(E)-β-Famesene


Van Den Dool and Kratz RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20HP-InnowaxRTX-WaxRTX-Wax
Column length (m) 50.50.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.220.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.280.230.230.
Heat rate (K/min) 2.2.3.2.2.
Initial hold (min)      
Final hold (min) 20.20. 35.35.
I 1663.1664.1672.1665.1665.
ReferenceBoti, Koukoua, et al., 2007Duquesnoy, Castola, et al., 2007Kundakovic, Fokialakis, et al., 2007Paolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20RTX-WaxHP-WaxBP-20Supelcowax-10
Column length (m) 50.60.30.50.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.220.220.250.220.2
Phase thickness (μm) 0.250.250.250.250.2
Tstart (C) 60.60.60.60.70.
Tend (C) 220.230.220.220.220.
Heat rate (K/min) 2.2.5.2.3.
Initial hold (min)   10.  
Final hold (min) 20.45. 20.15.
I 1662.1666.1661.1667.1666.
ReferenceBoti, Bighelli, et al., 2006Cavalli, Tomi, et al., 2006Flamini, Tebano, et al., 2006Gonny, Cavaleiro, et al., 2006Pinto, Pina-Vaz, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MBP-20DB-WaxDB-WaxBP-20
Column length (m) 25.50.60.30.50.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.22
Phase thickness (μm) 0.30.250.250.250.25
Tstart (C) 50.60.70.40.60.
Tend (C) 220.220.230.250.220.
Heat rate (K/min) 3.2.2.3.2.
Initial hold (min) 1. 2.  
Final hold (min) 5.20.20.20.20.
I 1668.1664.1674.1661.1661.
ReferenceRubiolo P., Matteodo M., et al., 2006Boti J.B., Koukoua G., et al., 2005Choi, 2005Fanciullino, Gancel, et al., 2005Ferrari, Tomi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxMegawaxSupelcowax-10HP-Wax
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.20.25
Tstart (C) 40.40.40.70.60.
Tend (C) 250.200.220.220.240.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min)   6.  
Final hold (min) 20.20.10.15. 
I 1660.1657.1649.1664.1668.
ReferenceGancel, Ollitrault, et al., 2005Seo and Baek, 2005Verzera, Trozzi, et al., 2005Cavaleiro, Salgueiro, et al., 2004Flamini, Bader, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-WaxBP-20DB-WaxHP-WaxRTX-Wax
Column length (m) 30.50.30.30.60.
Carrier gas N2 HeN2He
Substrate      
Column diameter (mm) 0.250.220.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 220.220.200.220.230.
Heat rate (K/min) 5.2.4.5.2.
Initial hold (min) 10. 5.10. 
Final hold (min)  20.20. 45.
I 1648.1663.1659.1670.1656.
ReferenceFlamini, Luigi Cioni, et al., 2004Gonny, Bradesi, et al., 2004Zheng, Kim, et al., 2004Bader, Caponi, et al., 2003Cavalli, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCP-Wax 52CBHP-InnowaxDB-Wax
Column length (m) 60.60.50.30.60.
Carrier gas N2H2HeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.20.50.25
Tstart (C) 70.40.32.60.70.
Tend (C) 230.245.220.260.230.
Heat rate (K/min) 2.1.51.3.2.
Initial hold (min) 2. 1.  
Final hold (min) 20.20.  20.
I 1674.1660.1650.1668.1664.
ReferenceChoi, 2003Gancel, Ollitrault, et al., 2003Kjeldsen, Christensen, et al., 2003Skaltsa, Demetzos, et al., 2003Choi, Kim. M.-S.L., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20RTX-WaxRTX-WaxBP-20CP-Wax 52CB
Column length (m) 50.30.30.50.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.220.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.2
Tstart (C) 60.45.45.60.32.
Tend (C) 220.250.250.230.220.
Heat rate (K/min) 2.3.3.2.1.
Initial hold (min)  6.6. 1.
Final hold (min) 20.  35. 
I 1654.1653.1668.1661.1650.
ReferenceLota, de Rocca Serra, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002Bianchini, Tomi, et al., 2001Kjeldsen, Christensen, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxSupelcowax-10BP-20BP-20
Column length (m) 60.60.30.50.50.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.50.250.320.220.22
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 40.70.75.60.60.
Tend (C) 290.230.200.230.230.
Heat rate (K/min) 4.2.2.52.2.
Initial hold (min) 2.2.   
Final hold (min) 5.20. 35.35.
I 1667.1673.1668.1654.1654.
ReferenceBartley and Jacobs, 2000Choi and Sawamura, 2000Lazari, Skaltsa, et al., 2000Lota, de Rocca Serra, et al., 2000Lota, Serra, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20Carbowax 20MBP-20BP-20
Column length (m) 50.50.25.50.50.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.220.220.250.220.22
Phase thickness (μm) 0.250.250.30.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 230.220.200.230.230.
Heat rate (K/min) 2.2.3.2.2.
Initial hold (min)   1.  
Final hold (min) 35.20.20.35.35.
I 1654.1658.1676.1658.1660.
ReferenceLota, Serra, et al., 1999Mazzoni, Tomi, et al., 1999Bicchi, Rubiolo, et al., 1998Mariotti, Costa, et al., 1997Mariotti, Tomi, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase HP-20MHP-FFAP
Column length (m) 50.50.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (μm)   
Tstart (C) 60.60.
Tend (C) 190.210.
Heat rate (K/min) 3.3.
Initial hold (min)   
Final hold (min)   
I 1658.1711.
ReferenceChung, Eiserich, et al., 1993Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Boti, Koukoua, et al., 2007
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Duquesnoy, Castola, et al., 2007
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Paolini J., Costa J., et al., 2007
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Boti, Bighelli, et al., 2006
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Flamini, Tebano, et al., 2006
Flamini, G.; Tebano, M.; Cioni, P.L.; Bagci, Y.; Dural, H.; Ertugrul, K.; Uysal, T.; Savran, A., A multivariate statistical approach to Centaurea classification using essential oil composition data of some species from Turkey, Pl. Syst. Evol., 2006, 261, 1-4, 217-228, https://doi.org/10.1007/s00606-006-0448-3 . [all data]

