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Benzo[ghi]fluoranthene

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Lee's RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MS5 % Phenyl methyl siloxane
Column length (m) 30.30.30.30. 
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Program 60C(2min) => 6C/min => 258C => 2C/min => 300C(4min)not specifiednot specifiednot specified70 0C (2 min) 30 0C/min -> 150 0C 5 0C/min -> 200 0C 4 0C/min -> 310 0C (5 min)
I 390.18389.92390.18390.28389.60
ReferenceWang, Li, et al., 2007Wang, Li, et al., 2007, 2Wang, Li, et al., 2007, 2Wang, Li, et al., 2007, 2Skrbic and Onjia, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSLM-5Ultra-1Ultra-1Ultra-1
Column length (m) 60.30.50.50.50.
Carrier gas  HeNitrogenNitrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (mum)  0.250.500.500.50
Program not specified60C(2min) => 15C/min => 180C => 5C/min => 280C (10min)40-100 0C 3-15 0C/min -> 290 0C40-100 0C 3-15 0C/min -> 290 0C40-100 0C 3-15 0C/min -> 290 0C
I 388.2389.69389.6389.6390.9
ReferenceAracil, Font, et al., 2005Ré-Poppi and Santiago-Silva, 2005Sremac, Skrbic, et al., 2005Sremac, Skrbic, et al., 2005Sremac, Skrbic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5LM-5DB-5SE-54
Column length (m) 30.30.30.30. 
Carrier gas Helium HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Program 70 0C 7 0C/min -> 280 0C (2 min) 7 0C/min -> 300 0C (2 min)not specified60C(2min) => 15C/min => 180C => 5C/min => 280C(5min)90C (1min) => 10C/min => 120C => 4C/min => 310C (20min)not specified
I 391.1390.9389.67390.96388.58
ReferenceBrack and Schirmer, 2003Lundstedt, Haglund, et al., 2003Ré-Poppi and Santiago-Silva, 2002Zamperlini, Silva, et al., 1997Guillen, Iglesias, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m)  30.30.30.30.
Carrier gas He    
Substrate      
Column diameter (mm)  0.320.320.320.32
Phase thickness (mum)      
Program 70C(2min) => 30C/min => 150C => 5C/min => 200C => 4C/min => 310Cnot specifiednot specifiednot specifiednot specified
I 389.64389.60389.60391.21391.41
ReferenceTakada, Onda, et al., 1990Naikwadi, Charbonneau, et al., 1987Naikwadi, Charbonneau, et al., 1987Naikwadi, Charbonneau, et al., 1987Naikwadi, Charbonneau, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5SE-52SE-52SE-52
Column length (m)  30.   
Carrier gas  He   
Substrate      
Column diameter (mm)  0.25   
Phase thickness (mum)      
Program not specifiednot specifiednot specifiednot specifiednot specified
I 391.6389.60385.75389.11389.60
ReferenceTucminen, Wickstrom, et al., 1986Tong, Centen, et al., 1985Shlyakhov, 1984Shlyakhov, 1984Shlyakhov, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SE-52SE-52
Column length (m)   
Carrier gas   
Substrate   
Column diameter (mm)   
Phase thickness (mum)   
Program not specifiednot specified
I 389.97391.00
ReferenceShlyakhov, 1984Shlyakhov, 1984
Comment MSDC-RI MSDC-RI

References

Go To: Top, Lee's RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Wang, Li, et al., 2007
Wang, Z.; Li, K.; Lambert, P.; Yang, C., Identification, characterization and quantitation of pyrogenic polycylic aromatic hydrocarbons and other organic compounds in tire fire products, J. Chromatogr. A, 2007, 1139, 1, 14-26, https://doi.org/10.1016/j.chroma.2006.10.085 . [all data]

Wang, Li, et al., 2007, 2
Wang, Z.; Li, K.; Lambert, P.; Brown, C.E.; Yang, C.; Hollebone, B.P., Identification and characterization of polycyclic aromatic compounds in tire fire products and differentiation of pyrogenic PAHs from petrogenic PAHs in Proceedings of the 30th Arctic and Marine Oilspill (AMOP) Technical Seminar. Vol.1, 2007, 61-85. [all data]

Skrbic and Onjia, 2006
Skrbic, B.; Onjia, A., Prediction of Lee Retention Indices of Polycyclic Aromatic Hydrocarbons by Artificial Neural Networks, J. Chromatorg. A, 2006, 1108, 2, 279-284, https://doi.org/10.1016/j.chroma.2006.01.080 . [all data]

