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(1R,3E,7E,11R)-1,5,5,8-Tetramethyl-12-oxabicyclo[9.1.0]dodeca-3,7-diene


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5 MSHP-5 MS
Column length (m) 25.25.25.30.30.
Carrier gas HydrogenHydrogenHydrogen Helium
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.520.520.520.250.25
Tstart (C) 40.40.40.60.60.
Tend (C) 280.280.280.300.220.
Heat rate (K/min) 4.4.4.15.5.
Initial hold (min)    2.10.
Final hold (min) 10.10.10.10. 
I 1603.1603.1603.1579.1609.
ReferenceVelickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Xu, Han, et al., 2012Ogunwande, Flamini, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneHP-5 MSSLB-5 MSDB-5 MSElite-1
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 90.60.50.50.60.
Tend (C) 225.300.250.300.246.
Heat rate (K/min) 3.15.3.5.3.
Initial hold (min)  2.2.5. 
Final hold (min) 3.10.10.5. 
I 1609.1579.1613.1603.1602.
ReferenceRetta, Gattuso, et al., 2009Xu, Han, et al., 2009Lo Presti, Sciarrone, et al., 2008Noudogbessi, Yedomonhan, et al., 2008Raj, Baby, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSDB-5MSCP Sil 5 CBHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeN2Helium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 240.230.240.300.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)  10.  5.
Final hold (min)  10.   
I 1652.1606.1607.1602.1608.
ReferenceSarikurkcu, Tepe, et al., 2008Adams, Beauchamp, et al., 2007Andrade, Oliveira, et al., 2007Baran, von Reuss, et al., 2007Capetanos, Saroglou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSHP-5MSDB-5MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 240.240.250.280.220.
Heat rate (K/min) 5.3.2.3.4.
Initial hold (min) 1. 8. 5.
Final hold (min) 4. 15.30.20.
I 1606.1607.1602.1568.1605.
ReferenceCheraif, Ben Jannet, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Marongiu B., Piras A., et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-5Elite-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHelium He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 50.60.40.40.40.
Tend (C) 260.300.260.210.280.
Heat rate (K/min) 2.53.4.2.4.
Initial hold (min) 1.   5.
Final hold (min) 20.  33.10.
I 1573.1578.1602.1600.1614.
ReferenceMonser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Sylvestre, Longtin, et al., 2007Tava, Pecetti, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5HP-5CP Sil 5 CB
Column length (m) 30.50.30.30.30.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 300.220.246.300.200.
Heat rate (K/min) 3.2.3.5.5.
Initial hold (min)    5. 
Final hold (min)  20. 5. 
I 1600.1600.1607.1610.1609.
ReferenceApel, Sobral, et al., 2006Boti, Yao, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Figuérédo, Cabassu, et al., 2006Martin, Joseph, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5HP-5MS
Column length (m) 25.30.30.25.30.
Carrier gas N2HydrogenHydrogenH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.70.70.60.60.
Tend (C) 200.280.280.240.243.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 3.4.4.  
Final hold (min)      
I 1602.1601.1606.1613.1598.
ReferenceOuamba, Ouabonzi, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006Potzernheim, Bizzo, et al., 2006Sabulal, Dan, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5SPB-1DB-5DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.3
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.50.40.60.
Tend (C) 280.260.250.250.240.
Heat rate (K/min) 4.2.4.4.2.
Initial hold (min)  5.1.  
Final hold (min)  20.10.  
I 1610.1610.1576.1608.1604.
ReferenceSajjadi, 2006Senatore, Landolfi, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Chagonda and Chalchat, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5HP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 40.60.60.50.60.
Tend (C) 220.240.300.300.200.
Heat rate (K/min) 3.3.3.5.4.
Initial hold (min) 5. 3.5.30.
Final hold (min)    5. 
I 1610.1606.1605.1610.1601.
ReferenceChagonda and Chalchat, 2005, 2Chaverri and Cicció, 2005Ferraz, Limberger, et al., 2005Figuérédo, Cabassu, et al., 2005Gauvin and Smadja, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.35.60.50.60.
Tend (C) 265.280.230.250.220.
Heat rate (K/min) 2.54.3.3.4.
Initial hold (min) 1.2. 10.4.
Final hold (min) 30.  5. 
I 1575.1620.1594.1616.1608.
ReferenceKhalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Kowalski and Wolski, 2005Limberger, Sobral, et al., 2005Melkani, Dev, et al., 2005Morteza-Semnani and Saeedi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5MSDB-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2 HeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 200.280.280.240.300.
Heat rate (K/min) 5.3.4.3.3.
Initial hold (min)      
Final hold (min)      
I 1593.1608.1606.1606.1597.
