(E)-β-Famesene


Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsCP-Sil 5 CBDB-5HP-5 MS
Column length (m)   50.60.30.
Carrier gas   NitrogenHeliumHelium
Substrate      
Column diameter (mm)   0.320.250.25
Phase thickness (μm)   1.201.000.25
Program not specifiednot specified36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0C (30 min)40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)70 0C (2 min) 10 0C/min -> 150 0C (15 min) 5 0C/min -> 240 0C
I 1455.1455.1486.1460.1415.
ReferenceRobinson, Adams, et al., 2012Robinson, Adams, et al., 2012Gros, Nizet, et al., 2011Miyazaki, Plotto, et al., 2011Bagci, Yazgin, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSZB-1 MSDB-5HP-5HP-5
Column length (m) 30.30.30.25.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.170.17
Program 60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)50 0C 3 0C/min -> 150 0C (10 min) 10 0C/min -> 250 0C50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)not specified
I 1438.1440.1461.1454.1456.
ReferenceLiu, Chu, et al., 2010Bajpai, Al-Reza, et al., 2009Courtois, Paine, et al., 2009Custer, 2009Custer, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5MSElite-5 MSDB-1DB-1HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHydrogenHydrogen 
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm) 0.250.250.250.25 
Program 40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1456.1446.1455.1455.1457.
ReferenceHEuskin, Godin, et al., 2009Kapoor, Singh, et al., 2009Mendes, Trindade, et al., 2009Mendes, Trindade, et al., 2009, 2Riahi, Pourbasheer, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5CB-1CB-1CP Sil 8 CB
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 250 0C (3 min)40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)not specified60C => 2.5C/min => 170C => 10C/min => 250C (5min)
I 1457.1456.1467.1446.1458.
ReferenceZellner, Amorim, et al., 2009Judzentiene and Budiene, 2008Kannaste, Vongvanich, et al., 2008Kannaste, Vongvanich, et al., 2008Kristiawan, Sobolik, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSDB-1CP-Sil 8CB-MSHP-1HP-5MS
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Program not specified45C => 3C/min => 175C => 15C/min => 300C (10min)50 0C(3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 260 0C40C(2min) => 2C/min => 200C => 15C/min => 250C (30min)40C(10min) => 3C/min => 200C => 2C/min => 220C
I 1450.1455.1454.1439.1460.
ReferenceLo Presti, Sciarrone, et al., 2008Nogueira, Marcelo-Curto, et al., 2008Profitt, Schatz, et al., 2008Barra, Baldovini, et al., 2007Cole, Haber, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSDB-5 MSDB-1HP-5
Column length (m) 30.30.30.30. 
Carrier gas HeHeliumHeliumH2 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.250.250.250.25 
Program 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C40 0C (5 min) 2 0C/min -> 250 0C (15 min) 10 0C/min -> 270 0C60 0C 3 0C/min -> 210 0C 5 0C/min -> 250 0C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1452.1452.1480.1455.1462.
ReferenceFormisano, Mignola, et al., 2007Formisano, Rigano, et al., 2007Haznagy-Radnai, Szigle, et al., 2007Kamatou, Viljoen, et al., 2007Liolios, Laouer, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5MSCP-SilCP-SilCP-Sil
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C40C(10min) => 3C/min => 200C => 2C/min => 220C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
I 1452.1461.1452.1454.1435.
ReferenceMeekijjaroenroj, Bessière, et al., 2007Moronkola, Ogunwande, et al., 2007Proffit, 2007Proffit, 2007Proffit, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-SilCP Sil 8 CBHP-5DB-1HP-5 MS
Column length (m) 30.50.30.30. 
Carrier gas HeliumHeliumHeliumHe 
Substrate      
Column diameter (mm) 0.250.320.250.25 
Phase thickness (μm) 0.250.250.250.25 
Program 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)not specified45C => 3C/min => 175C => 15C/min => 300C(10min)not specified
I 1454.1454.1457.1456.1460.
ReferenceProffit, 2007Radusiene, Judzentiene, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Rodrigues, Antunes, et al., 2007Stokes, Cole, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-5CP Sil 8 CBHP-5HP-5 MS
Column length (m) 30.60.50.30.30.
Carrier gas HeHeHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm)  1.0.250.250.25
Program 40C(10min) => 3C/min => 200C => 2C/min => 220C60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C (40min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)not specified40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
I 1462.1453.1457.1460.1458.
ReferenceTakaku, Haber, et al., 2007Chemat, Lucchesi, et al., 2006Judzentiene and Buzelyte, 2006Kucuk, Gulec, et al., 2006Schmidt, Noletto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5SE-52CP Sil 8 CBBP-5
Column length (m) 30.30.30.50.25.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (μm) 0.250.250.150.250.50
Program 60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C45C => 1C/min => 100C => 5C/min => 250C (10min)50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)
I 1457.1444.1457.1457.1452.
ReferenceSingh, Marimuthu, et al., 2006Srivastava, Mallavarapu, et al., 2006Tognolini, Barocelli, et al., 2006Butkienë, Nivinskienë, et al., 2005Eyres, Dufour, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5BP-5HP-5MSHP-5HP-5
Column length (m) 25.25.30.30.30.
Carrier gas HeliumHelium  He
Substrate      
Column diameter (mm) 0.320.320.250.320.25
Phase thickness (μm) 0.500.500.25 0.25
Program 60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)40C(5min) => 3C/min => 90C => 10C/min => 280C65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min)60C(5min) => 3C/min => 120C (2min) => 2C/min => 200C (2min) => 3C/min => 320C
I 1456.1462.1459.1460.1469.
ReferenceEyres, Dufour, et al., 2005Eyres, Dufour, et al., 2005Novak, Draxler, et al., 2005Singh, Maurya, et al., 2005Yasar, Üçüncü, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5MSHP-5MSBPX-5HP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeH2 
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)40C (2min) => 10C/min => 200C => 15C/min => 250C (5min)40C (2min) => 10C/min => 200C => 15C/min => 250C (5min)50 0C (1 min) 3 0C/min -> 150 0C 5 0C/min -> 250 0C (5 min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C
I 1457.1461.1461.1457.1452.
ReferenceButkienë, Nivinskienë, et al., 2004Demyttenaere, Moriña, et al., 2004Demyttenaere, Moriña, et al., 2004Koba, Sanda, et al., 2004Senatore, Apostolides Arnold, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSE-30SE-54HP-5DB-1
Column length (m) 30.  30.30.
Carrier gas    HeH2
Substrate      
Column diameter (mm) 0.25  0.250.25
Phase thickness (μm) 0.25  0.250.25
Program 60C(1min) => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)not specifiednot specified50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)
I 1469.1482.1443.1450.1456.
ReferenceSingh, Marimuthu, et al., 2004Vinogradov, 2004Kilic, 2002Usubillaga, Aparicio, et al., 2001da Silva, Pedro, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1CP Sil 5 CBDB-1CP Sil 5 CB
Column length (m) 30.30.25.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.390.25 
Phase thickness (μm) 0.250.25 0.25 
Program not specified45C => 3C/min => 170C => 15C/min => 300C(10min)not specified45C => 3C/min => 175C => 15C/min => 240C (10min)not specified
I 1462.1456.1453.1456.1482.
ReferenceBouwmeester, Wallaart, et al., 1999Pedro, da Silva, et al., 1999Weyerstahl, Marschall, et al., 1999Baratta, Dorman, et al., 1998Phan, Van, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1CP Sil 5 CBMethyl SiliconeDB-5
Column length (m) 25.30.25. 30.
Carrier gas N2H2N2  
Substrate      
Column diameter (mm)  0.25  0.32
Phase thickness (μm) 0.390.25  1.
Program not specified45C => 3C/min => 175C => 15C/min => 240C(10min)not specifiednot specified0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)
I 1445.1456.1446.1482.1453.
ReferenceWeyerstahl, Marschall, et al., 1998Figueiredo, Barroso, et al., 1997Weyerstahl, Marschall, et al., 1997Zenkevich, 1996Storer, Elmore, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-5DB-5
Column length (m) 30.30.
Carrier gas   
Substrate   
Column diameter (mm) 0.320.32
Phase thickness (μm) 1.1.
Program 0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)
I 1455.1456.
ReferenceStorer, Elmore, et al., 1993Storer, Elmore, et al., 1993
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Robinson, Adams, et al., 2012
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Miyazaki, T.; Plotto, A.; Goodner, K.; Gmitter F.G., Distribution of aroma volatile compounds in tangerine hybrids and proposed inheritance, J. Sci. Food Agric., 2011, 91, 3, 449-460, https://doi.org/10.1002/jsfa.4205 . [all data]

