1-Naphthalenol, 1,2,3,4,4a,7,8,8a-octahydro-1,6-dimethyl-4-(1-methylethyl)-, [1R-(1α,4β,4aβ,8aβ)]-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.55.60.
Tend (C) 240.250.280.240.240.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min)  4.5.2. 
Final hold (min)  10. 15. 
I 1647.1642.1643.1651.1645.
ReferenceMaccioni, Baldini, et al., 2007Quijano, Salamanca, et al., 2007Saroglou, Marin, et al., 2007Silva, Barbosa, et al., 2007Telascrea, de Araujo, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-1HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 280.220.220.280.280.
Heat rate (K/min) 3.5.4.3.3.
Initial hold (min)  10.   
Final hold (min)      
I 1620.1649.1646.1643.1615.
ReferenceBasta, Tzakou, et al., 2006Flamini, Tebano, et al., 2006Kuiate, Bessière, et al., 2006Kukic J., Petrovic S., et al., 2006Pavlovic, Kovacevic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5HP-5MSDB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.240.240.280.250.
Heat rate (K/min) 3.4.4.4.5.
Initial hold (min)    5.2.
Final hold (min)      
I 1632.1646.1643.1642.1646.
ReferencePavlovic, Tzakou, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Saroglou, Dorizas, et al., 2006Su, Ho, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.60.50.60.60.
Tend (C) 250.250.260.260.250.
Heat rate (K/min) 5.10.2.3.4.
Initial hold (min) 2.2.3. 2.
Final hold (min)  10.5. 20.
I 1646.1668.1622.1645.1643.
ReferenceSu, Ho, et al., 2006, 2Zhao J.Y., Liu J.M., et al., 2006Dob, Berramdane, et al., 2005Javidnia, Miri, et al., 2005Pino, Mesa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-1HP-5HP-5SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.2
Tstart (C) 40.70.60.60.70.
Tend (C) 260.220.220.220.220.
Heat rate (K/min) 2.3.5.5.3.
Initial hold (min) 5. 10.10. 
Final hold (min) 20.15.  15.
I 1647.1616.1645.1645.1619.
ReferenceSenatore, Napolitano, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Bertoli, Menichini, et al., 2004Bertoli, Pistelli, et al., 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5MSHP-5HP-5MSDB-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.170.25 0.250.25
Tstart (C) 50.60.60.60.40.
Tend (C) 200.280.260.280.280.
Heat rate (K/min) 3.4.3.4.4.
Initial hold (min)  5. 5.2.
Final hold (min)      
I 1611.1646.1645.1643.1656.
ReferenceFernández-Ocaña, Gómez-Rodríguez, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Javidnia, Miri, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSDB-1HP-5DB-5
Column length (m) 30.30.30.30.25.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25  
Tstart (C) 60.40.50.25.60.
Tend (C) 280.200.200.150.260.
Heat rate (K/min) 3.4.5.3.4.
Initial hold (min)  5. 5. 
Final hold (min)  20.0.  
I 1629.1640.1630.1645.1643.
ReferenceTzakou, Vagias, et al., 2004Yu, Kim, et al., 2004Boyom, Assembe, et al., 2003Isidorov, Vinogorova, et al., 2003Javidnia, Miri, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1RTX-5HP-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 40.45.60.60.50.
Tend (C) 260.250.280.280.280.
Heat rate (K/min) 2.3.4.3.3.
Initial hold (min) 5.6.5. 5.
Final hold (min) 20.    
I 1645.1656.1643.1646.1645.
ReferenceSenatore, Rigano, et al., 2003Shellie, Marriott, et al., 2003Skaltsa, Demetzos, et al., 2003Tsiri, Kretsi, et al., 2003Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5RTX-5CP Sil 5 CBRTX-5
Column length (m) 30.30.30.50.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.40.25
Tstart (C) 60.60.45.60.45.
Tend (C) 280.260.300.280.250.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min) 5. 6.10.6.
Final hold (min)   10.60. 
I 1646.1645.1654.1631.1645.
ReferenceFokialakis, Magiatis, et al., 2002Javidnia, Miri, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5DB-5CP Sil 5 CBHP-5MS
Column length (m) 30.30.30.50.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.40.25
Tstart (C) 45.60.60.60.60.
Tend (C) 250.260.240.280.280.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min) 6.  10.5.
Final hold (min)  10. 60. 
I 1652.1646.1646.1631.1643.
ReferenceShellie, Mondello, et al., 2002Couladis, Baziou, et al., 2001Nogueira, Bittrich, et al., 2001Pino, Marbot, et al., 2001Skaltsa, Mavrommati, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-1HP-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.50.50.
Tend (C) 240.280.280.220.250.
Heat rate (K/min) 3.4.4.3.2.5
Initial hold (min) 2.5.5.3.5.
Final hold (min)      
I 1645.1642.1645.1608.1620.
ReferenceMaia, de Paula, et al., 2000Skaltsa, Lazari, et al., 2000Lazari, Skaltsa, et al., 1999Muselli, Hoi, et al., 1999Stashenko, Cervantes, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5OV-1DB-1HP-101
Column length (m) 25.30.25.60.50.
Carrier gas   H2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.30.250.30.25 
Tstart (C) 50.50.50.50.70.
Tend (C) 200.250.200.250.200.
Heat rate (K/min) 3.3.3.3.53.
Initial hold (min) 1. 1.5. 
Final hold (min) 20. 20.  
I 1608.1649.1610.1627.1657.
ReferenceBicchi, Rubiolo, et al., 1998Isidorov, Zenkevich, et al., 1998Bicchi, Fresia, et al., 1997Stashenko, Prada, et al., 1996Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Maccioni, Baldini, et al., 2007
Maccioni, S.; Baldini, R.; Luigi Cioni, P.; Tebano, M.; Flamini, G., In vivo volatiles emission and essential oils from different organs and pollen of Cistus albidus from Caprione (Eastern Liguria, Italy), Flavour Fragr. J., 2007, 22, 1, 61-65, https://doi.org/10.1002/ffj.1759 . [all data]

