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(1R,4aS,8aR)-1-Isopropyl-4,7-dimethyl-1,2,4a,5,6,8a-hexahydronaphthalene


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-5MSHP-5MSHP-5MSHP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.60.60.80.
Tend (C) 200.280.280.280.300.
Heat rate (K/min) 3.4.4.3.4.
Initial hold (min) 2.5.5.  
Final hold (min) 15.    
I 1479.1482.1470.1479.1504.9
ReferencePoliteo, Jukic, et al., 2007Saroglou, Arfan, et al., 2007Saroglou, Marin, et al., 2007Vagionas, Ngassapa, et al., 2007Zeng, Zhao, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5HP-5MSDB-5MSDB-5
Column length (m) 50.60.30.60.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.26
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.250.280.200.246.
Heat rate (K/min) 2.3.4.2.3.
Initial hold (min)   5.  
Final hold (min) 20.  20. 
I 1475.1486.1474.1471.1484.
ReferenceBlanc, Bradesi, et al., 2006Perraudin, Popovici, et al., 2006Saroglou, Dorizas, et al., 2006Seo and Baek, 2005Adams, Habte, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSCP Sil 5 CBBP-1DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.40.
Tend (C) 280.280.200.220.200.
Heat rate (K/min) 4.4.5.5.4.
Initial hold (min) 5.5.  5.
Final hold (min)    13.20.
I 1485.1485.1491.1472.1483.
ReferenceGrujic-Jovanovic, Skaltsa, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004Martinez, Rosa, et al., 2004Raina, Kumar, et al., 2004Yu, Kim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5HP-5Ultra-2HP-5
Column length (m) 30.25.30.25.30.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 40.75.60.40.60.
Tend (C) 200.210.280.280.280.
Heat rate (K/min) 4.3.3.3.4.
Initial hold (min) 5.10. 2.5.
Final hold (min) 20.1. 10. 
I 1480.1506.1485.1482.1485.
ReferenceYu, Kim, et al., 2004, 2bin Ahmad and bin Jantan, 2003Bougatsos, Meyer, et al., 2003Ceva-Antunes, Bizzo, et al., 2003Karioti, Skaltsa, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5BP-1HP-5
Column length (m) 30.25.30.50. 
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.220.26
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.70.60.60.60.
Tend (C) 280.275.280.220.240.
Heat rate (K/min) 4.4.3.2.3.
Initial hold (min) 5. 5.  
Final hold (min)    20. 
I 1470.1468.1475.1470.1433.
ReferenceSkaltsa, Demetzos, et al., 2003Javidnia, Miri, et al., 2002Aligiannis, Kalpoutzakis, et al., 2001Rezzi, Cavaleiro, et al., 2001Oprean, Tamas, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 60.
Carrier gas He
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.25
Tstart (C) 50.
Tend (C) 250.
Heat rate (K/min) 3.5
Initial hold (min) 5.
Final hold (min)  
I 1453.
ReferenceStashenko, Prada, et al., 1996
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Politeo, Jukic, et al., 2007
Politeo, O.; Jukic, M.; Milos, M., Chemical composition and antioxidant capacity of free volatile aglycones from basil (Ocimum basilicum L.) compared with its essential oil, Food Chem., 2007, 101, 1, 379-385, https://doi.org/10.1016/j.foodchem.2006.01.045 . [all data]

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Saroglou, Dorizas, et al., 2006
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Seo and Baek, 2005
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Adams, Habte, et al., 2004
Adams, R.P.; Habte, M.; Park, S.; Dafforn, M.R., Preliminary comparison of vetiver root essential oils from cleansed (bacteria- and fungus-free) versus non-cleansed (normal) vetiver plants, Biochem. Syst. Ecol., 2004, 32, 12, 1137-1144, https://doi.org/10.1016/j.bse.2004.03.013 . [all data]

Grujic-Jovanovic, Skaltsa, et al., 2004
Grujic-Jovanovic, S.; Skaltsa, H.D.; Marin, P.; Sokovic, M., Composition and antibacterial activity of the essential oil of six Stachys species from Serbia, Flavour Fragr. J., 2004, 19, 2, 139-144, https://doi.org/10.1002/ffj.1275 . [all data]

