trans-Verbenol


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSRTX-5DB-5DB-5MS
Column length (m) 30.30.20.50.30.
Carrier gas HeliumHeliumHeliumNitrogenHe
Substrate      
Column diameter (mm) 0.250.250.180.200.25
Phase thickness (μm) 0.250.250.200.320.25
Tstart (C) 60.50.50.60.60.
Tend (C) 220.240.280.220.240.
Heat rate (K/min) 5.3.4.5.3.
Initial hold (min) 10. 1.3. 
Final hold (min)    5. 
I 1144.1133.1148.1144.1143.
ReferenceOgunwande, Flamini, et al., 2010Sarikurkcu, Tepe, et al., 2008Skalicka-Wozniak, Los, et al., 2008Amiri, 2007Andrade, Oliveira, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5DB-1Methyl SiliconeSPB-1DB-5
Column length (m) 60.30.50.30.30.
Carrier gas HeliumHeliumHeliumHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.25 0.20.25
Tstart (C) 60.50.50.70.50.
Tend (C) 260.260.240.220.250.
Heat rate (K/min) 4.2.53.3.4.
Initial hold (min)  1.   
Final hold (min)  20. 15. 
I 1145.1121.1144.1126.1136.
ReferenceMeccia, Rojas, et al., 2007Monser-Esfahani, Karamkhani, et al., 2007Ozcan and Chalchat, 2007Pinto, Salgueiro, et al., 2007Pontes, de Olivera, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSDB-5BP-1HP-5
Column length (m) 30.60.30.50.30.
Carrier gas HeliumHydrogenHe He
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.60.
Tend (C) 260.260.240.220.246.
Heat rate (K/min) 4.4.4.2.3.
Initial hold (min)      
Final hold (min)  20. 20. 
I 1142.1138.1142.1125.1144.
ReferenceRistic, Krivokuca-Dokic, et al., 2007Rojas, Velasco, et al., 2007Sefidkon, Abbasi, et al., 2007Boti, Yao, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBHP-5 MSHP-5NB-30
Column length (m) 30.30.30.30.30.
Carrier gas HeliumN2NitrogenN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.520.25
Tstart (C) 60.50.50.50.50.
Tend (C) 260.200.280.280.250.
Heat rate (K/min) 3.5.5.5.2.
Initial hold (min)      
Final hold (min)   5.5. 
I 1145.1145.1130.1130.1152.
ReferenceJavidnia, Miri, et al., 2006Martin, Joseph, et al., 2006Marzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Orav, Raal, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5MSDB-5DB-5
Column length (m) 25.50.30.30.30.
Carrier gas N2N2HeHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 50.95.40.70.70.
Tend (C) 200.240.260.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 3.  4.4.
Final hold (min)      
I 1145.1136.1147.1144.1145.
ReferenceOuamba, Ouabonzi, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Petrovic, Ristic, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1HP-5MSMethyl SiliconeHP-5
Column length (m) 30.60.30.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.30.2
Phase thickness (μm) 0.25 0.25 0.33
Tstart (C) 60.40.60.50.60.
Tend (C) 280.250.280.240.240.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)      
Final hold (min)     7.
I 1112.1123.1136.1144.1141.
ReferencePitarokili, Tzakou, et al., 2006Sefidkon, Jamzad, et al., 2006Basta, Tzakou, et al., 2005Chalchat and Özcan, 2005Duarte, Figueira, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1DB-5HP-5MSHP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.50.35.60.60.
Tend (C) 250.265.280.280.275.
Heat rate (K/min) 3.2.54.4.4.
Initial hold (min) 3.1.2.  
Final hold (min) 10.30.   
I 1148.1125.1150.1146.1147.
ReferenceGhasemi Y., Faridi P., et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Kowalski and Wolski, 2005Sajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5MSDB-5CP Sil 5 CB
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.50.
Tend (C) 250.280.240.280.200.
Heat rate (K/min) 5.3.3.3.5.
Initial hold (min)   3.  
Final hold (min) 10.    
I 1124.1146.1168.1117.1126.
ReferenceSalehi, Sonboli, et al., 2005Slavkovska, Couladis, et al., 2005Tepe B., Sokmen M., et al., 2005Tzakou and Constantinidis, 2005Agnaniet, Menut, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1NB-30HP-5MSHP-5MS
Column length (m) 25.30.50.30.30.
Carrier gas NitrogenN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 240.300.250.280.280.
