Perylene

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 17.533.316.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.210.500.500.500.50
Phase thickness (μm)      
Tstart (C) 100.50.50.50.50.
Tend (C) 280.320.320.320.320.
Heat rate (K/min) 2.6.6.6.6.
Initial hold (min)  5.5.5.5.
Final hold (min)      
I 2837.22800.2791.2795.2795.
ReferencePozhidaev, Berezkin, et al., 1988Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.616.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.500.500.500.500.50
Phase thickness (μm)      
Tstart (C) 50.50.50.50.50.
Tend (C) 320.320.320.320.320.
Heat rate (K/min) 6.6.6.6.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 2795.2795.2815.2815.2815.
ReferenceBeernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.616.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.500.500.500.500.50
Phase thickness (μm)      
Tstart (C) 50.50.50.50.50.
Tend (C) 320.320.320.320.320.
Heat rate (K/min) 6.6.6.6.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 2815.2825.2828.2832.2837.
ReferenceBeernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.612.12.65.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.500.500.30.280.3
Phase thickness (μm)   0.340.17 
Tstart (C) 50.50.50.50.100.
Tend (C) 320.320.250.250.300.
Heat rate (K/min) 6.6.2.2.1.8
Initial hold (min) 5.5.   
Final hold (min)      
I 2847.2848.2812.492815.422800.
ReferenceBeernaert, 1979Beernaert, 1979Lee, Vassilaros, et al., 1979Lee, Vassilaros, et al., 1979Carugno and Rossi, 1967
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pozhidaev, Berezkin, et al., 1988
Pozhidaev, V.M.; Berezkin, V.G.; Korolev, A.A.; Popova, T.P.; Pozhidaeva, K.A., Retention indices of polycyclic aromatic hydrocarbons on quartz capillary columns with chemically immobilized stationary phases, Zh. Anal. Khim., 1988, 43, 1082-1088. [all data]

Beernaert, 1979
Beernaert, H., Gas Chromatographic Analysis of Polyclylic Aromatic Hydrocarbons, J. Chromatogr., 1979, 173, 1, 109-118, https://doi.org/10.1016/S0021-9673(01)80450-7 . [all data]

Lee, Vassilaros, et al., 1979
Lee, M.L.; Vassilaros, D.L.; White, C.M.; Novotny, M., Retention Indices for Programmed-Temperature Capillary-Column Gas Chromatography of Polycyclic Aromatic Hydrocarbons, Anal. Chem., 1979, 51, 6, 768-773, https://doi.org/10.1021/ac50042a043 . [all data]

Carugno and Rossi, 1967
Carugno, N.; Rossi, S., Evaluation of polynuclear hydrocarbons in cigarette smoke by glass capillary columns, J. Gas Chromatogr., 1967, 5, 2, 103-106, https://doi.org/10.1093/chromsci/5.2.103 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References