Cubenol


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRTX-1HP-5 MSDB-5DB-5
Column length (m) 60.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.50.
Tend (C) 250.230.220.240.250.
Heat rate (K/min) 3.2.4.3.2.
Initial hold (min) 1. 20.  
Final hold (min) 20.5.20.  
I 1607.1630.1636.1642.1647.
ReferenceSardashti, Valizadeh, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Feizbakhsh and Naeemy, 2011Karimi, Farmani, et al., 2011Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSDB-5OV-101DB-5
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.70.40.70.40.
Tend (C) 240.290.240.220.230.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min) 2. 1.  
Final hold (min)  10.   
I 1645.1650.1592.1640.1648.
ReferenceKahriman, Tosun, et al., 2010Radulovic, Blagojevic, et al., 2010de Souza, Lopes, et al., 2010Benites, Moiteiro, et al., 2009Scrivanti, Anton, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5DB-5 MSRTX-1
Column length (m) 30.30.30.30.60.
Carrier gas Helium HeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.320.250.22
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.60.100.50.60.
Tend (C) 240.280.240.300.230.
Heat rate (K/min) 3.3.5.5.2.
Initial hold (min) 1. 2.5. 
Final hold (min)   5.5.35.
I 1592.1641.1642.1638.1631.
Referencede Souza, Lopes, et al., 2009Baziou, Couladis, et al., 2008Lago, Romoff, et al., 2008Noudogbessi, Yedomonhan, et al., 2008Paolini, Tomi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5 MSDB-5HP-1ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.35.60.60.
Tend (C) 270.230.220.240.220.
Heat rate (K/min) 3.3.3.2.4.
Initial hold (min)  10.  5.
Final hold (min)  10.40.20.20.
I 1604.1642.1644.1623.1642.
ReferenceVictorio, Alviano, et al., 2008Adams, Beauchamp, et al., 2007El-Ghorab A., El-Massry K.F., et al., 2007Hachicha, Skanji, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5 MSBP-1HP-5
Column length (m) 30.30.60.50.30.
Carrier gas HeliumHeliumHydrogen Helium
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 300.220.260.220.240.
Heat rate (K/min) 3.4.4.2.4.
Initial hold (min)      
Final hold (min)   20.20.5.
I 1612.1649.1654.1633.1633.
ReferenceMoreno, Lima, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Rojas, Velasco, et al., 2007Boti, Yao, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5DB-1HP-5DB-5
Column length (m) 30.25.50.30.30.
Carrier gas HeN2N2HeHydrogen
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.250.150.250.250.25
Tstart (C) 50.50.95.60.70.
Tend (C) 250.200.240.220.280.
Heat rate (K/min) 2.4.4.5.4.
Initial hold (min)  3. 10.4.
Final hold (min)      
I 1610.1640.1643.1645.1642.
ReferenceOrav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5Methyl SiliconeHP-5
Column length (m) 30.25.30.25.25.
Carrier gas H2H2HeN2H2
Substrate      
Column diameter (mm) 0.250.320.250.30.32
Phase thickness (μm) 0.250.250.250.150.52
Tstart (C) 50.60.60.50.50.
Tend (C) 280.240.260.210.280.
Heat rate (K/min) 4.3.5.2.2.5
Initial hold (min) 2.  5.5.
Final hold (min) 10.    
I 1642.1646.1664.1647.1630.
ReferencePino, Sauri-Duch, et al., 2006Potzernheim, Bizzo, et al., 2006Sabulal, Dan, et al., 2006Tonzibo, Coffy, et al., 2006Wang, Kong, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 8 CBHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.80.50.70.
Tend (C) 240.240.200.250.240.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)   5.10. 
Final hold (min)   5.5. 
I 1642.1645.1615.1650.1643.
ReferenceChaverri and Cicció, 2005Chaverri and Cicció, 2005Facey, Porter, et al., 2005Melkani, Dev, et al., 2005Oyedeji, Yani, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1CP Sil 8 CBDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeH2
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 300.220.290.280.290.
Heat rate (K/min) 3.5.3.3.4.
Initial hold (min)   5.  
Final hold (min)  15.   
I 1637.1606.1672.1617.1641.
ReferenceSimoes-Pires C.A., Debenedetti S., et al., 2005Srivastava, Srivastava, et al., 2005Suárez, Vásquez, et al., 2005Tzakou and Constantinidis, 2005Abreu, Reis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5MSDB-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.60.