Heat rate (K/min) 3.4.2.4.3.
Initial hold (min)      
Final hold (min)      
I 1143.1134.1150.1145.1146.
ReferenceJAvidnia, Mojab, et al., 2004Kalemba and Thiem, 2004Raal, Paaver, et al., 2004Sajjadi and Shahpiri, 2004Couladis, Özcan, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSRSL-200CP Sil 5 CBDB-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.35.60.
Tend (C) 220.275.280.280.240.
Heat rate (K/min) 5.4.6.5.3.
Initial hold (min) 20. 5.2.5 
Final hold (min) 20. 5.  
I 1148.1142.1139.1124.1143.
ReferenceFeizbaksh, Saber Tehrani, et al., 2003Ghannadi, Aghazari, et al., 2003Jirovetz, Buchbauer, et al., 2003Kanjilal, Kotoky, et al., 2003Maia, Taveira, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5HP-5DB-1
Column length (m) 30.50.30.30.60.
Carrier gas HeN2H2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.95.60.60.40.
Tend (C) 280.240.280.280.260.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min)   10. 5.
Final hold (min) 30. 40.  
I 1125.1141.1144.1145.1140.
ReferenceMarongiu, Porcedda, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Sajjadi and Mehregan, 2003Sefidkon, Naderi Nik, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5MSDB-1DB-1DB-5MS
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 70.60.40.40.60.
Tend (C) 220.240.250.280.270.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min)    5. 
Final hold (min) 15.    
I 1125.1145.1122.1143.1144.
ReferenceCavaleiro, Salgueiro, et al., 2002Maia, Zoghbi, et al., 2002Sefidkon, Dabiri, et al., 2002Sefidkon, Jalili, et al., 2002Zoghbi, Andrade, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1RSL-200BP-1DB-1
Column length (m) 30.30.60.25.60.
Carrier gas N2N2H2N2N2
Substrate      
Column diameter (mm) 0.250.250.320.330.25
Phase thickness (μm) 0.250.250.251.00.25
Tstart (C) 60.60.40.60.75.
Tend (C) 220.300.250.275.220.
Heat rate (K/min) 5.4.6.4.4.
Initial hold (min) 10.   1.
Final hold (min)     8.
I 1148.1135.1141.1146.1157.
ReferenceGallori, Flamini, et al., 2001Kalemba, Marschall, et al., 2001Jirovetz, Puschmann, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Bailac, Dellacasa, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase RTX-1SPB-5HP-1
Column length (m) 30.50.60.
Carrier gas N2HeHe
Substrate    
Column diameter (mm) 0.250.320.25
Phase thickness (μm) 0.250.250.25
Tstart (C) 60.60.50.
Tend (C) 300.240.280.
Heat rate (K/min) 4.3.4.
Initial hold (min)   5.
Final hold (min)  20. 
I 1135.1146.1144.
ReferenceKalemba, 1999Doneanu and Anitescu, 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ogunwande, Flamini, et al., 2010
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Sefidkon, Jamzad, et al., 2006
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Duarte, Figueira, et al., 2005
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Ghasemi Y., Faridi P., et al., 2005
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Kowalski and Wolski, 2005
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Sajjadi S.E. and Eskandari B., 2005
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Sajjadi and Ghannadi, 2005
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Salehi, Sonboli, et al., 2005
Salehi, P.; Sonboli, A.; Eftekhar, F.; Nejad-Ebrahimi, S.; Yousefzadi, M., Essential Oil Composition, Antibacterial and Antioxidant Activity of the Oil and Various Extracts of Ziziphora clinopodioides subsp. rigida (BOISS.) RECH. f. from Iran, Biol. Pharm. Bull., 2005, 28, 10, 1892-1896, https://doi.org/10.1248/bpb.28.1892 . [all data]

Slavkovska, Couladis, et al., 2005
Slavkovska, V.; Couladis, M.; Bojovic, S.; Tzakou, O.; Pavlovic, M.; Lakusic, B.; Jancic, R., Essential oil and its systematic significance in species of Micromeria Bentham from Serbia Montenegro, Plant Systematics and Evolution, 2005, 255, 1-2, 1-15, https://doi.org/10.1007/s00606-005-0303-y . [all data]

Tepe B., Sokmen M., et al., 2005
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Notes

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