Aracil, Font, et al., 2005
Aracil, I.; Font, R.; Conesa, J.A., Semivolatile and volatile compounds from the pyrolysis and combustion of polyvinyl chloride, J. Anal. Appl. Pyrolysis, 2005, 74, 1-2, 465-478, https://doi.org/10.1016/j.jaap.2004.09.008 . [all data]

Ré-Poppi and Santiago-Silva, 2005
Ré-Poppi, N.; Santiago-Silva, M., Polycyclic aromatic hydrocarbons and other selected organic compounds in ambient air of Campo Grande City, Brazil, Atmos. Environ., 2005, 39, 16, 2839-2850, https://doi.org/10.1016/j.atmosenv.2004.10.006 . [all data]

Sremac, Skrbic, et al., 2005
Sremac, S.; Skrbic, B.; Onjia, A., Artificial neural network prediction of quantitative structure-retention relationships of polycyclic aromatic hydrocarbons in gas chromatography, J. Serb. Chem. Soc., 2005, 70, 11, 1291-1300, https://doi.org/10.2298/JSC0511291S . [all data]

Brack and Schirmer, 2003
Brack, W.; Schirmer, K., Effect-directed identification of oxygen and sulfur heterocycles as major polycyclic aromatic cytochrome P4501A-inducers in a contaminated sedimet, Environ. Sci. Technol., 2003, 37, 14, 3062-3070, https://doi.org/10.1021/es020248j . [all data]

Lundstedt, Haglund, et al., 2003
Lundstedt, S.; Haglund, P.; Öberg, L., Degradation and formation of polycyclic aromatic compounds during bioslurry treatment of an aged gasworks soil, Environ. Toxicol. Chem., 2003, 22, 7, 1413-1420, https://doi.org/10.1002/etc.5620220701 . [all data]

Ré-Poppi and Santiago-Silva, 2002
Ré-Poppi, N.; Santiago-Silva, M.R., Identification of polycyclic aromatic hydrocarbons and methoxylated phenols in wood smoke emitted during production of charcoal, Chromatographia, 2002, 55, 7/8, 475-481, https://doi.org/10.1007/BF02492280 . [all data]

Zamperlini, Silva, et al., 1997
Zamperlini, G.C.M.; Silva, M.R.S.; Vilegas, W., Identification of polycyclic aromatic hydrocarbons in sugar cane soot by gas chromatography-mass spectrometry, Chromatographia, 1997, 46, 11/12, 655-663, https://doi.org/10.1007/BF02490527 . [all data]

Guillen, Iglesias, et al., 1992
Guillen, M.D.; Iglesias, M.J.; Dominguez, A.; Blanco, C.G., Polynuclear aromatic hydrocarbon retention indices on SE-54 stationary phase of the volatile components of a coal tar pitch. Relationships between chromatographic retention and thermal reactivity, J. Chromatogr., 1992, 591, 1-2, 287-295, https://doi.org/10.1016/0021-9673(92)80246-Q . [all data]

Takada, Onda, et al., 1990
Takada, H.; Onda, T.; Ogura, N., Determination of polycyclic aromatic hydrocarbons in urban street dusts and their source materials by capillary gas chromatography, Environ. Sci. Technol., 1990, 24, 8, 1179-1186, https://doi.org/10.1021/es00078a005 . [all data]

Naikwadi, Charbonneau, et al., 1987
Naikwadi, K.P.; Charbonneau, G.M.; Karasek, F.W.; Clement, R.E., Separation and Identification of Organic Compounds in Air Particulate Extracts by High-Performance Liquid Chromatography and Gas Chromatography-Mass Spectrometry, J. Chromatogr., 1987, 398, 227-237, https://doi.org/10.1016/S0021-9673(01)96508-2 . [all data]

Tucminen, Wickstrom, et al., 1986
Tucminen, A.; Wickstrom, K.; Pyysalo, H., Determination of Polycyclic Aromatic Compounds by GLC-Selected Ion Monitoring (SIM) Technique, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 469-471, https://doi.org/10.1002/jhrc.1240090813 . [all data]

Tong, Centen, et al., 1985
Tong, H.Y.; Centen, J.D.; Karasek, F.W.; Jellum, E.; Helland, P., Identification of Trace Organic Compounds in Dimethyl Sulphoxide Solution Using High-Performance Liquid Chromatography and Gas Chromatography-Mass Spectrometry, J. Chromatogr., 1985, 324, 373-383, https://doi.org/10.1016/S0021-9673(01)81336-4 . [all data]

Shlyakhov, 1984
Shlyakhov, A.F., Gas chromatography in organic geochemistry, Nedra, Moscow, 1984, 221. [all data]


Notes

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