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cis-Verbenol


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneHP-5HP-5 MSHP-5 MSSPB-1
Column length (m) 60.30.30.30.30.
Carrier gas HeliumN2HeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 90.60.50.50.70.
Tend (C) 225.220.240.230.220.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min)  10. 10. 
Final hold (min) 3.  10.15.
I 1142.1144.1129.1141.1118.
ReferenceRetta, Gattuso, et al., 2009Flamini, Tebano, et al., 2008Sarikurkcu, Tepe, et al., 2008Adams, Beauchamp, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-1HP-5MSHP-5MSRTX-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.200.250.250.32
Phase thickness (mum) 0.250.200.250.250.25
Tstart (C) 50.70.50.50.60.
Tend (C) 240.220.250.280.300.
Heat rate (K/min) 4.3.2.5.4.
Initial hold (min)    4. 
Final hold (min)  15. 10. 
I 1140.1122.1140.1152.1130.
ReferenceSefidkon, Abbasi, et al., 2007Cavaleiro, Pinto, et al., 2006Farah, Afifi, et al., 2006Kim, Abd El-Aty, et al., 2006Kula, Izydorczyk, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5NB-30HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.520.250.250.25
Tstart (C) 50.50.60.50.40.
Tend (C) 280.280.220.250.260.
Heat rate (K/min) 5.5.4.2.4.
Initial hold (min)   5.  
Final hold (min) 5.5.   
I 1128.1128.1143.1132.1143.
ReferenceMarzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Orav, Raal, et al., 2006Petrovic, Ristic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-1DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.60.50.35.40.
Tend (C) 280.280.265.280.250.
Heat rate (K/min) 4.3.2.54.5.
Initial hold (min) 4. 1.2.0.5
Final hold (min)   30. 2.
I 1141.1105.1118.1142.1140.
ReferencePino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Kowalski and Wolski, 2005Özel, Gögüs, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1DB-1DB-1HP-5
Column length (m) 30.60.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 280.250.265.250.260.
Heat rate (K/min) 4.5.2.55.5.
Initial hold (min)   1. 2.
Final hold (min)  10.20.10.13.
I 1140.1111.1120.1106.1135.
ReferenceSajjadi S.E. and Eskandari B., 2005Salehi, Sonboli, et al., 2005Sarkhail, Amin, et al., 2005Sonboli, Salehi, et al., 2005Yayli, Yasar, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5RTX-1NB-30RSL-200DB-1
Column length (m) 60.30.50.30.60.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.250.250.200.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.40.40.
Tend (C) 260.300.250.280.260.
Heat rate (K/min) 6.4.2.6.4.
Initial hold (min) 4.6  5.5.
Final hold (min) 1.  5. 
I 1146.1130.1132.1165.1123.
ReferenceJürgens and Dötterl, 2004Kalemba and Thiem, 2004Raal, Paaver, et al., 2004Jirovetz, Buchbauer, et al., 2003Sefidkon, Naderi Nik, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5SPB-5DB-1DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.320.250.250.250.25
Tstart (C) 60.60.50.40.60.
Tend (C) 250.275.240.280.240.
Heat rate (K/min) 5.4.5.4.3.
Initial hold (min) 30. 3.5. 
Final hold (min)   10.  
I 1146.1138.1117.1126.1143.
ReferenceYassa, Akhani, et al., 2003Ghannadi, Sajjadi, et al., 2002Kim and Lee, 2002Sefidkon, Jalili, et al., 2002Zoghbi, Andrade, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1RTX-1PONA
Column length (m) 30.30.30.50.
Carrier gas N2N2N2He
Substrate     
Column diameter (mm) 0.250.250.250.2
Phase thickness (mum) 0.250.250.250.5
Tstart (C) 60.60.60.40.
Tend (C) 220.300.300.250.
Heat rate (K/min) 5.4.4.6.
Initial hold (min) 10.  5.
Final hold (min)     
I 1141.1130.1129.1140.
ReferenceGallori, Flamini, et al., 2001Kalemba, Marschall, et al., 2001Kalemba, 1999Ramalho, de Freitas, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Retta, Gattuso, et al., 2009
Retta, D.; Gattuso, M.; Gattuso, S.; Lira, P. Di Leo; van Baren, C.; Ferraro, G.; Bandoni A., Essential oil composition of Achyrocline flaccida (Weinm.) DC. (Asteraceae) from different locations of Argentina, Biochem. Systematics Ecol., 2009, 36, 12, 877-881, https://doi.org/10.1016/j.bse.2008.11.001 . [all data]