Gonny, Cavaleiro, et al., 2006
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Pinto, Pina-Vaz, et al., 2006
Pinto, E.; Pina-Vaz, C.; Salgueiro, L.; Goncalves, M.J.; Costa-de-Oliveira, S.; Cavaleiro, C.; Palmeira, A.; Rodrigues, A.; Martinez-de-Oliveira, J., Antifuncal activity of the essential oil Thymus pulegioides on Candida, Aspergillus and dermatophyte species, Journal of Medical Microbiology, 2006, 55, 10, 1367-1373, https://doi.org/10.1099/jmm.0.46443-0 . [all data]

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Choi, 2005
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Fanciullino, A.-L.; Gancel, A.-L.; Froelicher, Y.; Luro, F.; Ollitrault, P.; Brillouet, J.-M., Effects of Nucleo-cytoplasmic Interactions on Leaf Volatile Compounds from Citrus Somatic Diploid Hybrids, J. Agric. Food Chem., 2005, 53, 11, 4517-4523, https://doi.org/10.1021/jf0502855 . [all data]

Ferrari, Tomi, et al., 2005
Ferrari, B.; Tomi, F.; Casanova, J., Composition and chemical variability of Ferula communis essential oil from Corsica, Flavour Fragr. J., 2005, 20, 2, 180-185, https://doi.org/10.1002/ffj.1405 . [all data]

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Gancel, A.-L.; Ollitrault, P.; Froelicher, Y.; Tomi, F.; Jacquemond, C.; Luro, F.; Brillouet, J.-M., Leaf volatile compounds of six citrus somatic allotetraploid hybrids originating from various combinations of lime, lemon, citron, sweet orange, and grapefruit, J. Agric. Food Chem., 2005, 53, 6, 2224-2230, https://doi.org/10.1021/jf048315b . [all data]