Tend (C) 200.230.240.300.280.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)      
Final hold (min)     30.
I 1637.1632.1644.1633.1601.
ReferenceAgnaniet, Menut, et al., 2004González, Guerra, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004Marongiu, Porcedda, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Methyl SiliconeHP-5 MSCP Sil 5 CBDB-1
Column length (m) 50.60.30.20.30.
Carrier gas N2HeHeliumHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 95.60.60.100.50.
Tend (C) 240.200.200.270.200.
Heat rate (K/min) 4.4.4.8.5.
Initial hold (min)  1.1.2. 
Final hold (min)  20.20.  
I 1617.1643.1643.1620.1595.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2004Rojas, Usubillaga, et al., 2004Royas, Usubillaga, et al., 2004Thappa, Bakshi, et al., 2004Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSMethyl SiliconeRSL-200DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 280.250.280.250.280.
Heat rate (K/min) 4.2.6.3.3.
Initial hold (min)  2.5.  
Final hold (min)  5.5. 30.
I 1642.1610.1602.1639.1628.
ReferenceGhasemi, Asghari, et al., 2003Jayaprakasha, Rao, et al., 2003Jirovetz, Buchbauer, et al., 2003Limberger, Simões-Pires, et al., 2003Marongiu, Porcedda, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5DB-5HP-5
Column length (m) 30.50.30.30.60.
Carrier gas HeN2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.95.60.60.40.
Tend (C) 280.240.280.240.250.
Heat rate (K/min) 3.4.3.3.5.
Initial hold (min)     15.
Final hold (min) 30.    
I 1630.1633.1625.1646.1627.
ReferenceMarongiu, Porcedda, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pitarokili, Tzakou, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-15 % Phenyl methyl siloxaneRSL-200
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.75.40.
Tend (C) 240.240.280.200.280.
Heat rate (K/min) 3.3.4.3.6.
Initial hold (min)    4.5.
Final hold (min)    8.5.
I 1643.1643.1617.1647.1645.
ReferenceTaveira, de Lima, et al., 2003Zoghbi, Andrade, et al., 2003Ahmadi, Mirza, et al., 2002Cicció and Gómez-Laurito, 2002Jirovetz, Buchbauer, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.35.60.60.
Tend (C) 210.240.280.250.240.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 2. 2.  
Final hold (min) 33. 15.  
I 1644.1641.1638.1636.1645.
ReferenceKabouss, Charrouf, et al., 2002Kobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Limberger, Simões-Pires, et al., 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1DB-1DB-1DB-1
Column length (m) 30.60.60.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.40.40.80.60.
Tend (C) 240.280.280.225.240.
Heat rate (K/min) 3.4.4.4.3.
Initial hold (min)  5.5.  
Final hold (min)      
I 1642.1602.1620.1608.1645.0
ReferenceMaia, Zoghbi, et al., 2002Dabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Santos, Moreira, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-101OV-101DB-1
Column length (m) 60.30.25.50.50.
Carrier gas N2HeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.25  0.25
Tstart (C) 60.60.50.80.70.
Tend (C) 220.240.200.200.240.
Heat rate (K/min) 3.3.5.1.4.
Initial hold (min) 5.    
Final hold (min) 22.  20. 
I 1637.1641.1638.1639.1609.
ReferenceBailac, Dellacasa, et al., 2000Tellez, Dayan, et al., 2000Ayedoun, Adéoti, et al., 1999Menon, Chacko, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5MSDB-1DB-5
Column length (m) 60.30.30. 30.
Carrier gas HeHeHe Helium
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 40.60.60.80.60.
Tend (C) 280.240.240.220.240.
Heat rate (K/min) 4.3.3.6.3.
Initial hold (min) 5.    
Final hold (min)      
I 1610.1641.1640.1600.1642.
ReferenceSefidkon, Dabiri, et al., 1999Tellez, Canel, et al., 1999Zoghbi, Andrade, et al., 1999Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-5CBP-1OV-101
Column length (m) 30.25.50.
Carrier gas HeHeN2
Substrate    
Column diameter (mm) 0.250.220.25
Phase thickness (μm)   0.17
Tstart (C) 60.60.50.
Tend (C) 240.240.220.
Heat rate (K/min) 4.5.5.
Initial hold (min)    
Final hold (min)    
I 1642.1632.1620.
ReferenceZunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Chacko, Jayalekshmy, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

