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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1BP-1DB-5Methyl Silicone
Column length (m) 50.50.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.80.
Tend (C) 220.220.220.240.220.
Heat rate (K/min) 2.2.2.3.2.
Initial hold (min)      
Final hold (min) 20.20.20. 15.
I 1628.1627.1627.1643.1635.
ReferenceBoti, Koukoua, et al., 2007Duquesnoy, Castola, et al., 2007Lesueur, de Rocca Serra, et al., 2007Maccioni, Baldini, et al., 2007Melo, Corrêa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5SPB-1HP-5MSDB-5
Column length (m) 60.30.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 230.250.250.280.200.
Heat rate (K/min) 2.4.5.4.2.
Initial hold (min)  4.3.5. 
Final hold (min) 35.10.15. 60.
I 1628.1640.1626.1641.1646.
ReferencePaolini, Muselli, et al., 2007Quijano, Salamanca, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007Rout, Rao, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSBP-1BP-1
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.280.220.220.
Heat rate (K/min) 4.3.3.2.2.
Initial hold (min) 5.    
Final hold (min)    20.20.
I 1641.1645.1617.1629.1620.
ReferenceSaroglou, Marin, et al., 2007Vagionas, Ngassapa, et al., 2007Basta, Tzakou, et al., 2006Blanc, Bradesi, et al., 2006Duquesnoy, Dinh, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1DB-1SPB-1OV-1
Column length (m) 30.50.30.30.25.
Carrier gas N2HeN2HeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.50.
Tend (C) 220.220.220.250.220.
Heat rate (K/min) 5.2.4.5.3.
Initial hold (min) 10.  3.1.
Final hold (min)  20. 15.5.
I 1646.1629.1644.1645.1643.
ReferenceFlamini, Tebano, et al., 2006Gonny, Cavaleiro, et al., 2006Kuiate, Bessière, et al., 2006Radulovic, Mananjarasoa, et al., 2006Rubiolo P., Matteodo M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5SE-54HP-5
Column length (m) 30.30.30.50.30.
Carrier gas HeHeHeH2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.270.25
Tstart (C) 60.50.40.50.60.
Tend (C) 280.250.300.300.220.
Heat rate (K/min) 4.5.4.5.5.
Initial hold (min) 5.2.5. 10.
Final hold (min)      
I 1639.1642.1653.1659.1643.
ReferenceSaroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Vundac, Pfeifhofer, et al., 2006Brantner, Pfeifhofer, et al., 2005Celik, Gokturk, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBRTX-1HP-5MSBP-1
Column length (m) 30.50.60.30.50.
Carrier gas N2H2HeHeHe
Substrate      
Column diameter (mm) 0.250.220.220.250.22
Phase thickness (mum) 0.250.130.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 220.300.230.250.230.
Heat rate (K/min) 5.4.2.4.2.
Initial hold (min) 10.  2. 
Final hold (min)  10.35.20.35.
I 1643.1630.1625.1641.1636.
ReferenceFlamini, Luigi Cioni, et al., 2005Idzojtic, Kajba, et al., 2005Paolini, Costa, et al., 2005Pino, Mesa, et al., 2005Vellutini, Baldovini, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MSSPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.80.80.60.70.
Tend (C) 290.290.290.280.220.
Heat rate (K/min) 2.4.6.3.3.
Initial hold (min)      
Final hold (min)     15.
I 1638.21645.71651.21654.1628.
ReferenceZhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5HP-5MSHP-5MSDB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.60.60.40.
Tend (C) 220.220.280.280.280.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min)  10.5.5.2.
Final hold (min) 15.    
I 1615.1642.1640.1641.1654.
ReferenceCavaleiro, Salgueiro, et al., 2004Flamini, Luigi Cioni, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200BP-1HP-5HP-5HP-5MS
Column length (m) 30.30.25.50.30.
Carrier gas H2N2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.20.20.25
Phase thickness (mum) 0.250.250.330.20.25
Tstart (C) 40.60.60.35.60.
Tend (C) 280.220.240.250.280.
Heat rate (K/min) 6.5.3.3.3.
Initial hold (min) 5.  15. 
Final hold (min) 5.13.7.40. 
I 1658.1627.1643.1641.1620.
