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cis-Verbenol


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSBPX-5OV-1HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHeliumHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)40 0C (5 min) 2 0C/min -> 250 0C (15 min) 10 0C/min -> 270 0C50C => 3C/min => 150C(10min) => 10C/min => 250C40 0C (2 min) 6 0C/min -> 130 0C 10 0C/min -> 300 0C60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
I 1110.1145.1145.1144.1188.
ReferenceMendes, Trindade, et al., 2009Formisano, Rigano, et al., 2007Ozer H., Sokmen M., et al., 2007Suschke, Sporer, et al., 2007Jordan, Martinez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5BPX-5CP Sil 8 CB
Column length (m) 30.30.30.30.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.50.25
Program not specified40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C40C(1min) => 9C/min => 130C => 2C/min => 230C60C(1min) => 3.5C/min => 180C => 20C/min => 280C(2min)60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)
I 1188.1144.1131.1100.1141.
ReferenceMartinez, Madrid, et al., 2006Senatore, Apostolides Arnold, et al., 2006Hamm, Bleton, et al., 2005Koutsoudaki, Krsek, et al., 2005Nivinskienë, Butkienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program 40C(1min) => 9C/min => 130C => 2C/min => 230C60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C40C (1min) => 9C/min => 130C => 2C/min => 230Cnot specified45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)
I 1131.1188.1131.1139.1110.
ReferenceHamm, Bleton, et al., 2004Sotomayor, Martínez, et al., 2004Hamm, Lesellier, et al., 2003Aparicio, Romero, et al., 2001Figueiredo, Miguel, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase DB-1DB-1Polydimethyl siloxanesDB-1OV-101
Column length (m) 30.30. 30.2.5
Carrier gas HeHe H2N2
Substrate     Chromosorb G 60-80mesh DMCS
Column diameter (mm) 0.250.25 0.25 
Phase thickness (mum) 0.250.25 0.25 
Program 45C => 3C/min => 175C => 15C/min => 240C (10min)45C => 3C/min => 175C => 15C/min => 280Cnot specified45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min)not specified
I 1110.1110.1135.1110.1165.
ReferenceBaratta, Dorman, et al., 1998Gaspar, Palma, et al., 1997Zenkevich, 1997Barroso, Figueiredo, et al., 1996Swigar and Silverstein, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mendes, Trindade, et al., 2009
Mendes, M.D.; Trindade, H.; Figueiredo, A.C.; Pedro, L.G.; Barroso, J.G., Chaerophyllum azoricun Trel. grown in the Azores archipelago, Portugal: evaluation of the genetic diversity using molecular markers and comparison with volatile oils profiles, Flavour Fragr. J., 2009, 24, 5, 259-265, https://doi.org/10.1002/ffj.1939 . [all data]

Formisano, Rigano, et al., 2007
Formisano, C.; Rigano, D.; Napolitano, F.; Senatore, F.; Arnold, N.A.; Piozzi, F.; Rosselli, S., Volatile constituents of Calamintha ariganifolia Boiss. growing wild in Lebanon, Natural Product Communications, 2007, 2, 12, 1253-1256. [all data]

Ozer H., Sokmen M., et al., 2007
Ozer H.; Sokmen M.; Gulluce M.; Adiguzel A.; Sahin F.; Sokmen A.; Kilic H.; Baris O., Chemical Composition and Antimicrobial and Antioxidant Activities of the Essential Oil and Methanol Extract of Hippomarathrum microcarpum (Bieb.) from Turkey, J. Agric. Food Chem., 2007, 55, 3, 937-942, https://doi.org/10.1021/jf0624244 . [all data]

Suschke, Sporer, et al., 2007
Suschke, U.; Sporer, F.; Schneele, J.; Geiss, H.K.; Reichling, J., Antibacterial and Cytotoxic activity of Nepeta cataria L., Nepeta cataria var. citriodora (Beck.) Balb. and Melissa officinalis L. essential oils, Natural Product Communications, 2007, 2, 12, 1277-1286. [all data]

Jordan, Martinez, et al., 2006
Jordan, M.J.; Martinez, R.M.; Goodner, K.L.; Baldwin, E.A.; Sotomayor, J.A., Seasonal variation of Thymus hyemalis Lange and Spanish Thymus vulgaris L. essential oils composition, Ind. Crops Prod., 2006, 24, 3, 253-263, https://doi.org/10.1016/j.indcrop.2006.06.011 . [all data]

Martinez, Madrid, et al., 2006
Martinez, S.; Madrid, J.; Hernández, F.; Megias, M.D.; Sotomayor, J.A.; Jordan, M.J., Effect of thyme essential oils (Thymus hyemalis and Thymus zygis) and Monensin on in Vitro Ruminal degradation and volatile fatty acid production, J. Agric. Food Chem., 2006, 54, 18, 6598-6602, https://doi.org/10.1021/jf060985p . [all data]

