Cyclohexene, 3-(1,5-dimethyl-4-hexenyl)-6-methylene-, [S-(R*,S*)]-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSPolydimethyl siloxane with 5 % PhDB-5DB-5HP-5 MS
Column length (m) 30.30.35.35.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.25 0.200.200.25
Phase thickness (μm) 0.25 0.100.100.25
Tstart (C) 40.80.50.50.50.
Tend (C) 250.200.200.200.180.
Heat rate (K/min) 3.5.4.4.2.
Initial hold (min) 1.    
Final hold (min) 3.25.   
I 1525.1524.1524.1540.1518.
ReferenceJian-Yu, Zhu, et al., 2012Priya, Prathapan, et al., 2012Silva, Suzuki, et al., 2012Silva, Suzuki, et al., 2012Hammami, Kamoun, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSDB-1DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.70.60.40.35.
Tend (C) 200.290.250.240.220.
Heat rate (K/min) 2.5.4.3.3.
Initial hold (min)   1.1. 
Final hold (min)   10. 40.
I 1561.1530.1518.1518.1524.
ReferencePattiram, Lasekan, et al., 2011Lazarevic, Radulovic, et al., 2010Mirjalili, Salehi, et al., 2010de Souza, Lopes, et al., 2010El-Massry, El-Ghorab, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DB-5HP-5RTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeliumNitrogenHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.320.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.40.60.
Tend (C) 250.250.240.240.230.
Heat rate (K/min) 2.3.3.4.2.
Initial hold (min) 8.1.1.4. 
Final hold (min) 15.10.  35.
I 1534.1523.1518.1527.1516.
ReferenceFarhat, Ginies, et al., 2009Rahimi-Nasrabadi, Gholivand, et al., 2009de Souza, Lopes, et al., 2009Zhannan, Shiqiong, et al., 2009Paolini, Tomi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5MSDB-5Methyl Silicone
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.320.250.250.25 
Tstart (C) 60.60.60.60.50.
Tend (C) 250.280.240.240.240.
Heat rate (K/min) 5.3.3.2.3.
Initial hold (min) 30.    
Final hold (min)      
I 1526.1507.1523.1517.1523.
ReferenceYassa and Akhani, 2008Basta, Pavlovic, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007Miyazawa and Tamura, 2007Ozcan and Chalchat, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5HP-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas NitrogenHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.320.250.250.25
Tstart (C) 60.60.50.50.40.
Tend (C) 250.250.265.300.210.
Heat rate (K/min) 5.5.2.55.2.
Initial hold (min)  30.1.5.2.
Final hold (min) 10. 20.5.33.
I 1519.1526.1529.1523.1526.
ReferenceSonboli, Kanani, et al., 2007Yassa and Akhani, 2007Bazargani, Almasirad, et al., 2006Figuérédo, Cabassu, et al., 2006Garneau F.X., Collin G., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneBP-1ZB-5Methyl SiliconeBPX-5
Column length (m) 30.25.30.25.50.
Carrier gas HeliumHeHeN2 
Substrate      
Column diameter (mm) 0.250.30.250.30.22
Phase thickness (μm) 0.25 0.250.151.
Tstart (C) 60.70.40.50.70.
Tend (C) 280.220.300.210.280.
Heat rate (K/min) 3.4.2.2.4.
Initial hold (min)  2. 5. 
Final hold (min) 30.10.  4.
I 1493.1512.1504.1543.1557.
ReferenceMarongiu, Piras, et al., 2006Moody, Gundidza, et al., 2006Sari M., Biondi D.M., et al., 2006Tonzibo, Coffy, et al., 2006Wohlmuth, Smith, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5DB-1CP Sil 5 CBHP-5MS
Column length (m) 30.50.30.25.30.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.250.30.250.250.2
Phase thickness (μm) 0.250.250.250.15 
Tstart (C) 50.60.50.50.60.
Tend (C) 250.240.265.230.280.
Heat rate (K/min) 4.2.2.53.3.
Initial hold (min) 1. 1.  
Final hold (min) 10. 20.  
I 1507.1522.1516.1520.1523.
ReferenceWong, Sivasothy, et al., 2006Chagonda and Chalchat, 2005Khanavi, Ghasemian, et al., 2005Olawore, Ogunwande, et al., 2005Petrakis, Roussis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeHP-5MSHP-5MSRTX-5DB-1
Column length (m) 12.530.30.30.50.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.90.