Flamini, Tebano, et al., 2008
Flamini, G.; Tebano, M.; Cioni, P.L., Composition of the essential oils from leafy parts of the shoots, flowers and fruits of Eryngium amethystinum from Amiata Mount (Tuscany, Italy), Food Chem., 2008, 107, 2, 671-674, https://doi.org/10.1016/j.foodchem.2007.08.064 . [all data]

Sarikurkcu, Tepe, et al., 2008
Sarikurkcu, C.; Tepe, B.; Daferera, D.; Polissiou, M.; Harmandar, M., Studies on the anioxidant activity of the essential oil and methanol extract of Marrubium globosum subsp. globosum (lamiaceae) by three different chemical assays, Bioresource Technol., 2008, 99, 10, 4239-4246, https://doi.org/10.1016/j.biortech.2007.08.058 . [all data]

Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Pinto, Salgueiro, et al., 2007
Pinto, E.; Salgueiro, L.R.; Cavaleiro, C.; Palmeira, A.; Goncalves, M.J., In vitro susceptibility of some species of yeasts and filamentous fungi to essential oils of Salvia of?cinalis, Ind. Crops Prod., 2007, 26, 2, 135-141, https://doi.org/10.1016/j.indcrop.2007.02.004 . [all data]

Sefidkon, Abbasi, et al., 2007
Sefidkon, F.; Abbasi, K.; Jamzad, Z.; Ahmadi, S., The effect of distillation methods and stage of plant growth on the essential oil content and composition of Satureja rechingeri Jamzad, Food Chem., 2007, 100, 3, 1054-1058, https://doi.org/10.1016/j.foodchem.2005.11.016 . [all data]

Cavaleiro, Pinto, et al., 2006
Cavaleiro, C.; Pinto, E.; Gonsales, M.J.; Salguero, L., Antifungal activity of Juniperus essential oils agains dermatophyte, Asrgillus and Candida strains, J. Appl. Microbiol., 2006, 100, 6, 1333-1338, https://doi.org/10.1111/j.1365-2672.2006.02862.x . [all data]

Farah, Afifi, et al., 2006
Farah, A.; Afifi, A.; Fechtal, M.; Chhen, A.; Satrani, B.; Talbi, M.; Chaouch, A., Fractional distillation effect on the chemical composition of Moroccan myrtle (Myrtus communis L.) essential oils, Flavour Fragr. J., 2006, 21, 2, 351-354, https://doi.org/10.1002/ffj.1651 . [all data]

Kim, Abd El-Aty, et al., 2006
Kim, M.R.; Abd El-Aty, A.M.; Kim, I.S.; Shim, J.H., Determination of volatile flavor components in danggui cultivars by solvent free injection and hydrodistillation followed by gas chromatographic-mass spectrometric analysis, J. Chromatogr. A, 2006, 1116, 1-2, 259-264, https://doi.org/10.1016/j.chroma.2006.03.060 . [all data]

Kula, Izydorczyk, et al., 2006
Kula, J.; Izydorczyk, K.; Czajkowska, A.; Bonikowski, R., Chemical composition of carrot umbel oils from Daucus carota L. ssp. sativus cultivated in Poland, Flavour Fragr. J., 2006, 21, 4, 667-669, https://doi.org/10.1002/ffj.1646 . [all data]

Marzouk, Mansour, et al., 2006
Marzouk, Z.; Mansour, H.B.; Chraief, I.; Mosrati, R.; Cheriaa, J.; Neffati, A.; Marzouk, B.; Sfari, M.; Boukef, K.; Barillies, D.; Ghedira, L.C., Chemical composition, antibacterial and antimutagenic activities of four populations of Rosmarinus officinalis L. oils from Tunisia, J. Food Agriculture Environment, 2006, 4, 2, 89-94. [all data]

Marzouk, Neffati, et al., 2006
Marzouk, Z.; Neffati, A.; Marzouk, B.; Chraief, I.; Fathia, K.; Ghedira, L.C.; Boukef, K., Chemical composition and antibacterial and antimutagenic activity of Tunisian Rosmarinus officinalis L. oil from Kasrine, Journal of Food, Agriculture Environment, 2006, 4, 34, 61-65. [all data]

Morteza-Semnani K., Saeedi M., et al., 2006
Morteza-Semnani K.; Saeedi M.; Changizi S., The essential oil composition of Hypericum scabrum L. from Iran, Flavour Fragr. J., 2006, 21, 3, 513-515, https://doi.org/10.1002/ffj.1614 . [all data]

