Carrier gas H2He
Substrate   
Column diameter (mm) 0.300.3
Phase thickness (μm) 0.250.34
Tstart (C) 40.50.
Tend (C) 265.250.
Heat rate (K/min) 4.2.
Initial hold (min) 2. 
Final hold (min)   
I 498.90497.66
ReferenceVassilaros, Kong, et al., 1982Lee, Vassilaros, et al., 1979
Comment MSDC-RI MSDC-RI

References

Go To: Top, Lee's RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Skrbic and Onjia, 2006
Skrbic, B.; Onjia, A., Prediction of Lee Retention Indices of Polycyclic Aromatic Hydrocarbons by Artificial Neural Networks, J. Chromatorg. A, 2006, 1108, 2, 279-284, https://doi.org/10.1016/j.chroma.2006.01.080 . [all data]

Marynowski, Pieta, et al., 2004
Marynowski, L.; Pieta, M.; Janeczek, J., Composition and source of polycyclic aromatic compounds in deposited dust from selected sites around the Upper Silesia, Poland, Geol. Q., 2004, 48, 2, 169-180. [all data]

Piao, Chu, et al., 1999
Piao, M.; Chu, S.; Zheng, M.; Xu, X., Characterization of the combustion products of polyethylene, Chemosphere, 1999, 39, 9, 1497-1512, https://doi.org/10.1016/S0045-6535(99)00054-5 . [all data]

Wise, Benner, et al., 1988
Wise, S.A.; Benner, B.A.; Byrd, G.D.; Chesler, S.N.; Rebbert, R.E.; Schantz, M.M., Determination of polycyclic aromatic hydrocarbons in a coal tar standard reference material, Anal. Chem., 1988, 60, 9, 887-894, https://doi.org/10.1021/ac00160a012 . [all data]

Vassilaros, Kong, et al., 1982
Vassilaros, D.L.; Kong, R.C.; Later, D.W.; Lee, M.L., Linear retention index system for polycyclic aromatic compounds. Critical evaluation and additional indices, J. Chromatogr., 1982, 252, 1-20, https://doi.org/10.1016/S0021-9673(01)88394-1 . [all data]

Lee, Vassilaros, et al., 1979
Lee, M.L.; Vassilaros, D.L.; White, C.M.; Novotny, M., Retention Indices for Programmed-Temperature Capillary-Column Gas Chromatography of Polycyclic Aromatic Hydrocarbons, Anal. Chem., 1979, 51, 6, 768-773, https://doi.org/10.1021/ac50042a043 . [all data]


Notes

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