ReferenceNyegue, Belinga-Ndoye, et al., 2005Petrakis, Roussis, et al., 2005Sajjadi S.E. and Eskandari B., 2005da Silva, Andrade, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5CP Sil 5 CBDB-1RTX-1
Column length (m) 30.30.30.30.30.
Carrier gas N2H2N2N2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.50.60.
Tend (C) 220.290.200.200.300.
Heat rate (K/min) 5.4.5.5.4.
Initial hold (min)      
Final hold (min) 15.    
I 1596.1608.1600.1601.1597.
ReferenceSrivastava, Srivastava, et al., 2005Abreu, Reis, et al., 2004Agnaniet, Menut, et al., 2004Fekam Boyom, Fotio, et al., 2004Kalemba and Thiem, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5MSDB-5DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 260.240.300.210.280.
Heat rate (K/min) 2.3.3.2.3.
Initial hold (min) 5.  2. 
Final hold (min)    33. 
I 1596.1606.1602.1601.1609.
ReferenceKilic, Hafizoglu, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004Lopez Arze, Collin, et al., 2004Malencic, Couladis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5CP Sil 5 CBDB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.150.390.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.220.220.250.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)   3.  
Final hold (min)      
I 1603.1603.1602.1597.1604.
ReferenceMalencic, Couladis, et al., 2004Malencic, Couladis, et al., 2004Mevy, Bessiere, et al., 2004Khanavi, Hadjiakhoondi, et al., 2003Limberger, Simões-Pires, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.280.280.280.280.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)     10.
Final hold (min)  30.30.30.40.
I 1609.1587.1591.1590.1606.
ReferenceMaia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003Marongiu, Porcedda, et al., 2003Marongiu, Porcedda, et al., 2003Pino, Marbot, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5HP-5
Column length (m) 30.30.30.25.25.
Carrier gas H2HeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.530.53
Tstart (C) 60.60.60.40.40.
Tend (C) 280.280.240.280.280.
Heat rate (K/min) 4.3.3.4.4.
Initial hold (min) 10.    
Final hold (min) 40.    
I 1606.1589.1610.1602.1608.
ReferencePino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003da Silva, Luz, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.23
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 60.60.60.60.50.
Tend (C) 240.240.240.250.250.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min)      
I 1607.1609.1606.1594.1595.
ReferenceZoghbi, Andrade, et al., 2003Flamini, Ertugrul, et al., 2002Kobaisy, Tellez, et al., 2002Limberger, Simões-Pires, et al., 2002Mahmout, Bessière, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSOV-101DB-5MSDB-5HP-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 240.200.270.240.220.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min)     10.
Final hold (min)      
I 1606.1598.1606.1606.1608.
ReferenceMaia, Zoghbi, et al., 2002Menut, Bessière, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Flamini, Cioni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-1CP Sil 5 CBDB-5
Column length (m) 30.30.30.25.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.25 0.40.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.270.240.260.240.
Heat rate (K/min) 4.3.3.5.3.
Initial hold (min)    40. 
Final hold (min)      
I 1597.1613.1605.01591.1606.
ReferenceKalemba, Marschall, et al., 2001Palmeira, Conserva, et al., 2001Santos, Moreira, et al., 2001Baser, Özek, et al., 2000Tellez, Dayan, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CP Sil 5 CBCP Sil 5 CBDB-5MSDB-5
Column length (m) 30.25.25.30.30.
Carrier gas N2HeN2HeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (mum) 0.250.390.390.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.220.220.240.240.
Heat rate (K/min) 4.5.5.3.3.
Initial hold (min)  5.   
Final hold (min)  20.   
I 1597.1597.1598.1614.1607.
ReferenceKalemba, 1999Rustaiyan, Masoudi, et al., 1999Weyerstahl, Marschall, et al., 1999Zoghbi, Andrade, et al., 1999Maia, Zohhbi, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-5OV-1OV-101
Column length (m) 30.30.30.
Carrier gas Helium N2
Substrate    
Column diameter (mm) 0.250.320.25
Phase thickness (mum) 0.250.25 
Tstart (C) 60.40.100.
Tend (C) 240.270.220.
Heat rate (K/min) 3.2.5.
Initial hold (min)  4. 
Final hold (min)    
I 1610.1585.1614.
ReferenceSantos, Andrade, et al., 1998Kökdil, Tanker, et al., 1997Menut, Lamaty, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Velickovic, Ristic, et al., 2012
Velickovic, D.T.; Ristic, M.S.; Karabegovic, I.T.; Stojicevic, S.S.; Lazic, M.L., The influence of the distillation method on the chemical composition of the essential oil of sage (Salvia officinalis L.), Advanced Technologies, 2012, 1, 1, 47-51. [all data]