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Feizbakhsh, A.; Naeemy, A., Volatile constituents of essential oils of Eleocharis pauciflora (Light) Link and Eleocharis uniglumis (Link) J.A. Schultes growing wild in Iran, Bull. Chem. Soc. Ethiop., 2011, 25, 3, 461-464, https://doi.org/10.4314/bcse.v25i3.68606 . [all data]

Karimi, Farmani, et al., 2011
Karimi, H.; Farmani, A.; Nourizadeh, H., A performance comparison of modern statistical technique for molecular descriptor selection and retention prediction of essential oil from leaves, Amer. J. Sci. Res., 2011, 38, 36-40. [all data]

Ho, Wang, et al., 2010
Ho, C.-L.; Wang, E.I.-C.; Yu, H.-T.; Yu, H.-M.; Su, Y.-C., Composition amd antioxidant activities of essential oils of different tissues from Cryptomeria japonica D. Don, Quarterly J. Chin. Forestry, 2010, 32, 1, 63-76. [all data]

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Kahriman, N.; Tosun, G.; Genc, H.; Yayli, N., Comparative essential oil analysis of Geranium sylvaticum estracted by hydrodistillation and microwave distillation, Turk. J. Chem., 2010, 34, 969-976. [all data]

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Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

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Benites, Moiteiro, et al., 2009
Benites, J.; Moiteiro, C.; Miguel, G.; Rojo, L.; Lopez, J.; Venancio, F.; Ramalho, L.; Feio, S.; Dandlen, S.; Casanova, H.; Torres, I., Composition and biological activity of the essential oil of Peruvial Lantana camara, J. Chilean Chem. Soc., 2009, 54, 4, 379-384, https://doi.org/10.4067/S0717-97072009000400012 . [all data]

Scrivanti, Anton, et al., 2009
Scrivanti, L.R.; Anton, A.M.; Zygadlo, J.A., Essential oil conposition of Bothriochloa Kuntze (Poaceae) from South America and their chemotaxonomy, Biochem. Systematics Ecol., 2009, 37, 3, 206-213, https://doi.org/10.1016/j.bse.2009.03.009 . [all data]

de Souza, Lopes, et al., 2009
de Souza, A.; Lopes, E.M.C.; da Silva, M.C.; Cordeiro, I.; Young, M.C.M.; Sobral, M.E.G.; Moreno, P.R.H., Chemical composition and acetylcholinesterase inhibitory activity of essential oils of Myrceugenia myrcioides (Chambess.) O. Berg and Eugenia riedeliana O. Berg, Myrtaceae, Braz. J. Pharmacognosy, 2009, 20, 2, 175-179. [all data]

Baziou, Couladis, et al., 2008
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Lago, Romoff, et al., 2008
Lago, J.H.G.; Romoff, P.; Favero, O.A.; Souza, F.O.; Soares, M.G.; Baraldi, P.T.; Correa, A.G., Chemical composition of male and female Baccharis trimera (Less.) DC. (Asteraceae) essential oils, Biochem. Systematics Ecol., 2008, 36, 9, 737-740, https://doi.org/10.1016/j.bse.2008.05.009 . [all data]

Noudogbessi, Yedomonhan, et al., 2008
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Paolini, Tomi, et al., 2008
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Victorio, Alviano, et al., 2008
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Adams, Beauchamp, et al., 2007
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El-Ghorab A., El-Massry K.F., et al., 2007
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Hachicha, Skanji, et al., 2007
Hachicha, S.F.; Skanji, T.; Barrek, S.; Ghrabi, Z.G.; Zarrouk, H., Composition of the essential oil of Teucrium ramosissimum Desf. (Lamiaceae) from Tunisia, Flavour Fragr. J., 2007, 22, 2, 101-104, https://doi.org/10.1002/ffj.1764 . [all data]

Mohottalage, Tabacchi, et al., 2007
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Moreno, Lima, et al., 2007
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Morteza-Semnani, Saeedi, et al., 2007
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Rojas, Velasco, et al., 2007
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Cicció and Gómez-Laurito, 2002
Cicció, J.F.; Gómez-Laurito, J., Volatile constituents of the leaves of Siparuna thecaphora (Siparunaceae) from Turrialba, Costa Rica, Rev. Biol. Trop., 2002, 50, 3/4, 963-967. [all data]

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Maia, Zoghbi, et al., 2002
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Dabiri and Sefidkon, 2001
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Salgueiro, Vila, et al., 1997
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Chacko, Jayalekshmy, et al., 1996
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Notes

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