Orav, Raal, et al., 2006
Orav, A.; Raal, A.; Arak, E.; Müürisepp, M.; Kailas, T., Composition of the essential oil of Artemisia absinthium L. of different geographical origin, Proc. Est. Acad. Sci. Chem., 2006, 55, 3, 155-165. [all data]

Petrovic, Ristic, et al., 2006
Petrovic, S.; Ristic, M.; Milenkovic, M.; Kukic, J.; Antic-Stankovic, J.; Niketic, M., Composition and antimicrobial activity of essential oil of Stachys plumosa Griseb., Flavour Fragr. J., 2006, 21, 2, 250-252, https://doi.org/10.1002/ffj.1570 . [all data]

Pino, Marbot, et al., 2006
Pino, J.A.; Marbot, R.; Payo, A.; Chao, D.; Herrera, P., Aromatic Plants from Western Cuba VII. Composition of the Leaf Oil of Psidium wrightii KRug et Urb., Lantana involucrata L., Cinnamonum montanum (Sw.) Berchtold et J. Persl. and Caesalpinia violacea (Mill.) Standley, J. Essent. Oil. Res., 2006, 18, 2, 170-174, https://doi.org/10.1080/10412905.2006.9699058 . [all data]

Pitarokili, Tzakou, et al., 2006
Pitarokili, D.; Tzakou, O.; Loukis, A., Essential oil composition of Salvia verticillata, S. verbenaca, S. glutinosa and S. candidissima growing wild in Greece, Flavour Fragr. J., 2006, 21, 4, 670-673, https://doi.org/10.1002/ffj.1647 . [all data]

Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005
Khalighi-Sigaroodi, F.; Hadijiakhoondi, A.; Shahverdi, A.R.; Mozaffarian, V.-A.; Shafiee, A., Chemical composition and antimicrobial activity of the essential oil of Ferulago Bernardii Tomk. and M.Pimen., DARU, 2005, 13, 3, 100-104. [all data]

Kowalski and Wolski, 2005
Kowalski, R.; Wolski, T., The chemical composition of essential oils of Silphium perfoliatum L., Flavour Fragr. J., 2005, 20, 3, 306-310, https://doi.org/10.1002/ffj.1418 . [all data]

Özel, Gögüs, et al., 2005
Özel, M.Z.; Gögüs, F.; Hamilton, J.F.; Lewis, A.C., Analysis of volatile components from Ziziphora taurica subsp. taurica by steam distillation, superheated-water extraction, and direct thermal desorption with GC×GC-TOFMS, Anal. Bioanal. Chem., 2005, 382, 1, 115-119, https://doi.org/10.1007/s00216-005-3156-x . [all data]

Sajjadi S.E. and Eskandari B., 2005
Sajjadi S.E.; Eskandari B., Chemical constituents of the essential oil of Nepeta oxyodonta, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 2, 175-177, https://doi.org/10.1007/s10600-005-0106-y . [all data]

Salehi, Sonboli, et al., 2005
Salehi, P.; Sonboli, A.; Eftekhar, F.; Nejad-Ebrahimi, S.; Yousefzadi, M., Essential Oil Composition, Antibacterial and Antioxidant Activity of the Oil and Various Extracts of Ziziphora clinopodioides subsp. rigida (BOISS.) RECH. f. from Iran, Biol. Pharm. Bull., 2005, 28, 10, 1892-1896, https://doi.org/10.1248/bpb.28.1892 . [all data]

Sarkhail, Amin, et al., 2005
Sarkhail, P.; Amin, G.; Surmaghi, M.H.S.; Shafiee, A., Composition of the volatile oils of Phlomis lanceolata Boiss. Hohen., Phlomis anisodonta Boiss. and Phlomis bruguieri Desf. from Iran, Flavour Fragr. J., 2005, 20, 3, 327-329, https://doi.org/10.1002/ffj.1427 . [all data]

Sonboli, Salehi, et al., 2005
Sonboli, A.; Salehi, P.; Allahyari, L., Essential oil composition of Nepeta involucrata from Iran, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 6, 683-685, https://doi.org/10.1007/s10600-006-0011-z . [all data]

Yayli, Yasar, et al., 2005
Yayli, N.; Yasar, A.; Gülec, C.; Usta, A.; Kolayli, S.; Coskuncelebi, K.; Karaoglu, S., Composition and antimicrobial activity of essential oils from Centaurea sessilis and Centaurea armena, Phytochemistry, 2005, 66, 14, 1741-1745, https://doi.org/10.1016/j.phytochem.2005.04.006 . [all data]