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Bagci, E.; Yazgin, A.; Hayta, S.; Cakilcioglu, U., Composition of the essential oil of Teucrium chamaedrys L. (Lamiaceae) from Turkey, J. Med. Plants Res., 2010, 4, 23, 2588-2590. [all data]

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Liu, Z.L.; Chu, S.S.; Liu, Q.R., Chemical composition and insecticidial activity against Sitophilus zeamais of the essential oils of Artemisia capillaris and Artemisia mongolica, Molecules, 2010, 15, 4, 2600-2608, https://doi.org/10.3390/molecules15042600 . [all data]

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HEuskin, S.; Godin, B.; Leroy, P.; Quentin C.; Wathelet, J.-P.; Verheggen, F.; Haubruge, E.; Lognay, G., Fast gas chromatography characterization of purified semiochemicals from essential oils of Matricaria chamomilla L. (Asteraceae) and Nepeta cataria L. (Lamiaceae), J. Chromatorg. A., 2009, 1216, 14, 2768-2775, https://doi.org/10.1016/j.chroma.2008.09.109 . [all data]

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Mendes, M.D.; Trindade, H.; Figueiredo, A.C.; Pedro, L.G.; Barroso, J.G., Chaerophyllum azoricun Trel. grown in the Azores archipelago, Portugal: evaluation of the genetic diversity using molecular markers and comparison with volatile oils profiles, Flavour Fragr. J., 2009, 24, 5, 259-265, https://doi.org/10.1002/ffj.1939 . [all data]

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Formisano, Rigano, et al., 2007
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Haznagy-Radnai, Szigle, et al., 2007
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Kamatou, Viljoen, et al., 2007
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Notes

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