Senatore, Apostolides Arnold, et al., 2006
Senatore, F.; Apostolides Arnold, N.; Piozzi, F.; Formisano, C., Chemical composition of the essential oil of Salvia microstegia Boiss. et Balansa growing wild in Lebanon, J. Chromatogr. A, 2006, 1108, 2, 276-278, https://doi.org/10.1016/j.chroma.2006.01.066 . [all data]

Hamm, Bleton, et al., 2005
Hamm, S.; Bleton, J.; Connan, J.; Tchapla, A., A chemical investigation by headspace SPME and GC-MS of volatile and semi-volatile terpenes in various olibanum samples, Phytochemistry, 2005, 66, 12, 1499-1514, https://doi.org/10.1016/j.phytochem.2005.04.025 . [all data]

Koutsoudaki, Krsek, et al., 2005
Koutsoudaki, C.; Krsek, M.; Rodger, A., Chemical composition and antibacterial activity of the essential oil and the gum of pistacia lentiscus Var. chia, J. Agric. Food Chem., 2005, 53, 20, 7681-7685, https://doi.org/10.1021/jf050639s . [all data]

Nivinskienë, Butkienë, et al., 2005
Nivinskienë, O.; Butkienë, R.; Mockutë, D., Chemical composition of seed (fruit) essential oils of Angelica archangelica L. growing wild in Lithuania, Chemija, 2005, 16, 3-4, 51-54. [all data]

Hamm, Bleton, et al., 2004
Hamm, S.; Bleton, J.; Tchapla, A., Headspace solid phase microextraction for screening for the presence of resins in Egyptian archaeological samples, J. Sep. Sci., 2004, 27, 3, 235-243, https://doi.org/10.1002/jssc.200301611 . [all data]

Sotomayor, Martínez, et al., 2004
Sotomayor, J.A.; Martínez, R.M.; García, A.J.; Jordán, M.J., Thymus zygis Subsp. Gracilis: watering level effect on phytomass production and essential oil quality, J. Agric. Food Chem., 2004, 52, 17, 5418-5424, https://doi.org/10.1021/jf0496245 . [all data]

Hamm, Lesellier, et al., 2003
Hamm, S.; Lesellier, E.; Bleton, J.; Tchapla, A., Optimization of headspace solid phase microextraction for gas chromatography/mass spectrometry analysis of widely different volatility and polarity terpenoids in olibanum, J. Chromatogr. A, 2003, 1018, 1, 73-83, https://doi.org/10.1016/j.chroma.2003.08.027 . [all data]

Aparicio, Romero, et al., 2001
Aparicio, R.; Romero, M.; Rojas, L.B.; Khouri, N.; Usubillaga, A., Composition of the essential oil of four species of Ruilopezia from the Venezuelan Andes, Flavour Fragr. J., 2001, 16, 3, 172-174, https://doi.org/10.1002/ffj.973 . [all data]

Figueiredo, Miguel, et al., 2001
Figueiredo, A.C.; Miguel, M.G.; Duarte, A.M.F.; Barroso, J.G.; Pedro, L.G., Essential oil composition of Thymus lotocephallus G. López R. Morales, collected during flowering and vegetative phases, Flavour Fragr. J., 2001, 16, 6, 417-421, https://doi.org/10.1002/ffj.1028 . [all data]

Baratta, Dorman, et al., 1998
Baratta, M.T.; Dorman, H.J.; Deans, S.G.; Figueiredo, A.C.; Barroso, J.G.; Ruberto, G., Antimicrobial and antioxidant properties of some commercial essential oils, Flavour Fragr. J., 1998, 13, 4, 235-244, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<235::AID-FFJ733>3.0.CO;2-T . [all data]

Gaspar, Palma, et al., 1997
Gaspar, H.; Palma, F.M.S.B.; de la Torre, M.C.; Rodríguez, B.; Barroso, J.G.; Figueiredo, A.C., Composition of the essential oil of Teucrium haenseleri Boiss., Flavour Fragr. J., 1997, 12, 5, 355-357, https://doi.org/10.1002/(SICI)1099-1026(199709/10)12:5<355::AID-FFJ656>3.0.CO;2-B . [all data]

Zenkevich, 1997
Zenkevich, I.G., Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons, Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]

Barroso, Figueiredo, et al., 1996
Barroso, J.G.; Figueiredo, A.C.; Pedro, L.G.; Antunes, T.; Sevinate-Pinto, I.; Fontinha, S.S.; Scheffer, J.J.C., Composition of the essential oil of teucrium heterophyllum L'Her. Grown on Madiera, Flavour Fragr. J., 1996, 11, 2, 129-132, https://doi.org/10.1002/(SICI)1099-1026(199603)11:2<129::AID-FFJ550>3.0.CO;2-Z . [all data]

Swigar and Silverstein, 1981
Swigar, A.A.; Silverstein, R.M., Monoterpenes, Aldrich Chemical Company, Milwaukee, WI, USA, 1981, 130. [all data]


Notes

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