Seo and Baek, 2005
Seo, W.H.; Baek, H.H., Identification of characteristic aroma-active compounds from water dropword (Oenanthe javanica DC.), J. Agric. Food Chem., 2005, 53, 17, 6766-6770, https://doi.org/10.1021/jf050150z . [all data]

Verzera, Trozzi, et al., 2005
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Cavaleiro, Salgueiro, et al., 2004
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Flamini, Bader, et al., 2004
Flamini, G.; Bader, A.; Cioni, P.L.; Katbeh-Bader, A.; Morelli, I., Composition of the essential oil of leaves, galls, and ripe and unripe fruits of Jordian Pistacia palaestina Boiss., J. Agric. Food Chem., 2004, 52, 3, 572-576, https://doi.org/10.1021/jf034773t . [all data]

Flamini, Luigi Cioni, et al., 2004
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Gonny, Bradesi, et al., 2004
Gonny, M.; Bradesi, P.; Casanova, J., Identification of the components of the essential oil from wild Corsican Daucus carota L. using 13C-NMR spectroscopy, Flavour Fragr. J., 2004, 19, 5, 424-433, https://doi.org/10.1002/ffj.1330 . [all data]

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Cavalli, Tomi, et al., 2003
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Choi, 2003
Choi, H.-S., Character impact odorants of Citrus Hallabong [(C. unshiu Marcov × C. sinensis Osbeck) × C. reticulata Blanco] cold-pressed peel oil, J. Agric. Food Chem., 2003, 51, 9, 2687-2692, https://doi.org/10.1021/jf021069o . [all data]

Gancel, Ollitrault, et al., 2003
Gancel, A.-L.; Ollitrault, P.; Froelicher, Y.; Tomi, F.; Jacquemond, C.; Luro, F.; Brillouet, J.-M., Leaf volatile compounds of seven citrus somatic tetraploid hybrids sharing willow leaf mandarin (Citrus deliciosa Ten.) as their common parent, J. Agric. Food Chem., 2003, 51, 20, 6006-6013, https://doi.org/10.1021/jf0345090 . [all data]

Kjeldsen, Christensen, et al., 2003
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Skaltsa, Demetzos, et al., 2003
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Choi, Kim. M.-S.L., et al., 2002
Choi, H.-S.; Kim. M.-S.L.; Sawamura, M., Constituents of the essential oil of cnidium officinale Makino, a Korean medicinal plant, Flavour Fragr. J., 2002, 17, 1, 49-53, https://doi.org/10.1002/ffj.1038 . [all data]

Lota, de Rocca Serra, et al., 2002
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Jacquemond, C.; Casanova, J., Volatile components of peel and leaf oils of lemon and lime species, J. Agric. Food Chem., 2002, 50, 4, 796-805, https://doi.org/10.1021/jf010924l . [all data]

Shellie, Mondello, et al., 2002
Shellie, R.; Mondello, L.; Marriott, P.; Dugo, G., Characterisation of lavender essential oils by using gas chromatography-mass spectrometry with correlation of linear retention indices and comparison with comprehensive two-dimensional gas chromatography, J. Chromatogr. A, 2002, 970, 1-2, 225-234, https://doi.org/10.1016/S0021-9673(02)00653-2 . [all data]

Bianchini, Tomi, et al., 2001
Bianchini, A.; Tomi, P.; Costa, J.; Bernardini, A.F., Composition of Helichrysum italicum (Roth) G. Don fil. subsp. italicum essential oils from Corsica (France), Flavour Fragr. J., 2001, 16, 1, 30-34, https://doi.org/10.1002/1099-1026(200101/02)16:1<30::AID-FFJ941>3.0.CO;2-F . [all data]