Xu, Han, et al., 2012
Xu, L.-L.; Han, T.; Wu, J.-Z.; Zhang, Q.-Y.; Zhang, H.; Huang, B.-K.; Rahman, K., Comparative research of chemical constituents, antifungal and antitumor properties of ether extracts of Panax ginseng and its endophytic fungus, 2012, retrieved from http://www.thefreelibrary.com/Comparative .... [all data]

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Ogunwande, I.A.; Flamini, G.; Cioni, P.L.; Omikorede, O.; Azeez, R.A.; Ayodele, A.A.; Kamil, Y.O., Aromatic plants growing in Nigeria: essential oil constituents of Cassia alata (Linn.) Roxb. and Helianthus annuus L., Rec. Nat. Prod., 2010, 4, 4, 211-217. [all data]

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Retta, D.; Gattuso, M.; Gattuso, S.; Lira, P. Di Leo; van Baren, C.; Ferraro, G.; Bandoni A., Essential oil composition of Achyrocline flaccida (Weinm.) DC. (Asteraceae) from different locations of Argentina, Biochem. Systematics Ecol., 2009, 36, 12, 877-881, https://doi.org/10.1016/j.bse.2008.11.001 . [all data]

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Xu, L.-L.; Han, T.; Wu, J.-Z.; Zhang, Q.-Y.; Zhang, H.; Huang, B.-K.; Rahman, K., Comparative research of chemical constituents, antifungal and antitumor properties of ether extracts of Panax ginseng and its endophytic fungus, Phytomedicine: Int. J. Phytotherapy Phytopharmacology, 2009, 16, 6-7, 609-616, https://doi.org/10.1016/j.phymed.2009.03.014 . [all data]

Lo Presti, Sciarrone, et al., 2008
Lo Presti, M.; Sciarrone, D.; Crupi, M.C.; Costa, R.; Ragusa, S.; Dugo, G.; Mondello, L., Evaliation of the volatile and chiral composition in Pistacia lentiscus L. essential oil, Flavour Fragr. J., 2008, 23, 4, 249-257, https://doi.org/10.1002/ffj.1878 . [all data]

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Noudogbessi, J.-P.; Yedomonhan, P.; Sohounhloue, D.C.K.; Chalchat, J.-C.; Figueredo, G., Chemical composition of essential oil of syzygium guineense (Willd.) DC. var. guineense (Myrtaceae) from Benin, Rec. Nat. Prod., 2008, 33-38. [all data]

Raj, Baby, et al., 2008
Raj, G.; Baby, S.; Dan, M.; Thaha, A.R.M.; Sethuraman, M.G.; George, V., Volatile constituents from the rhisomes of Curcuma haritha Mangaly and Sabu from Sauthern India, Flavour Fragr. J., 2008, 23, 5, 348-352, https://doi.org/10.1002/ffj.1891 . [all data]

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Notes

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