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Gibbane-1,10-dicarboxylic acid, 4a-hydroxy-1-methyl-8-methylene-, 1,4a-lactone, 10-methyl ester, (1«alpha»,4a«alpha»,4b«beta»,10«beta»)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-52349.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillaryHP-52350.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillarySE-302343.Odén, Wang, et al., 199525. m/0.25 mm/0.25 «mu»m; Program: 80C(1min) => (20C/min) => 200C => (4C/min) => 250C
CapillaryDB-12322.Tanno, Yokota, et al., 1992Column length: 15. m; Column diameter: 0.258 mm; Program: 130C(2m) => 32C/min => 220(4min) => 8C/min270C(2min)
PackedNonpolar2337.Poling, 1991Program: not specified
PackedNonpolar2339.Poling, 1991Program: not specified
CapillaryUltra-22326.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22327.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-12305.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryHP-12305.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryDB-52362.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-52363.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-12352.Kang, Jun, et al., 1999He; Column length: 15. m; Column diameter: 0.25 mm; Program: 80C (1min) => 30C/min => 245 C => 5C/min => 300C
CapillaryBP-12321.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2319.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryCP Sil 5 CB2319.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryDB-12312.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12313.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12332.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillarySE-522298.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySE-522298.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-12309.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12310.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12310.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12310.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12305.Oyama, Yamauchi, et al., 1996, 2160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-12332.Nakayama, Koshioka, et al., 200130. m/0.25 mm/0.25 «mu»m, He; Program: 60C (2min) => 2C/min => 210C => 2C/min => 280C(5min)
CapillarySE-302334.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillarySE-302334.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12346.Kawaide, Sassa, et al., 1995He; Column length: 15. m; Column diameter: 0.25 mm; Program: 80C(1min) => 30C/min => 245C => 5C/min => 300C
CapillaryDB-12300.Koshioka, Nishijama, et al., 199515. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryUltra-22327.Talon, Zeevaart, et al., 199125. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 8C/min => 280C
CapillaryDB-12320.Nakayama, Yamane, et al., 1990Helium; Column length: 15. m; Column diameter: 0.258 mm; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Morvan-Bertrand, Ernstsen, et al., 2001
Morvan-Bertrand, A.; Ernstsen, A.; Lindgård, B.; Koshioka, M.; le Saos, J.; Boucaud, J.; Prud'homme, M.-P.; Junttila, O., Endogenous gibberellins in Lolium perenne and influence of defoliation on their contents in elongating leaf bases and in leaf sheaths, Physiol. Plant., 2001, 111, 2, 225-231, https://doi.org/10.1034/j.1399-3054.2001.1110214.x . [all data]

Odén, Wang, et al., 1995
Odén, P.C.; Wang, Q.; Högberg, K.-A.; Werner, M., Transport and metabolism of gibberellins in relation to flower bud differentiation in Norway spruce (Picea abies), Tree Physiol., 1995, 15, 7-8, 451-456, https://doi.org/10.1093/treephys/15.7-8.451 . [all data]

Tanno, Yokota, et al., 1992
Tanno, N.; Yokota, T.; Abe, M.; Okagami, N., Identification of endogenous gibberellins in dormant bulbils of Chinese yam, Dioscorea opposita, Plant Physiol., 1992, 100, 4, 1823-1826, https://doi.org/10.1104/pp.100.4.1823 . [all data]

Poling, 1991
Poling, S.M., Identification of endogenous gibberellins in immature navel orange fruit, J. Agric. Food Chem., 1991, 39, 4, 677-680, https://doi.org/10.1021/jf00004a010 . [all data]

Talon, Koornneef, et al., 1990
Talon, M.; Koornneef, M.; Zeevaart, J.A.D., Endogenous gibberellins in Arabidopsis thaliana and possible steps blocked in the biosynthetic pathways of the semidwarf ga4 and ga5 mutants, Proc. Nat. Acad. Sci. U.S.A., 1990, 87, 20, 7983-7987, https://doi.org/10.1073/pnas.87.20.7983 . [all data]

Kim, Lee, et al., 2003
Kim, S.-K.; Lee, S.-C.; Shin, D.-H.; Jang, S.-W.; Nam, J.-W.; Park, T.-S.; Lee, I.-J., Quantification of endogenous gibberellins in leaves and tubers of Chinese yam, Dioscorea opposita Thunb. cv. Tsukune during tuber enlargement, Plant Growth Regul., 2003, 39, 2, 125-130, https://doi.org/10.1023/A:1022569506883 . [all data]