Kjeldsen, Christensen, et al., 2001
Kjeldsen, F.; Christensen, L.P.; Edelenbos, M., Quantitative analysis of aroma compounds in carrot (Daucus carota L.) cultivars by capillary gas chromatography using large-volume injection technique, J. Agric. Food Chem., 2001, 49, 9, 4342-4348, https://doi.org/10.1021/jf010213n . [all data]

Bartley and Jacobs, 2000
Bartley, J.P.; Jacobs, A.L., Effects of drying on flavour compounds in Australian-grown ginger (Zingiber officinale), J. Sci. Food Agric., 2000, 80, 2, 209-215, https://doi.org/10.1002/(SICI)1097-0010(20000115)80:2<209::AID-JSFA516>3.0.CO;2-8 . [all data]

Choi and Sawamura, 2000
Choi, H.-S.; Sawamura, M., Composition of the essential oil of Citrus tamurana Hort. ex Tanaka (Hyuganatsu), J. Agric. Food Chem., 2000, 48, 10, 4868-4873, https://doi.org/10.1021/jf000651e . [all data]

Lazari, Skaltsa, et al., 2000
Lazari, D.M.; Skaltsa, H.D.; Constantinidis, T., Volatile constituents of Cerastium candidissimum, a Greek endemic species, Flavour Fragr. J., 2000, 15, 3, 174-176, https://doi.org/10.1002/1099-1026(200005/06)15:3<174::AID-FFJ886>3.0.CO;2-Y . [all data]

Lota, de Rocca Serra, et al., 2000
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of mandarins from Citrus reticulata Blanco, Biochem. Syst. Ecol., 2000, 28, 1, 61-78, https://doi.org/10.1016/S0305-1978(99)00036-8 . [all data]

Lota, Serra, et al., 1999
Lota, M.-L.; Serra, D.R.; Tomi, F.; Bessiere, J.-M.; Casanova, J., Chemical composition of peel and leaf essential oils of Citrus medica L. and C. limonimedica Lush., Flavour Fragr. J., 1999, 14, 3, 161-166, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<161::AID-FFJ801>3.0.CO;2-8 . [all data]

Mazzoni, Tomi, et al., 1999
Mazzoni, V.; Tomi, F.; Casanova, J., A daucane-type sesquiterpene from Faucus carota seed oil, Flavour Fragr. J., 1999, 14, 5, 268-272, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<268::AID-FFJ823>3.0.CO;2-Z . [all data]

Bicchi, Rubiolo, et al., 1998
Bicchi, C.; Rubiolo, P.; Marschall, H.; Weyerstahl, P.; Laurent, R., Constituents of Artemisia roxburghiana Besser essential oil, Flavour Fragr. J., 1998, 13, 1, 40-46, https://doi.org/10.1002/(SICI)1099-1026(199801/02)13:1<40::AID-FFJ688>3.0.CO;2-Z . [all data]

Mariotti, Costa, et al., 1997
Mariotti, J.P.; Costa, J.; Bianchini, A.; Bernardini, A.F.; Casanova, J., Composition and variability of the essential oil of Stachys glutinosa L. from Corsica (France), Flavour Fragr. J., 1997, 12, 3, 205-209, https://doi.org/10.1002/(SICI)1099-1026(199705)12:3<205::AID-FFJ636>3.0.CO;2-I . [all data]

Mariotti, Tomi, et al., 1997
Mariotti, J.P.; Tomi, F.; Casanova, J.; Costa, J.; Bernardini, A.F., Composition of the essential oil of Cistus Iadaniferus L. cultivated in corsica (France), Flavour Fragr. J., 1997, 12, 3, 147-151, https://doi.org/10.1002/(SICI)1099-1026(199705)12:3<147::AID-FFJ631>3.0.CO;2-Q . [all data]

Chung, Eiserich, et al., 1993
Chung, T.Y.; Eiserich, J.P.; Shibamoto, T., Volatile compounds isolated from edible Korean chamchwi (Aster scaber Thunb), J. Agric. Food Chem., 1993, 41, 10, 1693-1697, https://doi.org/10.1021/jf00034a033 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References