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Silva, C.J.; Barbosa, L.C.A.; Maltha, C.R.A.; Pinheiro, A.L.; Ismail, F.M.D., Comparative study of the essential oils of seven Melaleuca (Myrtaceae) species grown in Brazil, Flavour Fragr. J., 2007, 22, 6, 474-478, https://doi.org/10.1002/ffj.1823 . [all data]

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Senatore, Rigano, et al., 2003
Senatore, F.; Rigano, D.; de Fusco, R.; Bruno, M., Volatile components of Centaurea cineraria L. subsp. umbrosa (lacaita) Pign. and Centaurea napifolia L. (Asteraceae), two species growing wild in Sicily, Flavour Fragr. J., 2003, 18, 3, 248-251, https://doi.org/10.1002/ffj.1179 . [all data]

Shellie, Marriott, et al., 2003
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Skaltsa, Demetzos, et al., 2003
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Tsiri, Kretsi, et al., 2003
Tsiri, D.; Kretsi, O.; Chinou, I.B.; Spyropoulos, C.G., Composition of fruit volatiles and annual changes in the volatiles of leaves of Eucalyptus camaldulensis Dehn. growing in Greece, Flavour Fragr. J., 2003, 18, 3, 244-247, https://doi.org/10.1002/ffj.1220 . [all data]

Demetzos, Angelopoulou, et al., 2002
Demetzos, C.; Angelopoulou, D.; Perdetzoglou, D., A comparative study of the essential oils of Cistus salviifolius in several populations of Crete (Greece), Biochem. Syst. Ecol., 2002, 30, 7, 651-665, https://doi.org/10.1016/S0305-1978(01)00145-4 . [all data]

Fokialakis, Magiatis, et al., 2002
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References