Jürgens and Dötterl, 2004
Jürgens, A.; Dötterl, S., Chemical composition of anther volatiles in Ranunculaceae: genera-specific profiles in Aemone, Aquilegia, Caltha, Pulsatilla, Ranunculus, and Trollius species, American Journal of Botany, 2004, 91, 12, 1969-1980, https://doi.org/10.3732/ajb.91.12.1969 . [all data]

Kalemba and Thiem, 2004
Kalemba, D.; Thiem, B., Constituents of the essential oils of four micropropagated Solidago species, Flavour Fragr. J., 2004, 19, 1, 40-43, https://doi.org/10.1002/ffj.1271 . [all data]

Raal, Paaver, et al., 2004
Raal, A.; Paaver, U.; Arak, E.; Orav, A., Content and composition of the essential oil of Thymus serpyllum L. growing wild in Estonia, Medicina (Kaunas), 2004, 40, 8, 795-800. [all data]

Jirovetz, Buchbauer, et al., 2003
Jirovetz, L.; Buchbauer, G.; Shafi, M.P.; Kaniampady, M.M., Chemotaxonomical analysis of the essential oil aroma compounds of four different Ocimumspecies from southern India, Eur. Food Res. Technol., 2003, 217, 2, 120-124, https://doi.org/10.1007/s00217-003-0708-1 . [all data]

Sefidkon, Naderi Nik, et al., 2003
Sefidkon, F.; Naderi Nik, A.; Bagaii, P.; Javidtash, I., Analysis of the essential oil of Stachys ixodes Boiss. Hausskn. ex Boiss. from Iran, Flavour Fragr. J., 2003, 18, 4, 301-302, https://doi.org/10.1002/ffj.1170 . [all data]

Yassa, Akhani, et al., 2003
Yassa, N.; Akhani, H.; Aqaahmadi, M.; Salimian, M., Essential oils from two endemic species of Apiaceae from Iran, Z. Naturforsch. C:, 2003, 58, 459-463. [all data]

Ghannadi, Sajjadi, et al., 2002
Ghannadi, A.; Sajjadi, S.E.; Beigihasan, A., Composition of the essential oil of Ferula ovina (Boiss.) Boiss. from Iran, DARU, 2002, 10, 4, 165-167, retrieved from http://www1.tums.ac.ir/daru/Daru4%202002/Ghannadi.PDF. [all data]

Kim and Lee, 2002
Kim, N.-S.; Lee, D.-S., Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry, J. Chromatogr. A, 2002, 982, 1, 31-47, https://doi.org/10.1016/S0021-9673(02)01445-0 . [all data]

Sefidkon, Jalili, et al., 2002
Sefidkon, F.; Jalili, A.; Mirhaji, T., Essential oil composition of three Artemisia spp. from Iran, Flavour Fragr. J., 2002, 17, 2, 150-152, https://doi.org/10.1002/ffj.1063 . [all data]

Zoghbi, Andrade, et al., 2002
Zoghbi, M.G.B.; Andrade, E.H.A.; da Silva, M.H.; Maia, J.G.S.; Luz, A.I.R.; da Silva, J.D., Chemical variation in the essential oils of Hyptis crenata Pohl ex Benth., Flavour Fragr. J., 2002, 17, 1, 5-8, https://doi.org/10.1002/ffj.1031 . [all data]

Gallori, Flamini, et al., 2001
Gallori, S.; Flamini, G.; Bilia, A.R.; Morelli, I.; Landini, A.; Vincieri, F.F., Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.), J. Agric. Food Chem., 2001, 49, 12, 5907-5910, https://doi.org/10.1021/jf0107656 . [all data]

Kalemba, Marschall, et al., 2001
Kalemba, D.; Marschall, H.; Bradesi, P., Constituents of the essential oil of Solidago gigantea Ait. (giant goldenrod), Flavour Fragr. J., 2001, 16, 1, 19-26, https://doi.org/10.1002/1099-1026(200101/02)16:1<19::AID-FFJ940>3.0.CO;2-U . [all data]

Kalemba, 1999
Kalemba, D., Constituents of the essential oil of Artemisia asiatica Nakai, Flavour Fragr. J., 1999, 14, 3, 173-176, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<173::AID-FFJ805>3.0.CO;2-Q . [all data]

Ramalho, de Freitas, et al., 1999
Ramalho, P.S.; de Freitas, V.A.P.; Macedo, A.; Silva, G.; Silva, A.M.S., Volatile components of Cistus ladanifer leaves, Flavour Fragr. J., 1999, 14, 5, 300-302, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<300::AID-FFJ830>3.0.CO;2-X . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References