ReferenceNgassoum, Ousmaila, et al., 2004Raina, Kumar, et al., 2004Sartoratto, Machado, et al., 2004Stashenko, Jaramillo, et al., 2004Tzakou, Vagias, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima 5DB-5MSDB-5MSDB-1HP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.40.50.60.
Tend (C) 280.200.200.200.220.
Heat rate (K/min) 3.4.4.5.5.
Initial hold (min)  5.5. 10.
Final hold (min) 20.20.20.0. 
I 1628.1651.1661.1627.1608.
ReferenceVérité, Nacer, et al., 2004Yu, Kim, et al., 2004Yu, Kim, et al., 2004, 2Boyom, Assembe, et al., 2003Campeol, Flamini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1RTX-1HP-5DB-1DB-1
Column length (m) 30.60.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.20.220.250.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.60.40.40.
Tend (C) 220.230.220.250.250.
Heat rate (K/min) 3.2.5.2.2.
Initial hold (min)   10.5.5.
Final hold (min) 15.45. 20. 
I 1627.1633.1643.1611.1623.
ReferenceCavaleiro, Salgueiro, et al., 2003Cavalli, Tomi, et al., 2003Dural, Bagci, et al., 2003de Feo, Bruno, et al., 2003de Feo, Urrunaga Soria, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-1SPB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (mum) 0.250.250.330.200.25
Tstart (C) 60.60.40.70.50.
Tend (C) 280.240.260.220.280.
Heat rate (K/min) 4.3.2.3.3.
Initial hold (min) 5. 5. 5.
Final hold (min)   20.15. 
I 1641.1643.1641.1627.1641.
ReferenceKarioti, Skaltsa, et al., 2003Macchioni, Cioni, et al., 2003Senatore, Rigano, et al., 2003Cavaleiro, Salgueiro, et al., 2002Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBRTX-5HP-1CP Sil 5 CBCP Sil 5 CB
Column length (m) 50.30.24.30.50.
Carrier gas H2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (mum) 0.150.250.170.250.4
Tstart (C) 40.45.60.60.60.
Tend (C) 300.300.250.280.280.
Heat rate (K/min) 4.3.4.2.3.
Initial hold (min) 3.6.2.10.10.
Final hold (min)  10.20.40.60.
I 1654.1650.1621.1630.1622.
ReferenceHeinrich, Pfeifhofer, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5CP Sil 5 CBBP-1BP-1
Column length (m) 30.30.50.50.50.
Carrier gas HeH2HeHe 
Substrate      
Column diameter (mm) 0.250.250.320.220.22
Phase thickness (mum) 0.250.250.40.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.240.280.220.220.
Heat rate (K/min) 3.3.3.2.2.
Initial hold (min) 5. 10.  
Final hold (min)   60.20.20.
I 1641.1643.1622.1630.1638.
ReferenceGiamakis, Kretsi, et al., 2001Nogueira, Bittrich, et al., 2001Pino, Marbot, et al., 2001Rezzi, Bighelli, et al., 2001Rezzi, Cavaleiro, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5DB-5CP Sil 5 CB
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum) 0.250.250.250.250.13
Tstart (C) 60.50.50.60.40.
Tend (C) 280.280.280.240.300.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min) 5.5.5.2. 
Final hold (min)     10.
I 1641.1641.1641.1641.1649.
ReferenceSkaltsa, Mavrommati, et al., 2001Lazari, Skaltsa, et al., 2000Lazari, Skaltsa, et al., 2000, 2Maia, de Paula, et al., 2000Pfeifhofer, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1Methyl SiliconeOV-1DB-1
Column length (m) 30.30.50.25.60.
Carrier gas He N2 He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.170.30.25
Tstart (C) 50.50.80.50.50.
Tend (C) 280.220.200.200.250.
Heat rate (K/min) 4.3.2.3.3.5
Initial hold (min) 5.3. 1.5.
Final hold (min)    20. 
I 1641.1606.1619.1608.1639.
ReferenceLazari, Skaltsa, et al., 1999Muselli, Hoi, et al., 1999Sumathykutty, Rao, et al., 1999Bicchi, Rubiolo, et al., 1998Stashenko, Prada, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase HP-101
Column length (m) 50.
Carrier gas N2
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 200.
Heat rate (K/min) 3.
Initial hold (min)  
Final hold (min)  
I 1659.
ReferenceChung, Eiserich, et al., 1993
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References