Pearce, Hutt, et al., 2002
Pearce, D.W.; Hutt, O.E.; Rood, S.B.; Mander, L.N., Gibberellins in shoots and developing capsules of Populus species, Phytochemistry, 2002, 59, 6, 679-687, https://doi.org/10.1016/S0031-9422(02)00009-2 . [all data]

Kang, Jun, et al., 1999
Kang, H.-G.; Jun, S.-H.; Kim, J.; Kawaide, H.; Kamiya, Y.; An, G., Cloning and molecular analyses of a gibberellin 20-oxidase gene expressed specifically in developing seeds of watermelon, Plant Physiol., 1999, 121, 2, 373-382, https://doi.org/10.1104/pp.121.2.373 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Ridoutt, Pharis, et al., 1995
Ridoutt, B.G.; Pharis, R.P.; Sands, R., Identification and quantification of cambial region hormones of Eucalyptus globulus, Plant Cell Physiol., 1995, 36, 6, 1143-1147. [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Oyama, Yamauchi, et al., 1996
Oyama, N.; Yamauchi, T.; Yamane, H.; Yamaguchi, I.; Schraudolf, H.; Mander, L.N.; Murofushi, N., Gibberellins and antheridiogens in prothallia and sporophytes of Anemia phyllitidis, Biosci. Biotechnol. Biochem., 1996, 60, 2, 301-304, https://doi.org/10.1271/bbb.60.301 . [all data]

Oyama, Yamauchi, et al., 1996, 2
Oyama, N.; Yamauchi, T.; Yamane, H.; Murofushi, N.; Agatsuma, M.; Pour, M.; Mander, L.N., Identification of gibberellins and 9,15-cyclogibberellins in developing apple seeds, Biosci. Biotechnol. Biochem., 1996, 60, 2, 305-308, https://doi.org/10.1271/bbb.60.305 . [all data]

Nakayama, Koshioka, et al., 2001
Nakayama, M.; Koshioka, M.; Matsui, H.; Ohara, H.; Mander, L.N.; Leitch, S.K.; Twitchin, B.; Kraft-Klaunzer, P.; Pharis, R.P.; Yokota, T., Endogenous gibberellins in immature seeds of Prunus persica L.: identification of GA118, GA119, GA120, GA121, GA122 and GA126, Phytochemistry, 2001, 57, 5, 749-758, https://doi.org/10.1016/S0031-9422(01)00154-6 . [all data]

Wang, Little, et al., 1996
Wang, Q.; Little, C.H.A.; Moritz, T.; Odén, P.C., Identification of endogenous gibberellins, and metabolism of tritiated and deuterated GA4, GA9, and GA20, in Scots pine (Pinus sylvestris) shoots, Physiol. Plant., 1996, 97, 4, 764-771, https://doi.org/10.1111/j.1399-3054.1996.tb00542.x . [all data]

Kawaide, Sassa, et al., 1995
Kawaide, H.; Sassa, T.; Kamiya, Y., Plant-like biosynthesis of gibberellin A1 in the fungus Phaeosphaeria Sp. L487, Phytochemistry, 1995, 39, 2, 305-310, https://doi.org/10.1016/0031-9422(95)00006-S . [all data]

Koshioka, Nishijama, et al., 1995
Koshioka, M.; Nishijama, T.; Mander, L.N., Gibberellin metabolism in suspension cultured cells of Raphanus Sativus, Phytochemistry, 1995, 38, 2, 359-363, https://doi.org/10.1016/0031-9422(94)00624-3 . [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526, https://doi.org/10.1104/pp.97.4.1521 . [all data]

Nakayama, Yamane, et al., 1990
Nakayama, M.; Yamane, H.; Yokota, T.; Yamaguchi, I.; Murofushi, N.; Takahashi, N.; Nishijima, T.; Katsura, N.; Nonaka, M.; Gaskin, P.; MacMillan, J.; Mander, L.N.; Chu, A., Endogenous gibberellins in mature seed of Raphanus sativus L. cv. Taibyo-sobutori, Agric. Biol. Chem., 1990, 54, 3, 837-840, https://doi.org/10.1271/bbb1961.54.837 . [all data]


Notes

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