Tend (C) 270.280.280.220.240.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min)      
Final hold (min)      
I 1512.1523.1523.1523.1501.
ReferenceRicci, Fraternale, et al., 2005Sajjadi S.E. and Eskandari B., 2005Sajjadi, 2005Szafranek, Chrapkowska, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5DB-5HP-5MSDB-1
Column length (m) 50.60.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.25 
Tstart (C) 50.40.60.60.50.
Tend (C) 220.280.300.275.250.
Heat rate (K/min) 4.4.3.4.4.
Initial hold (min) 3.4.   
Final hold (min) 30.    
I 1521.1525.1524.1522.1512.
ReferenceWong, Lee, et al., 2005Kalvandi, Sefidkon, et al., 2004Tirillini, Pellegrino, et al., 2004Afsharypuor and Jahromy, 2003Dabiri and Sefidkon, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5SilHP-1HP-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 70.70.70.60.60.
Tend (C) 200.200.210.275.240.
Heat rate (K/min) 4.10.2.4.3.
Initial hold (min)    5. 
Final hold (min) 10. 60.  
I 1524.1529.1520.1524.1528.
ReferenceDudai, Larkov, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003Mookdasanit, Tamura, et al., 2003Morteza-Semnani and Saeedi, 2003da Silva, Luz, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Cross-Linked MethylsiliconeDB-5DB-5DB-5
Column length (m) 60.25.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 40.70.60.60.60.
Tend (C) 250.250.240.240.240.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min) 15.    
Final hold (min)      
I 1524.1501.1525.1526.1526.
ReferenceStashenko, Jaramillo, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Zoghbi, Andrade, et al., 2003Flamini, Ertugrul, et al., 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1DB-1SPB-5HP-5
Column length (m) 30.50.50.60.30.
Carrier gas HeN2N2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.80.95.40.60.
Tend (C) 240.225.240.220.220.
Heat rate (K/min) 3.4.4.3.5.
Initial hold (min)    5.10.
Final hold (min)    15. 
I 1528.1503.1500.1527.1525.
ReferenceMaia, Zoghbi, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Cornu, Carnat, et al., 2001Flamini, Cioni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5DB-1OV-1
Column length (m) 30.30.30.33.50.
Carrier gas N2HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.500.25
Tstart (C) 60.60.60.50.50.
Tend (C) 220.240.270.135.250.
Heat rate (K/min) 5.3.3.20.10.
Initial hold (min) 10.  2.5.
Final hold (min)  30.  20.
I 1525.1518.1528.1518.1500.
ReferenceGallori, Flamini, et al., 2001Marongiu, Porcedda, et al., 2001Palmeira, Conserva, et al., 2001Feger, Brandauer, et al., 2000Kökdil, Kurucu, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1SE-54OV-1SE-30
Column length (m) 30.60.30.50.30.
Carrier gas  HeHydrogenHe 
Substrate      
Column diameter (mm) 0.250.250.250.20 
Phase thickness (μm) 0.250.250.250.20 
Tstart (C) 60.50.60.30.50.
Tend (C) 300.250.250.220.240.
Heat rate (K/min) 4.2.52.2.4.
Initial hold (min) 2.5.5. 2.
Final hold (min) 5. 2. 10.
I 1517.41514.1521.1504.1512.
ReferenceGawdzik, Mardarowicz, et al., 1996Stashenko, Puertas, et al., 1996Kollmannsberger, Nitz, et al., 1992de Pooter, Nicolai, et al., 1988Ramaswami, Briscese, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30
Column length (m) 30.
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 50.
Tend (C) 240.
Heat rate (K/min) 4.
Initial hold (min) 2.
Final hold (min) 10.
I 1512.
ReferenceRamaswami, Briscese, et al., 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Wong, Sivasothy, et al., 2006
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Khanavi, Ghasemian, et al., 2005
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Olawore, Ogunwande, et al., 2005
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Petrakis, Roussis, et al., 2005
Petrakis, P.V.; Roussis, V.; Papadimitriou, D.; Vagias, C.; Tsitsimpikou, C., The effect of terpenoid extracts from 15 pine species on the feeding behavioural sequence of the late instars of the pine processionary caterpillar Thaumetopoea pityocampa, Behav. Processes, 2005, 69, 3, 303-322, https://doi.org/10.1016/j.beproc.2004.12.008 . [all data]

Ricci, Fraternale, et al., 2005
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Notes

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