Karioti, Hadjipavlou-Litina, et al., 2004
Karioti, A.; Hadjipavlou-Litina, D.; Mensah, M.L.K.; Fleischer, T.C.; Skaltsa, H., Composition and antioxidant activity of the essential oils of Xylopia aethiopica (Dun) A. Rich. (Annonaceae) leaves, stem bark, root bark, and fresh and dried fruits, growing in Ghana, J. Agric. Food Chem., 2004, 52, 26, 8094-8098, https://doi.org/10.1021/jf040150j . [all data]

Martinez, Rosa, et al., 2004
Martinez, J.; Rosa, P.T.V.; Menut, C.; Leydet, A.; Brat, P.; Pallet, D.; Meireles, M.A.A., Valorization of Brazilian vetiver (Vetiveria zizanioides (L.) Nash ex Small) oil, J. Agric. Food Chem., 2004, 52, 21, 6578-6584, https://doi.org/10.1021/jf049182x . [all data]

Raina, Kumar, et al., 2004
Raina, V.K.; Kumar, A.; Srivastava, S.K.; Syamsundar, K.V.; Kahol, A.P., Essential oil composition of 'kewda' (Pandanus odoratissimus) from India, Flavour Fragr. J., 2004, 19, 5, 434-436, https://doi.org/10.1002/ffj.1331 . [all data]

Yu, Kim, et al., 2004
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Aroma-active compounds of Pinus densiflora (red pine) needles, Flavour Fragr. J., 2004, 19, 6, 532-537, https://doi.org/10.1002/ffj.1337 . [all data]

Yu, Kim, et al., 2004, 2
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Characterization of aroma-active compounds of Abies nephrolepis (Khingan fir) needles using aroma extract dilution analysis, Flavour Fragr. J., 2004, 19, 1, 74-79, https://doi.org/10.1002/ffj.1314 . [all data]

bin Ahmad and bin Jantan, 2003
bin Ahmad, F.; bin Jantan, I., Chemical constituents of the essential oils of Goniothalamus uvariodes King, Flavour Fragr. J., 2003, 18, 2, 128-130, https://doi.org/10.1002/ffj.1142 . [all data]

Bougatsos, Meyer, et al., 2003
Bougatsos, C.; Meyer, J.J.M.; Magiatis, P.; Vagias, C.; Chinou, I.B., Composition and antimicrobial activity of the essential oils of Helichrysum kraussii Sch. Bip. and H. rugulosum Less. from south Africa, Flavour Fragr. J., 2003, 18, 1, 48-51, https://doi.org/10.1002/ffj.1152 . [all data]

Ceva-Antunes, Bizzo, et al., 2003
Ceva-Antunes, P.M.N.; Bizzo, H.R.; Alves, S.M.; Antunes, O.A.C., Analysis of volatile compounds of taperebá (Spondias mombin L.) and Cajá (Spondias mombin L.) by simultaneous distillation and extraction (SDE) and solid phase microextraction (SPME), J. Agric. Food Chem., 2003, 51, 5, 1387-1392, https://doi.org/10.1021/jf025873m . [all data]

Karioti, Skaltsa, et al., 2003
Karioti, A.; Skaltsa, H.; Demetzos, C.; Perdetzoglou, D.; Economakis, C.D.; Salem, A.B., Effect of nitrogen concentration of the nutrient solution on the volatile constituents of leaves of Salvia fruticosa Mill. in solution culture, J. Agric. Food Chem., 2003, 51, 22, 6505-6508, https://doi.org/10.1021/jf030308k . [all data]

Skaltsa, Demetzos, et al., 2003
Skaltsa, H.D.; Demetzos, C.; Lazari, D.; Sokovic, M., Essential oil analysis and antimicrobial activity of eight Stachys species from Greece, Phytochemistry, 2003, 64, 3, 743-752, https://doi.org/10.1016/S0031-9422(03)00386-8 . [all data]

Javidnia, Miri, et al., 2002
Javidnia, K.; Miri, R.; Safavi, F.; Azarpira, A.; Shafiee, A., Composition of the essential oil of Nepeta persica Boiss from Iran, Flavour Fragr. J., 2002, 17, 1, 20-22, https://doi.org/10.1002/ffj.1023 . [all data]

Aligiannis, Kalpoutzakis, et al., 2001
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Rezzi, Cavaleiro, et al., 2001
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Stashenko, Prada, et al., 1996
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References